Heterometallic Na-Y(Ln) trifluoroacetate diglyme complexes as novel single-source precursors for upconverting NaYF4 nanocrystals co-doped with Yb and Er/Tm ions.
Identifieur interne : 000482 ( PubMed/Checkpoint ); précédent : 000481; suivant : 000483Heterometallic Na-Y(Ln) trifluoroacetate diglyme complexes as novel single-source precursors for upconverting NaYF4 nanocrystals co-doped with Yb and Er/Tm ions.
Auteurs : Shashank Mishra [France] ; Stéphane Daniele ; Gilles Ledoux ; Erwann Jeanneau ; Marie-France JoubertSource :
- Chemical communications (Cambridge, England) [ 1364-548X ] ; 2010.
Descripteurs français
- KwdFr :
- MESH :
English descriptors
- KwdEn :
- MESH :
- chemical , chemistry : Alkenes, Coordination Complexes, Erbium, Ethylene Glycols, Fluorides, Methyl Ethers, Thulium, Trifluoroacetic Acid, Yttrium.
- chemistry : Nanoparticles.
- Molecular Conformation, Temperature.
Abstract
We report synthesis of new single-source heterometallic precursors [NaLn(TFA)(4)(diglyme)] (Ln = Y, Er, Tm, Yb; TFA = trifluoroacetate), which decompose in 1-octadecene at significantly low temperature, without using any surfactant or capping reagent, to give sub-50 nm particles of cubic and/or hexagonal NaYF(4) : Yb(3+), Er(3+)/Tm(3+) materials forming well-dispersed colloidal solutions in dichloromethane and exhibiting green/blue upconversion luminescence.
DOI: 10.1039/b921474g
PubMed: 20401365
Affiliations:
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pubmed:20401365Le document en format XML
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<front><div type="abstract" xml:lang="en">We report synthesis of new single-source heterometallic precursors [NaLn(TFA)(4)(diglyme)] (Ln = Y, Er, Tm, Yb; TFA = trifluoroacetate), which decompose in 1-octadecene at significantly low temperature, without using any surfactant or capping reagent, to give sub-50 nm particles of cubic and/or hexagonal NaYF(4) : Yb(3+), Er(3+)/Tm(3+) materials forming well-dispersed colloidal solutions in dichloromethane and exhibiting green/blue upconversion luminescence.</div>
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