Bis[μ-2-(4-hy-droxy-phen-yl)acetato]-κO,O':O;κO:O,O'-bis-{aqua-(4,4'-bipyridine-κN)bis-[2-(4-hy-droxy-phen-yl)acetato-κO,O']thulium(III)} mono-hydrate.
Identifieur interne : 000492 ( PubMed/Checkpoint ); précédent : 000491; suivant : 000493Bis[μ-2-(4-hy-droxy-phen-yl)acetato]-κO,O':O;κO:O,O'-bis-{aqua-(4,4'-bipyridine-κN)bis-[2-(4-hy-droxy-phen-yl)acetato-κO,O']thulium(III)} mono-hydrate.
Auteurs : Jia-Lu Liu [République populaire de Chine] ; Jian-Feng Liu ; Guo-Liang ZhaoSource :
- Acta crystallographica. Section E, Structure reports online [ 1600-5368 ] ; 2010.
Abstract
In the title dinuclear complex, [Tm(2)(C(8)H(7)O(3))(6)(C(10)H(8)N(2))(2)(H(2)O)(2)]·H(2)O, the Tm(III) atoms are coordinated by eight O atoms from four 2-(4-hy-droxy-phen-yl)acetate (HPAA) ligands and a water mol-ecule, and one N atom from a 4,4'-bipyridine ligand in a distorted tricapped trigonal-prismatic geometry. While four of the HPAA ligands coordinate to just one Tm atom, the remaining two HPAA ligands bridge the two Tm atoms. In the crystal, O-H⋯O and O-H⋯N hydrogen bonds link the mol-ecules into a three-dimensional network.
DOI: 10.1107/S1600536810043898
PubMed: 21588910
Affiliations:
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<author><name sortKey="Liu, Jia Lu" sort="Liu, Jia Lu" uniqKey="Liu J" first="Jia-Lu" last="Liu">Jia-Lu Liu</name>
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<front><div type="abstract" xml:lang="en">In the title dinuclear complex, [Tm(2)(C(8)H(7)O(3))(6)(C(10)H(8)N(2))(2)(H(2)O)(2)]·H(2)O, the Tm(III) atoms are coordinated by eight O atoms from four 2-(4-hy-droxy-phen-yl)acetate (HPAA) ligands and a water mol-ecule, and one N atom from a 4,4'-bipyridine ligand in a distorted tricapped trigonal-prismatic geometry. While four of the HPAA ligands coordinate to just one Tm atom, the remaining two HPAA ligands bridge the two Tm atoms. In the crystal, O-H⋯O and O-H⋯N hydrogen bonds link the mol-ecules into a three-dimensional network.</div>
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<CommentsCorrectionsList><CommentsCorrections RefType="Cites"><RefSource>Inorg Chem. 2006 Jun 12;45(12):4801-10</RefSource>
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<CommentsCorrections RefType="Cites"><RefSource>Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22</RefSource>
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<CommentsCorrections RefType="Cites"><RefSource>Inorg Chem. 2008 Feb 4;47(3):1037-43</RefSource>
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