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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Isolation and Structural Characterization of Two Very Large, and Largely Empty, Endohedral Fullerenes: Tm@C3v-C94 and Ca@C3v-C94</title><author><name sortKey="Che, Yuliang" sort="Che, Yuliang" uniqKey="Che Y" first="Yuliang" last="Che">Yuliang Che</name><affiliation><nlm:aff id="A1"> Department of Chemistry, Zhejiang University, Hangzhou 310027, China</nlm:aff></affiliation></author><author><name sortKey="Yang, Hua" sort="Yang, Hua" uniqKey="Yang H" first="Hua" last="Yang">Hua Yang</name><affiliation><nlm:aff id="A1"> Department of Chemistry, Zhejiang University, Hangzhou 310027, China</nlm:aff></affiliation></author><author><name sortKey="Wang, Zhimin" sort="Wang, Zhimin" uniqKey="Wang Z" first="Zhimin" last="Wang">Zhimin Wang</name><affiliation><nlm:aff id="A1"> Department of Chemistry, Zhejiang University, Hangzhou 310027, China</nlm:aff></affiliation></author><author><name sortKey="Jin, Hongxiao" sort="Jin, Hongxiao" uniqKey="Jin H" first="Hongxiao" last="Jin">Hongxiao Jin</name><affiliation><nlm:aff id="A1"> Department of Chemistry, Zhejiang University, Hangzhou 310027, China</nlm:aff></affiliation></author><author><name sortKey="Liu, Ziyang" sort="Liu, Ziyang" uniqKey="Liu Z" first="Ziyang" last="Liu">Ziyang Liu</name><affiliation><nlm:aff id="A1"> Department of Chemistry, Zhejiang University, Hangzhou 310027, China</nlm:aff></affiliation></author><author><name sortKey="Lu, Chunxin" sort="Lu, Chunxin" uniqKey="Lu C" first="Chunxin" last="Lu">Chunxin Lu</name><affiliation><nlm:aff id="A1"> Department of Chemistry, Zhejiang University, Hangzhou 310027, China</nlm:aff></affiliation></author><author><name sortKey="Zuo, Tianming" sort="Zuo, Tianming" uniqKey="Zuo T" first="Tianming" last="Zuo">Tianming Zuo</name><affiliation><nlm:aff id="A2"> Department of Chemistry, Virginia Polytechnic Institute and State University, Blacksburg, VA, 24061</nlm:aff></affiliation></author><author><name sortKey="Dorn, Harry C" sort="Dorn, Harry C" uniqKey="Dorn H" first="Harry C." last="Dorn">Harry C. Dorn</name><affiliation><nlm:aff id="A2"> Department of Chemistry, Virginia Polytechnic Institute and State University, Blacksburg, VA, 24061</nlm:aff></affiliation></author><author><name sortKey="Beavers, Christine M" sort="Beavers, Christine M" uniqKey="Beavers C" first="Christine M." last="Beavers">Christine M. Beavers</name><affiliation><nlm:aff id="A3"> Department of Chemistry, University of California, Davis, One Shields Avenue, Davis, California 95616</nlm:aff></affiliation></author><author><name sortKey="Olmstead, Marilyn M" sort="Olmstead, Marilyn M" uniqKey="Olmstead M" first="Marilyn M." last="Olmstead">Marilyn M. Olmstead</name><affiliation><nlm:aff id="A3"> Department of Chemistry, University of California, Davis, One Shields Avenue, Davis, California 95616</nlm:aff></affiliation></author><author><name sortKey="Balch, Alan L" sort="Balch, Alan L" uniqKey="Balch A" first="Alan L." last="Balch">Alan L. Balch</name><affiliation><nlm:aff id="A3"> Department of Chemistry, University of California, Davis, One Shields Avenue, Davis, California 95616</nlm:aff></affiliation></author></titleStmt><publicationStmt><idno type="wicri:source">PMC</idno><idno type="pmid">19507844</idno><idno type="pmc">2878390</idno><idno type="url">http://www.ncbi.nlm.nih.gov/pmc/articles/PMC2878390</idno><idno type="RBID">PMC:2878390</idno><idno type="doi">10.1021/ic900322d</idno><date when="2009">2009</date><idno type="wicri:Area/Pmc/Corpus">000215</idno><idno type="wicri:explorRef" wicri:stream="Pmc" wicri:step="Corpus" wicri:corpus="PMC">000215</idno></publicationStmt><sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Isolation and Structural Characterization of Two Very Large, and Largely Empty, Endohedral Fullerenes: Tm@C3v-C94 and Ca@C3v-C94</title><author><name sortKey="Che, Yuliang" sort="Che, Yuliang" uniqKey="Che Y" first="Yuliang" last="Che">Yuliang Che</name><affiliation><nlm:aff id="A1"> Department of Chemistry, Zhejiang University, Hangzhou 310027, China</nlm:aff></affiliation></author><author><name sortKey="Yang, Hua" sort="Yang, Hua" uniqKey="Yang H" first="Hua" last="Yang">Hua Yang</name><affiliation><nlm:aff id="A1"> Department of Chemistry, Zhejiang University, Hangzhou 310027, China</nlm:aff></affiliation></author><author><name sortKey="Wang, Zhimin" sort="Wang, Zhimin" uniqKey="Wang Z" first="Zhimin" last="Wang">Zhimin Wang</name><affiliation><nlm:aff id="A1"> Department of Chemistry, Zhejiang University, Hangzhou 310027, China</nlm:aff></affiliation></author><author><name sortKey="Jin, Hongxiao" sort="Jin, Hongxiao" uniqKey="Jin H" first="Hongxiao" last="Jin">Hongxiao Jin</name><affiliation><nlm:aff id="A1"> Department of Chemistry, Zhejiang University, Hangzhou 310027, China</nlm:aff></affiliation></author><author><name sortKey="Liu, Ziyang" sort="Liu, Ziyang" uniqKey="Liu Z" first="Ziyang" last="Liu">Ziyang Liu</name><affiliation><nlm:aff id="A1"> Department of Chemistry, Zhejiang University, Hangzhou 310027, China</nlm:aff></affiliation></author><author><name sortKey="Lu, Chunxin" sort="Lu, Chunxin" uniqKey="Lu C" first="Chunxin" last="Lu">Chunxin Lu</name><affiliation><nlm:aff id="A1"> Department of Chemistry, Zhejiang University, Hangzhou 310027, China</nlm:aff></affiliation></author><author><name sortKey="Zuo, Tianming" sort="Zuo, Tianming" uniqKey="Zuo T" first="Tianming" last="Zuo">Tianming Zuo</name><affiliation><nlm:aff id="A2"> Department of Chemistry, Virginia Polytechnic Institute and State University, Blacksburg, VA, 24061</nlm:aff></affiliation></author><author><name sortKey="Dorn, Harry C" sort="Dorn, Harry C" uniqKey="Dorn H" first="Harry C." last="Dorn">Harry C. Dorn</name><affiliation><nlm:aff id="A2"> Department of Chemistry, Virginia Polytechnic Institute and State University, Blacksburg, VA, 24061</nlm:aff></affiliation></author><author><name sortKey="Beavers, Christine M" sort="Beavers, Christine M" uniqKey="Beavers C" first="Christine M." last="Beavers">Christine M. Beavers</name><affiliation><nlm:aff id="A3"> Department of Chemistry, University of California, Davis, One Shields Avenue, Davis, California 95616</nlm:aff></affiliation></author><author><name sortKey="Olmstead, Marilyn M" sort="Olmstead, Marilyn M" uniqKey="Olmstead M" first="Marilyn M." last="Olmstead">Marilyn M. Olmstead</name><affiliation><nlm:aff id="A3"> Department of Chemistry, University of California, Davis, One Shields Avenue, Davis, California 95616</nlm:aff></affiliation></author><author><name sortKey="Balch, Alan L" sort="Balch, Alan L" uniqKey="Balch A" first="Alan L." last="Balch">Alan L. Balch</name><affiliation><nlm:aff id="A3"> Department of Chemistry, University of California, Davis, One Shields Avenue, Davis, California 95616</nlm:aff></affiliation></author></analytic><series><title level="j">Inorganic chemistry</title><idno type="ISSN">0020-1669</idno><idno type="eISSN">1520-510X</idno><imprint><date when="2009">2009</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en"><p id="P1">The structures of two newly synthesized endohedral fullerenes - Tm@<italic>C<sub>3v</sub></italic>-C<sub>94</sub> and Ca@<italic>C<sub>3v</sub></italic>-C<sub>94</sub> - have been determined by single crystal X-ray diffraction on samples co-crystallized with Ni<sup>II</sup>(octaethylporphyrin). Both compounds exhibit the same cage geometry and conform to the isolated pentagon rule (IPR). The metal ions within these rather large cages are localized near one end and along the C<sub>3</sub> axis. While the calcium ion is situated over a C-C bond at a 6:6 ring junction, the thulium ion is positioned above a six-membered ring of the fullerene.</p></div></front></TEI><pmc article-type="research-article" xml:lang="EN"><pmc-comment>The publisher of this article does not allow downloading of the full text in XML form.</pmc-comment>
<pmc-dir>properties manuscript</pmc-dir>
<front><journal-meta><journal-id journal-id-type="nlm-journal-id">0366543</journal-id><journal-id journal-id-type="pubmed-jr-id">21948</journal-id><journal-id journal-id-type="nlm-ta">Inorg Chem</journal-id><journal-title>Inorganic chemistry</journal-title><issn pub-type="ppub">0020-1669</issn><issn pub-type="epub">1520-510X</issn></journal-meta><article-meta><article-id pub-id-type="pmid">19507844</article-id><article-id pub-id-type="pmc">2878390</article-id><article-id pub-id-type="doi">10.1021/ic900322d</article-id><article-id pub-id-type="manuscript">NIHMS134071</article-id><article-categories><subj-group subj-group-type="heading"><subject>Article</subject></subj-group></article-categories><title-group><article-title>Isolation and Structural Characterization of Two Very Large, and Largely Empty, Endohedral Fullerenes: Tm@C3v-C94 and Ca@C3v-C94</article-title></title-group><contrib-group><contrib contrib-type="author"><name><surname>Che</surname><given-names>Yuliang</given-names></name><xref rid="A1" ref-type="aff">‡</xref></contrib><contrib contrib-type="author"><name><surname>Yang</surname><given-names>Hua</given-names></name><xref rid="A1" ref-type="aff">‡</xref></contrib><contrib contrib-type="author"><name><surname>Wang</surname><given-names>Zhimin</given-names></name><xref rid="A1" ref-type="aff">‡</xref></contrib><contrib contrib-type="author"><name><surname>Jin</surname><given-names>Hongxiao</given-names></name><xref rid="A1" ref-type="aff">‡</xref></contrib><contrib contrib-type="author" corresp="yes"><name><surname>Liu</surname><given-names>Ziyang</given-names></name><xref rid="A1" ref-type="aff">‡</xref><email>zyliu@zju.edu.cn</email></contrib><contrib contrib-type="author"><name><surname>Lu</surname><given-names>Chunxin</given-names></name><xref rid="A1" ref-type="aff">‡</xref></contrib><contrib contrib-type="author"><name><surname>Zuo</surname><given-names>Tianming</given-names></name><xref rid="A2" ref-type="aff">†</xref></contrib><contrib contrib-type="author" corresp="yes"><name><surname>Dorn</surname><given-names>Harry C.</given-names></name><xref rid="A2" ref-type="aff">†</xref><email>hdorn@vt.edu</email></contrib><contrib contrib-type="author"><name><surname>Beavers</surname><given-names>Christine M.</given-names></name><xref rid="A3" ref-type="aff">+</xref></contrib><contrib contrib-type="author" corresp="yes"><name><surname>Olmstead</surname><given-names>Marilyn M.</given-names></name><xref rid="A3" ref-type="aff">+</xref><email>mmolmstead@ucdavis.edu</email></contrib><contrib contrib-type="author" corresp="yes"><name><surname>Balch</surname><given-names>Alan L.</given-names></name><xref rid="A3" ref-type="aff">+</xref><email>albalch@ucdavis.edu</email></contrib></contrib-group><aff id="A1"><label>‡</label> Department of Chemistry, Zhejiang University, Hangzhou 310027, China</aff><aff id="A2"><label>†</label> Department of Chemistry, Virginia Polytechnic Institute and State University, Blacksburg, VA, 24061</aff><aff id="A3"><label>+</label> Department of Chemistry, University of California, Davis, One Shields Avenue, Davis, California 95616</aff><pub-date pub-type="nihms-submitted"><day>5</day><month>11</month><year>2009</year></pub-date><pub-date pub-type="ppub"><day>6</day><month>7</month><year>2009</year></pub-date><pub-date pub-type="pmc-release"><day>6</day><month>7</month><year>2010</year></pub-date><volume>48</volume><issue>13</issue><fpage>6004</fpage><lpage>6010</lpage><abstract><p id="P1">The structures of two newly synthesized endohedral fullerenes - Tm@<italic>C<sub>3v</sub></italic>-C<sub>94</sub> and Ca@<italic>C<sub>3v</sub></italic>-C<sub>94</sub> - have been determined by single crystal X-ray diffraction on samples co-crystallized with Ni<sup>II</sup>(octaethylporphyrin). Both compounds exhibit the same cage geometry and conform to the isolated pentagon rule (IPR). The metal ions within these rather large cages are localized near one end and along the C<sub>3</sub> axis. While the calcium ion is situated over a C-C bond at a 6:6 ring junction, the thulium ion is positioned above a six-membered ring of the fullerene.</p></abstract><contract-num rid="CA1">R01 CA119371-01
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