ThuliumV1, Pmc, Checkpoint, bibRecord, 000331

catena-Poly[[[diaquathulium(III)]-μ-6-carboxynicotinato-μ-pyridine-2,5-dicarboxylato] dihydrate]

Identifieur interne : 000331 ( Pmc/Checkpoint ); précédent : 000330; suivant : 000332

catena-Poly[[[diaquathulium(III)]-μ-6-carboxynicotinato-μ-pyridine-2,5-dicarboxylato] dihydrate]

Auteurs : Sheng Li [République populaire de Chine] ; Yue Chen [République populaire de Chine] ; Hong-Mei He [République populaire de Chine] ; Yuan-Fang Ma [République populaire de Chine]

Source :

Acta Crystallographica Section E: Structure Reports Online [ 1600-5368 ] ; 2009.

RBID : PMC:2968913

Abstract

The title compound, {[Tm(C₇H₃NO₄)(C₇H₄NO₄)(H₂O)₂]·2H₂O}_n, is isotypic with the analogous Tb^III compound [Li et al. (2009 ▶). Acta Cryst. E65, m410]. All interatomic distances and angles and the hydrogen-bond geometries are very similar for the two structures. The refined Flack parameter of 0.49 (2) suggests inversion twinning.

Url:

http://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968913

DOI: 10.1107/S1600536809008836
PubMed: 21582354
PubMed Central: 2968913

Affiliations:

République populaire de Chine

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PMC:2968913

Le document en format XML

<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en"><italic>catena</italic>
-Poly[[[diaquathulium(III)]-μ-6-carboxynicotinato-μ-pyridine-2,5-dicarboxylato] dihydrate]</title>
<author><name sortKey="Li, Sheng" sort="Li, Sheng" uniqKey="Li S" first="Sheng" last="Li">Sheng Li</name>
<affiliation wicri:level="1"><nlm:aff id="a">Institute of Immunology, Key Laboratory of Natural Drugs and Immunological Engineering of Henan Province, College of Medicine, Henan University, Kaifeng 475003,<country>People’s Republic of China</country>
</nlm:aff>
<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Chen, Yue" sort="Chen, Yue" uniqKey="Chen Y" first="Yue" last="Chen">Yue Chen</name>
<affiliation wicri:level="1"><nlm:aff id="b">College of Medicine, Henan University, Kaifeng 475003,<country>People’s Republic of China</country>
</nlm:aff>
<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="He, Hong Mei" sort="He, Hong Mei" uniqKey="He H" first="Hong-Mei" last="He">Hong-Mei He</name>
<affiliation wicri:level="1"><nlm:aff id="b">College of Medicine, Henan University, Kaifeng 475003,<country>People’s Republic of China</country>
</nlm:aff>
<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Ma, Yuan Fang" sort="Ma, Yuan Fang" uniqKey="Ma Y" first="Yuan-Fang" last="Ma">Yuan-Fang Ma</name>
<affiliation wicri:level="1"><nlm:aff id="a">Institute of Immunology, Key Laboratory of Natural Drugs and Immunological Engineering of Henan Province, College of Medicine, Henan University, Kaifeng 475003,<country>People’s Republic of China</country>
</nlm:aff>
<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
</titleStmt>
<publicationStmt><idno type="wicri:source">PMC</idno>
<idno type="pmid">21582354</idno>
<idno type="pmc">2968913</idno>
<idno type="url">http://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968913</idno>
<idno type="RBID">PMC:2968913</idno>
<idno type="doi">10.1107/S1600536809008836</idno>
<date when="2009">2009</date>
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<idno type="wicri:explorRef" wicri:stream="Pmc" wicri:step="Checkpoint">000331</idno>
</publicationStmt>
<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main"><italic>catena</italic>
-Poly[[[diaquathulium(III)]-μ-6-carboxynicotinato-μ-pyridine-2,5-dicarboxylato] dihydrate]</title>
<author><name sortKey="Li, Sheng" sort="Li, Sheng" uniqKey="Li S" first="Sheng" last="Li">Sheng Li</name>
<affiliation wicri:level="1"><nlm:aff id="a">Institute of Immunology, Key Laboratory of Natural Drugs and Immunological Engineering of Henan Province, College of Medicine, Henan University, Kaifeng 475003,<country>People’s Republic of China</country>
</nlm:aff>
<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Chen, Yue" sort="Chen, Yue" uniqKey="Chen Y" first="Yue" last="Chen">Yue Chen</name>
<affiliation wicri:level="1"><nlm:aff id="b">College of Medicine, Henan University, Kaifeng 475003,<country>People’s Republic of China</country>
</nlm:aff>
<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="He, Hong Mei" sort="He, Hong Mei" uniqKey="He H" first="Hong-Mei" last="He">Hong-Mei He</name>
<affiliation wicri:level="1"><nlm:aff id="b">College of Medicine, Henan University, Kaifeng 475003,<country>People’s Republic of China</country>
</nlm:aff>
<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
<author><name sortKey="Ma, Yuan Fang" sort="Ma, Yuan Fang" uniqKey="Ma Y" first="Yuan-Fang" last="Ma">Yuan-Fang Ma</name>
<affiliation wicri:level="1"><nlm:aff id="a">Institute of Immunology, Key Laboratory of Natural Drugs and Immunological Engineering of Henan Province, College of Medicine, Henan University, Kaifeng 475003,<country>People’s Republic of China</country>
</nlm:aff>
<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
</author>
</analytic>
<series><title level="j">Acta Crystallographica Section E: Structure Reports Online</title>
<idno type="eISSN">1600-5368</idno>
<imprint><date when="2009">2009</date>
</imprint>
</series>
</biblStruct>
</sourceDesc>
</fileDesc>
<profileDesc><textClass></textClass>
</profileDesc>
</teiHeader>
<front><div type="abstract" xml:lang="en"><p>The title compound, {[Tm(C<sub>7</sub>
H<sub>3</sub>
NO<sub>4</sub>
)(C<sub>7</sub>
H<sub>4</sub>
NO<sub>4</sub>
)(H<sub>2</sub>
O)<sub>2</sub>
]·2H<sub>2</sub>
O}<sub><italic>n</italic>
</sub>
, is isotypic with the analogous Tb<sup>III</sup>
 compound [Li <italic>et al.</italic>
 (2009<xref ref-type="bibr" rid="bb5"> ▶</xref>
). <italic>Acta Cryst</italic>
. E<bold>65</bold>
, m410]. All interatomic distances and angles and the hydrogen-bond geometries are very similar for the two structures. The refined Flack parameter of 0.49 (2) suggests inversion twinning.</p>
</div>
</front>
<back><div1 type="bibliography"><listBibl><biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
</listBibl>
</div1>
</back>
</TEI>
<pmc article-type="research-article"><pmc-dir>properties open_access</pmc-dir>
  <front><journal-meta><journal-id journal-id-type="nlm-ta">Acta Crystallogr Sect E Struct Rep Online</journal-id>
<journal-id journal-id-type="publisher-id">Acta Cryst. E</journal-id>
<journal-title-group><journal-title>Acta Crystallographica Section E: Structure Reports Online</journal-title>
</journal-title-group>
<issn pub-type="epub">1600-5368</issn>
<publisher><publisher-name>International Union of Crystallography</publisher-name>
</publisher>
</journal-meta>
<article-meta><article-id pub-id-type="pmid">21582354</article-id>
<article-id pub-id-type="pmc">2968913</article-id>
<article-id pub-id-type="publisher-id">bi2347</article-id>
<article-id pub-id-type="doi">10.1107/S1600536809008836</article-id>
<article-id pub-id-type="coden">ACSEBH</article-id>
<article-id pub-id-type="pii">S1600536809008836</article-id>
<article-categories><subj-group subj-group-type="heading"><subject>Metal-Organic Papers</subject>
</subj-group>
</article-categories>
<title-group><article-title><italic>catena</italic>
-Poly[[[diaquathulium(III)]-μ-6-carboxynicotinato-μ-pyridine-2,5-dicarboxylato] dihydrate]</article-title>
<alt-title><italic>[Tm(C<sub>7</sub>
H<sub>3</sub>
NO<sub>4</sub>
)(C<sub>7</sub>
H<sub>4</sub>
NO<sub>4</sub>
)(H<sub>2</sub>
O)<sub>2</sub>
]·2H<sub>2</sub>
O</italic>
</alt-title>
</title-group>
<contrib-group><contrib contrib-type="author"><name><surname>Li</surname>
<given-names>Sheng</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Chen</surname>
<given-names>Yue</given-names>
</name>
<xref ref-type="aff" rid="b">b</xref>
</contrib>
<contrib contrib-type="author"><name><surname>He</surname>
<given-names>Hong-Mei</given-names>
</name>
<xref ref-type="aff" rid="b">b</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Ma</surname>
<given-names>Yuan-Fang</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
<xref ref-type="corresp" rid="cor">*</xref>
</contrib>
<aff id="a"><label>a</label>
Institute of Immunology, Key Laboratory of Natural Drugs and Immunological Engineering of Henan Province, College of Medicine, Henan University, Kaifeng 475003,<country>People’s Republic of China</country>
</aff>
<aff id="b"><label>b</label>
College of Medicine, Henan University, Kaifeng 475003,<country>People’s Republic of China</country>
</aff>
</contrib-group>
<author-notes><corresp id="cor">Correspondence e-mail: <email>mayf_hd@126.com</email>
</corresp>
</author-notes>
<pub-date pub-type="collection"><day>01</day>
<month>4</month>
<year>2009</year>
</pub-date>
<pub-date pub-type="epub"><day>19</day>
<month>3</month>
<year>2009</year>
</pub-date>
<pub-date pub-type="pmc-release"><day>19</day>
<month>3</month>
<year>2009</year>
</pub-date>
<pmc-comment> PMC Release delay is 0 months and 0 days and was based on the 
 							. </pmc-comment>
      <volume>65</volume>
<issue>Pt 4</issue>
<issue-id pub-id-type="publisher-id">e090400</issue-id>
<fpage>m411</fpage>
<lpage>m411</lpage>
<history><date date-type="received"><day>13</day>
<month>1</month>
<year>2009</year>
</date>
<date date-type="accepted"><day>10</day>
<month>3</month>
<year>2009</year>
</date>
</history>
<permissions><copyright-statement>© Li et al. 2009</copyright-statement>
<copyright-year>2009</copyright-year>
<license license-type="open-access" xlink:href="http://creativecommons.org/licenses/by/2.0/uk/"><license-p>This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.</license-p>
</license>
</permissions>
<self-uri xlink:type="simple" xlink:href="http://dx.doi.org/10.1107/S1600536809008836">A full version of this article is available from Crystallography Journals Online.</self-uri>
<abstract><p>The title compound, {[Tm(C<sub>7</sub>
H<sub>3</sub>
NO<sub>4</sub>
)(C<sub>7</sub>
H<sub>4</sub>
NO<sub>4</sub>
)(H<sub>2</sub>
O)<sub>2</sub>
]·2H<sub>2</sub>
O}<sub><italic>n</italic>
</sub>
, is isotypic with the analogous Tb<sup>III</sup>
 compound [Li <italic>et al.</italic>
 (2009<xref ref-type="bibr" rid="bb5"> ▶</xref>
). <italic>Acta Cryst</italic>
. E<bold>65</bold>
, m410]. All interatomic distances and angles and the hydrogen-bond geometries are very similar for the two structures. The refined Flack parameter of 0.49 (2) suggests inversion twinning.</p>
</abstract>
</article-meta>
</front>
<floats-group><table-wrap id="table1" position="float"><label>Table 1</label>
<caption><title>Hydrogen-bond geometry (Å, °)</title>
</caption>
<table frame="hsides" rules="groups"><thead valign="bottom"><tr><th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom">H⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H⋯<italic>A</italic>
</th>
</tr>
</thead>
<tbody valign="top"><tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O1—H1⋯O12<sup>i</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.85</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.97</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.788 (11)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">162</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O9—H91⋯O4<sup>ii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.85</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.83</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.679 (10)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">180</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O9—H92⋯O4<sup>iii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.85</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.99</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.842 (10)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">180</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O10—H101⋯O7<sup>iv</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.85</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.83</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.675 (11)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">179</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O10—H102⋯O9<sup>i</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.85</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.14</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.996 (10)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">179</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O11—H111⋯O5</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.85</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.02</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.872 (11)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">179</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O11—H112⋯O2<sup>iv</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.85</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.91</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.763 (11)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">180</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O12—H121⋯O6<sup>v</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.85</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.15</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">3.004 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">179</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O12—H122⋯O6<sup>vi</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.85</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.08</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.933 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">179</td>
</tr>
</tbody>
</table>
<table-wrap-foot><p>Symmetry codes: (i) <inline-formula><inline-graphic xlink:href="e-65-0m411-efi2.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (ii) <inline-formula><inline-graphic xlink:href="e-65-0m411-efi3.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (iii) <inline-formula><inline-graphic xlink:href="e-65-0m411-efi4.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (iv) <inline-formula><inline-graphic xlink:href="e-65-0m411-efi5.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (v) <inline-formula><inline-graphic xlink:href="e-65-0m411-efi6.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (vi) <inline-formula><inline-graphic xlink:href="e-65-0m411-efi7.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
.</p>
</table-wrap-foot>
</table-wrap>
</floats-group>
</pmc>
<affiliations><list><country><li>République populaire de Chine</li>
</country>
</list>
<tree><country name="République populaire de Chine"><noRegion><name sortKey="Li, Sheng" sort="Li, Sheng" uniqKey="Li S" first="Sheng" last="Li">Sheng Li</name>
</noRegion>
<name sortKey="Chen, Yue" sort="Chen, Yue" uniqKey="Chen Y" first="Yue" last="Chen">Yue Chen</name>
<name sortKey="He, Hong Mei" sort="He, Hong Mei" uniqKey="He H" first="Hong-Mei" last="He">Hong-Mei He</name>
<name sortKey="Ma, Yuan Fang" sort="Ma, Yuan Fang" uniqKey="Ma Y" first="Yuan-Fang" last="Ma">Yuan-Fang Ma</name>
</country>
</tree>
</affiliations>
</record>

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catena-Poly[[[diaqua­thulium(III)]-μ-6-carboxy­nicotinato-μ-pyridine-2,5-di­carboxyl­ato] dihydrate]

catena-Poly[[[diaqua­thulium(III)]-μ-6-carboxy­nicotinato-μ-pyridine-2,5-di­carboxyl­ato] dihydrate]

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catena-Poly[[[diaquathulium(III)]-μ-6-carboxynicotinato-μ-pyridine-2,5-dicarboxylato] dihydrate]

catena-Poly[[[diaquathulium(III)]-μ-6-carboxynicotinato-μ-pyridine-2,5-dicarboxylato] dihydrate]