Tm-doped TiO2 and Tm2Ti2O7 pyrochlore nanoparticles: enhancing the photocatalytic activity of rutile with a pyrochlore phase.
Identifieur interne : 000045 ( PubMed/Checkpoint ); précédent : 000044; suivant : 000046Tm-doped TiO2 and Tm2Ti2O7 pyrochlore nanoparticles: enhancing the photocatalytic activity of rutile with a pyrochlore phase.
Auteurs : Desiré M. De Los Santos [Espagne] ; Javier Navas [Espagne] ; Teresa Aguilar [Espagne] ; Antonio Sánchez-Coronilla [Espagne] ; Concha Fernández-Lorenzo [Espagne] ; Rodrigo Alcántara [Espagne] ; Jose Carlos Pi Ero [Espagne] ; Ginesa Blanco [Espagne] ; Joaquín Martín-Calleja [Espagne]Source :
- Beilstein journal of nanotechnology [ 2190-4286 ] ; 2015.
Abstract
Tm-doped TiO2 nanoparticles were synthesized using a water-controlled hydrolysis reaction. Analysis was performed in order to determine the influence of the dopant concentration and annealing temperature on the phase, crystallinity, and electronic and optical properties of the resulting material. Various characterization techniques were utilized such as X-ray diffraction, Raman spectroscopy, X-ray photoelectron spectroscopy and UV-vis spectroscopy. For the samples annealed at 773 and 973 K, anatase phase TiO2 was obtained, predominantly internally doped with Tm(3+). ICP-AES showed that a doping concentration of up to 5.8 atom % was obtained without reducing the crystallinity of the samples. The presence of Tm(3+) was confirmed by X-ray photoelectron spectroscopy and UV-vis spectroscopy: the incorporation of Tm(3+) was confirmed by the generation of new absorption bands that could be assigned to Tm(3+) transitions. Furthermore, when the samples were annealed at 1173 K, a pyrochlore phase (Tm2Ti2O7) mixed with TiO2 was obtained with a predominant rutile phase. The photodegradation of methylene blue showed that this pyrochlore phase enhanced the photocatalytic activity of the rutile phase.
DOI: 10.3762/bjnano.6.62
PubMed: 25821701
Affiliations:
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De Los Santos</name><affiliation wicri:level="1"><nlm:affiliation>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</nlm:affiliation><country xml:lang="fr">Espagne</country><wicri:regionArea>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz)</wicri:regionArea><wicri:noRegion>E-11510 Puerto Real (Cádiz)</wicri:noRegion></affiliation></author><author><name sortKey="Navas, Javier" sort="Navas, Javier" uniqKey="Navas J" first="Javier" last="Navas">Javier Navas</name><affiliation wicri:level="1"><nlm:affiliation>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</nlm:affiliation><country xml:lang="fr">Espagne</country><wicri:regionArea>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz)</wicri:regionArea><wicri:noRegion>E-11510 Puerto Real (Cádiz)</wicri:noRegion></affiliation></author><author><name sortKey="Aguilar, Teresa" sort="Aguilar, Teresa" uniqKey="Aguilar T" first="Teresa" last="Aguilar">Teresa Aguilar</name><affiliation wicri:level="1"><nlm:affiliation>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</nlm:affiliation><country xml:lang="fr">Espagne</country><wicri:regionArea>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz)</wicri:regionArea><wicri:noRegion>E-11510 Puerto Real (Cádiz)</wicri:noRegion></affiliation></author><author><name sortKey="Sanchez Coronilla, Antonio" sort="Sanchez Coronilla, Antonio" uniqKey="Sanchez Coronilla A" first="Antonio" last="Sánchez-Coronilla">Antonio Sánchez-Coronilla</name><affiliation wicri:level="1"><nlm:affiliation>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</nlm:affiliation><country 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last="Alcántara">Rodrigo Alcántara</name><affiliation wicri:level="1"><nlm:affiliation>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</nlm:affiliation><country xml:lang="fr">Espagne</country><wicri:regionArea>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz)</wicri:regionArea><wicri:noRegion>E-11510 Puerto Real (Cádiz)</wicri:noRegion></affiliation></author><author><name sortKey="Pi Ero, Jose Carlos" sort="Pi Ero, Jose Carlos" uniqKey="Pi Ero J" first="Jose Carlos" last="Pi Ero">Jose Carlos Pi Ero</name><affiliation wicri:level="1"><nlm:affiliation>Departamento de Ciencias de los Materiales, Ingeniería Metalúrgica y Química Inorgánica, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</nlm:affiliation><country xml:lang="fr">Espagne</country><wicri:regionArea>Departamento de Ciencias de los Materiales, Ingeniería Metalúrgica y Química Inorgánica, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz)</wicri:regionArea><wicri:noRegion>E-11510 Puerto Real (Cádiz)</wicri:noRegion></affiliation></author><author><name sortKey="Blanco, Ginesa" sort="Blanco, Ginesa" uniqKey="Blanco G" first="Ginesa" last="Blanco">Ginesa Blanco</name><affiliation wicri:level="1"><nlm:affiliation>Departamento de Ciencias de los Materiales, Ingeniería Metalúrgica y Química Inorgánica, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</nlm:affiliation><country xml:lang="fr">Espagne</country><wicri:regionArea>Departamento de Ciencias de los Materiales, Ingeniería Metalúrgica y Química Inorgánica, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz)</wicri:regionArea><wicri:noRegion>E-11510 Puerto Real (Cádiz)</wicri:noRegion></affiliation></author><author><name sortKey="Martin Calleja, Joaquin" sort="Martin Calleja, Joaquin" uniqKey="Martin Calleja J" first="Joaquín" last="Martín-Calleja">Joaquín Martín-Calleja</name><affiliation wicri:level="1"><nlm:affiliation>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</nlm:affiliation><country xml:lang="fr">Espagne</country><wicri:regionArea>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz)</wicri:regionArea><wicri:noRegion>E-11510 Puerto Real (Cádiz)</wicri:noRegion></affiliation></author></analytic><series><title level="j">Beilstein journal of nanotechnology</title><idno type="eISSN">2190-4286</idno><imprint><date when="2015" type="published">2015</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Tm-doped TiO2 nanoparticles were synthesized using a water-controlled hydrolysis reaction. Analysis was performed in order to determine the influence of the dopant concentration and annealing temperature on the phase, crystallinity, and electronic and optical properties of the resulting material. Various characterization techniques were utilized such as X-ray diffraction, Raman spectroscopy, X-ray photoelectron spectroscopy and UV-vis spectroscopy. For the samples annealed at 773 and 973 K, anatase phase TiO2 was obtained, predominantly internally doped with Tm(3+). ICP-AES showed that a doping concentration of up to 5.8 atom % was obtained without reducing the crystallinity of the samples. The presence of Tm(3+) was confirmed by X-ray photoelectron spectroscopy and UV-vis spectroscopy: the incorporation of Tm(3+) was confirmed by the generation of new absorption bands that could be assigned to Tm(3+) transitions. Furthermore, when the samples were annealed at 1173 K, a pyrochlore phase (Tm2Ti2O7) mixed with TiO2 was obtained with a predominant rutile phase. The photodegradation of methylene blue showed that this pyrochlore phase enhanced the photocatalytic activity of the rutile phase.</div></front></TEI><pubmed><MedlineCitation Owner="NLM" Status="PubMed-not-MEDLINE"><PMID Version="1">25821701</PMID><DateCreated><Year>2015</Year><Month>03</Month><Day>30</Day></DateCreated><DateCompleted><Year>2015</Year><Month>03</Month><Day>30</Day></DateCompleted><DateRevised><Year>2015</Year><Month>04</Month><Day>01</Day></DateRevised><Article PubModel="Electronic-eCollection"><Journal><ISSN IssnType="Electronic">2190-4286</ISSN><JournalIssue CitedMedium="Print"><Volume>6</Volume><PubDate><Year>2015</Year></PubDate></JournalIssue><Title>Beilstein journal of nanotechnology</Title><ISOAbbreviation>Beilstein J Nanotechnol</ISOAbbreviation></Journal><ArticleTitle>Tm-doped TiO2 and Tm2Ti2O7 pyrochlore nanoparticles: enhancing the photocatalytic activity of rutile with a pyrochlore phase.</ArticleTitle><Pagination><MedlinePgn>605-16</MedlinePgn></Pagination><ELocationID EIdType="doi" ValidYN="Y">10.3762/bjnano.6.62</ELocationID><Abstract><AbstractText>Tm-doped TiO2 nanoparticles were synthesized using a water-controlled hydrolysis reaction. Analysis was performed in order to determine the influence of the dopant concentration and annealing temperature on the phase, crystallinity, and electronic and optical properties of the resulting material. Various characterization techniques were utilized such as X-ray diffraction, Raman spectroscopy, X-ray photoelectron spectroscopy and UV-vis spectroscopy. For the samples annealed at 773 and 973 K, anatase phase TiO2 was obtained, predominantly internally doped with Tm(3+). ICP-AES showed that a doping concentration of up to 5.8 atom % was obtained without reducing the crystallinity of the samples. The presence of Tm(3+) was confirmed by X-ray photoelectron spectroscopy and UV-vis spectroscopy: the incorporation of Tm(3+) was confirmed by the generation of new absorption bands that could be assigned to Tm(3+) transitions. Furthermore, when the samples were annealed at 1173 K, a pyrochlore phase (Tm2Ti2O7) mixed with TiO2 was obtained with a predominant rutile phase. The photodegradation of methylene blue showed that this pyrochlore phase enhanced the photocatalytic activity of the rutile phase.</AbstractText></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>De Los Santos</LastName><ForeName>Desiré M</ForeName><Initials>DM</Initials><AffiliationInfo><Affiliation>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Navas</LastName><ForeName>Javier</ForeName><Initials>J</Initials><AffiliationInfo><Affiliation>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Aguilar</LastName><ForeName>Teresa</ForeName><Initials>T</Initials><AffiliationInfo><Affiliation>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Sánchez-Coronilla</LastName><ForeName>Antonio</ForeName><Initials>A</Initials><AffiliationInfo><Affiliation>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Fernández-Lorenzo</LastName><ForeName>Concha</ForeName><Initials>C</Initials><AffiliationInfo><Affiliation>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Alcántara</LastName><ForeName>Rodrigo</ForeName><Initials>R</Initials><AffiliationInfo><Affiliation>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Piñero</LastName><ForeName>Jose Carlos</ForeName><Initials>JC</Initials><AffiliationInfo><Affiliation>Departamento de Ciencias de los Materiales, Ingeniería Metalúrgica y Química Inorgánica, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Blanco</LastName><ForeName>Ginesa</ForeName><Initials>G</Initials><AffiliationInfo><Affiliation>Departamento de Ciencias de los Materiales, Ingeniería Metalúrgica y Química Inorgánica, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Martín-Calleja</LastName><ForeName>Joaquín</ForeName><Initials>J</Initials><AffiliationInfo><Affiliation>Departamento de Química Física, Facultad de Ciencias, Universidad de Cádiz, E-11510 Puerto Real (Cádiz), Spain.</Affiliation></AffiliationInfo></Author></AuthorList><Language>eng</Language><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2015</Year><Month>03</Month><Day>02</Day></ArticleDate></Article><MedlineJournalInfo><Country>Germany</Country><MedlineTA>Beilstein J Nanotechnol</MedlineTA><NlmUniqueID>101551563</NlmUniqueID><ISSNLinking>2190-4286</ISSNLinking></MedlineJournalInfo><OtherID Source="NLM">PMC4362206</OtherID><KeywordList Owner="NOTNLM"><Keyword MajorTopicYN="N">nanoparticles</Keyword><Keyword MajorTopicYN="N">photocatalysis</Keyword><Keyword MajorTopicYN="N">pyrochlore</Keyword><Keyword MajorTopicYN="N">thulium</Keyword><Keyword MajorTopicYN="N">titanium dioxide</Keyword></KeywordList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="ecollection"><Year>2015</Year><Month></Month><Day></Day></PubMedPubDate><PubMedPubDate PubStatus="received"><Year>2014</Year><Month>9</Month><Day>10</Day></PubMedPubDate><PubMedPubDate PubStatus="accepted"><Year>2015</Year><Month>2</Month><Day>5</Day></PubMedPubDate><PubMedPubDate PubStatus="epublish"><Year>2015</Year><Month>3</Month><Day>2</Day></PubMedPubDate><PubMedPubDate PubStatus="entrez"><Year>2015</Year><Month>3</Month><Day>31</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="pubmed"><Year>2015</Year><Month>3</Month><Day>31</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="medline"><Year>2015</Year><Month>3</Month><Day>31</Day><Hour>6</Hour><Minute>1</Minute></PubMedPubDate></History><PublicationStatus>epublish</PublicationStatus><ArticleIdList><ArticleId IdType="doi">10.3762/bjnano.6.62</ArticleId><ArticleId IdType="pubmed">25821701</ArticleId><ArticleId IdType="pmc">PMC4362206</ArticleId></ArticleIdList></PubmedData></pubmed><affiliations><list><country><li>Espagne</li></country></list><tree><country name="Espagne"><noRegion><name sortKey="De Los Santos, Desire M" sort="De Los Santos, Desire M" uniqKey="De Los Santos D" first="Desiré M" last="De Los Santos">Desiré M. De Los Santos</name></noRegion><name sortKey="Aguilar, Teresa" sort="Aguilar, Teresa" uniqKey="Aguilar T" first="Teresa" last="Aguilar">Teresa Aguilar</name><name sortKey="Alcantara, Rodrigo" sort="Alcantara, Rodrigo" uniqKey="Alcantara R" first="Rodrigo" last="Alcántara">Rodrigo Alcántara</name><name sortKey="Blanco, Ginesa" sort="Blanco, Ginesa" uniqKey="Blanco G" first="Ginesa" last="Blanco">Ginesa Blanco</name><name sortKey="Fernandez Lorenzo, Concha" sort="Fernandez Lorenzo, Concha" uniqKey="Fernandez Lorenzo C" first="Concha" last="Fernández-Lorenzo">Concha Fernández-Lorenzo</name><name sortKey="Martin Calleja, Joaquin" sort="Martin Calleja, Joaquin" uniqKey="Martin Calleja J" first="Joaquín" last="Martín-Calleja">Joaquín Martín-Calleja</name><name sortKey="Navas, Javier" sort="Navas, Javier" uniqKey="Navas J" first="Javier" last="Navas">Javier Navas</name><name sortKey="Pi Ero, Jose Carlos" sort="Pi Ero, Jose Carlos" uniqKey="Pi Ero J" first="Jose Carlos" last="Pi Ero">Jose Carlos Pi Ero</name><name sortKey="Sanchez Coronilla, Antonio" sort="Sanchez Coronilla, Antonio" uniqKey="Sanchez Coronilla A" first="Antonio" last="Sánchez-Coronilla">Antonio Sánchez-Coronilla</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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