ThuliumV1, Pascal, Curation, bibRecord, 001377

X-ray and spectral characterization of defects in garnets

Identifieur interne : 001377 ( Pascal/Curation ); précédent : 001376; suivant : 001378

X-ray and spectral characterization of defects in garnets

Auteurs : A. Lupei [Roumanie] ; C. Stoicescu [Roumanie] ; V. Lupei [Roumanie]

Source :

Journal of crystal growth [ 0022-0248 ] ; 1997.

RBID : Pascal:97-0363417

Descripteurs français

Pascal (Inist)
- Etude expérimentale, Défaut cristallin, Grenats, Impureté, Spectrométrie RX, Spectrométrie optique, Addition néodyme, Addition thulium, Addition praséodyme, Composé ternaire, Yttrium oxyde, Aluminium oxyde, Gadolinium oxyde, Gallium oxyde, Matériau laser, 6172F, Y3Al5O12, Al O Y, Gd3Ga5O12, Ga Gd O.

English descriptors

KwdEn :
- Aluminium oxides, Crystal defects, Experimental study, Gadolinium oxides, Gallium oxides, Garnets, Impurities, Laser materials, Neodymium additions, Optical spectrometry, Praseodymium additions, Ternary compounds, Thulium additions, X-ray spectroscopy, Yttrium oxides.

Abstract

New information on the defects in high temperature (HT) grown YAG (Y₃Al₅O₁₂) and GGG(Gd₃Ga₅O₁₂) obtained from X-ray and optical spectroscopy of various rare earth dopants are presented. Low intensity {2 2 2} X-ray reflections, forbidden in the cubic garnet Ia3d space group, with equivalent intensities for the four [1 1 1] directions are observed in both crystals. Structural arguments in connection with optical spectroscopy data on various ions (Nd³⁺, Tm³⁺, Pr³⁺) allow us to assign these reflections (absent in flux grown crystals) to local reduction of symmetry introduced by nonstoichiometric random occupancy of octahedral sites by Y³⁺ or Gd³⁺ ions in HT garnets.

A01	`01`	`1`		`@0 0022-0248`
A02	`01`			`@0 JCRGAE`
A03		`1`		`@0 J. cryst. growth`
A05				`@2 177`
A06				`@2 3-4`
A08	`01`	`1`	`ENG`	`@1 X-ray and spectral characterization of defects in garnets`
A11	`01`	`1`		`@1 LUPEI (A.)`
A11	`02`	`1`		`@1 STOICESCU (C.)`
A11	`03`	`1`		`@1 LUPEI (V.)`
A14	`01`			`@1 Institute of Atomic Physics @2 Bucharest 76900 @3 ROM @Z 1 aut. @Z 2 aut. @Z 3 aut.`
A20				`@1 207-210`
A21				`@1 1997`
A23	`01`			`@0 ENG`
A43	`01`			`@1 INIST @2 13507 @5 354000067387520060`
A44				`@0 0000 @1 © 1997 INIST-CNRS. All rights reserved.`
A45				`@0 11 ref.`
A47	`01`	`1`		`@0 97-0363417`
A60				`@1 P`
A61				`@0 A`
A64	`01`	`1`		`@0 Journal of crystal growth`
A66	`01`			`@0 NLD`
C01	`01`		`ENG`	@0 New information on the defects in high temperature (HT) grown YAG (Y₃Al₅O₁₂) and GGG(Gd₃Ga₅O₁₂) obtained from X-ray and optical spectroscopy of various rare earth dopants are presented. Low intensity {2 2 2} X-ray reflections, forbidden in the cubic garnet Ia3d space group, with equivalent intensities for the four [1 1 1] directions are observed in both crystals. Structural arguments in connection with optical spectroscopy data on various ions (Nd³⁺, Tm³⁺, Pr³⁺) allow us to assign these reflections (absent in flux grown crystals) to local reduction of symmetry introduced by nonstoichiometric random occupancy of octahedral sites by Y³⁺ or Gd³⁺ ions in HT garnets.
C02	`01`	`3`		`@0 001B60A72F`
C03	`01`	`3`	`FRE`	`@0 Etude expérimentale @5 01`
C03	`01`	`3`	`ENG`	`@0 Experimental study @5 01`
C03	`02`	`3`	`FRE`	`@0 Défaut cristallin @5 02`
C03	`02`	`3`	`ENG`	`@0 Crystal defects @5 02`
C03	`03`	`3`	`FRE`	`@0 Grenats @5 03`
C03	`03`	`3`	`ENG`	`@0 Garnets @5 03`
C03	`04`	`3`	`FRE`	`@0 Impureté @5 04`
C03	`04`	`3`	`ENG`	`@0 Impurities @5 04`
C03	`05`	`3`	`FRE`	`@0 Spectrométrie RX @5 05`
C03	`05`	`3`	`ENG`	`@0 X-ray spectroscopy @5 05`
C03	`06`	`X`	`FRE`	`@0 Spectrométrie optique @5 06`
C03	`06`	`X`	`ENG`	`@0 Optical spectrometry @5 06`
C03	`06`	`X`	`SPA`	`@0 Espectrometría óptica @5 06`
C03	`07`	`3`	`FRE`	`@0 Addition néodyme @5 07`
C03	`07`	`3`	`ENG`	`@0 Neodymium additions @5 07`
C03	`08`	`3`	`FRE`	`@0 Addition thulium @5 08`
C03	`08`	`3`	`ENG`	`@0 Thulium additions @5 08`
C03	`09`	`3`	`FRE`	`@0 Addition praséodyme @5 09`
C03	`09`	`3`	`ENG`	`@0 Praseodymium additions @5 09`
C03	`10`	`3`	`FRE`	`@0 Composé ternaire @5 11`
C03	`10`	`3`	`ENG`	`@0 Ternary compounds @5 11`
C03	`11`	`3`	`FRE`	`@0 Yttrium oxyde @2 NK @5 13`
C03	`11`	`3`	`ENG`	`@0 Yttrium oxides @2 NK @5 13`
C03	`12`	`3`	`FRE`	`@0 Aluminium oxyde @2 NK @5 14`
C03	`12`	`3`	`ENG`	`@0 Aluminium oxides @2 NK @5 14`
C03	`13`	`3`	`FRE`	`@0 Gadolinium oxyde @2 NK @5 16`
C03	`13`	`3`	`ENG`	`@0 Gadolinium oxides @2 NK @5 16`
C03	`14`	`3`	`FRE`	`@0 Gallium oxyde @2 NK @5 17`
C03	`14`	`3`	`ENG`	`@0 Gallium oxides @2 NK @5 17`
C03	`15`	`3`	`FRE`	`@0 Matériau laser @5 18`
C03	`15`	`3`	`ENG`	`@0 Laser materials @5 18`
C03	`16`	`3`	`FRE`	`@0 6172F @2 PAC @4 INC @5 56`
C03	`17`	`3`	`FRE`	`@0 Y3Al5O12 @4 INC @5 92`
C03	`18`	`3`	`FRE`	`@0 Al O Y @4 INC @5 93`
C03	`19`	`3`	`FRE`	`@0 Gd3Ga5O12 @4 INC @5 94`
C03	`20`	`3`	`FRE`	`@0 Ga Gd O @4 INC @5 95`
C07	`01`	`3`	`FRE`	`@0 Composé minéral @5 10`
C07	`01`	`3`	`ENG`	`@0 Inorganic compounds @5 10`
C07	`02`	`3`	`FRE`	`@0 Métal transition composé @5 12`
C07	`02`	`3`	`ENG`	`@0 Transition element compounds @5 12`
C07	`03`	`3`	`FRE`	`@0 Lanthanide composé @5 15`
C07	`03`	`3`	`ENG`	`@0 Rare earth compounds @5 15`
N21				`@1 216`

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Le document en format XML

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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a">X-ray and spectral characterization of defects in garnets</title>
<author><name sortKey="Lupei, A" sort="Lupei, A" uniqKey="Lupei A" first="A." last="Lupei">A. Lupei</name>
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<sZ>1 aut.</sZ>
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<author><name sortKey="Stoicescu, C" sort="Stoicescu, C" uniqKey="Stoicescu C" first="C." last="Stoicescu">C. Stoicescu</name>
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<sZ>2 aut.</sZ>
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<author><name sortKey="Lupei, V" sort="Lupei, V" uniqKey="Lupei V" first="V." last="Lupei">V. Lupei</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Institute of Atomic Physics</s1>
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<series><title level="j" type="main">Journal of crystal growth</title>
<title level="j" type="abbreviated">J. cryst. growth</title>
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<seriesStmt><title level="j" type="main">Journal of crystal growth</title>
<title level="j" type="abbreviated">J. cryst. growth</title>
<idno type="ISSN">0022-0248</idno>
</seriesStmt>
</fileDesc>
<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Aluminium oxides</term>
<term>Crystal defects</term>
<term>Experimental study</term>
<term>Gadolinium oxides</term>
<term>Gallium oxides</term>
<term>Garnets</term>
<term>Impurities</term>
<term>Laser materials</term>
<term>Neodymium additions</term>
<term>Optical spectrometry</term>
<term>Praseodymium additions</term>
<term>Ternary compounds</term>
<term>Thulium additions</term>
<term>X-ray spectroscopy</term>
<term>Yttrium oxides</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Etude expérimentale</term>
<term>Défaut cristallin</term>
<term>Grenats</term>
<term>Impureté</term>
<term>Spectrométrie RX</term>
<term>Spectrométrie optique</term>
<term>Addition néodyme</term>
<term>Addition thulium</term>
<term>Addition praséodyme</term>
<term>Composé ternaire</term>
<term>Yttrium oxyde</term>
<term>Aluminium oxyde</term>
<term>Gadolinium oxyde</term>
<term>Gallium oxyde</term>
<term>Matériau laser</term>
<term>6172F</term>
<term>Y3Al5O12</term>
<term>Al O Y</term>
<term>Gd3Ga5O12</term>
<term>Ga Gd O</term>
</keywords>
</textClass>
</profileDesc>
</teiHeader>
<front><div type="abstract" xml:lang="en">New information on the defects in high temperature (HT) grown YAG (Y<sub>3</sub>
Al<sub>5</sub>
O<sub>12</sub>
) and GGG(Gd<sub>3</sub>
Ga<sub>5</sub>
O<sub>12</sub>
) obtained from X-ray and optical spectroscopy of various rare earth dopants are presented. Low intensity {2 2 2} X-ray reflections, forbidden in the cubic garnet Ia3d space group, with equivalent intensities for the four [1 1 1] directions are observed in both crystals. Structural arguments in connection with optical spectroscopy data on various ions (Nd<sup>3+</sup>
, Tm<sup>3+</sup>
, Pr<sup>3+</sup>
) allow us to assign these reflections (absent in flux grown crystals) to local reduction of symmetry introduced by nonstoichiometric random occupancy of octahedral sites by Y<sup>3+</sup>
 or Gd<sup>3+</sup>
 ions in HT garnets.</div>
</front>
</TEI>
<inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>0022-0248</s0>
</fA01>
<fA02 i1="01"><s0>JCRGAE</s0>
</fA02>
<fA03 i2="1"><s0>J. cryst. growth</s0>
</fA03>
<fA05><s2>177</s2>
</fA05>
<fA06><s2>3-4</s2>
</fA06>
<fA08 i1="01" i2="1" l="ENG"><s1>X-ray and spectral characterization of defects in garnets</s1>
</fA08>
<fA11 i1="01" i2="1"><s1>LUPEI (A.)</s1>
</fA11>
<fA11 i1="02" i2="1"><s1>STOICESCU (C.)</s1>
</fA11>
<fA11 i1="03" i2="1"><s1>LUPEI (V.)</s1>
</fA11>
<fA14 i1="01"><s1>Institute of Atomic Physics</s1>
<s2>Bucharest 76900</s2>
<s3>ROM</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
</fA14>
<fA20><s1>207-210</s1>
</fA20>
<fA21><s1>1997</s1>
</fA21>
<fA23 i1="01"><s0>ENG</s0>
</fA23>
<fA43 i1="01"><s1>INIST</s1>
<s2>13507</s2>
<s5>354000067387520060</s5>
</fA43>
<fA44><s0>0000</s0>
<s1>© 1997 INIST-CNRS. All rights reserved.</s1>
</fA44>
<fA45><s0>11 ref.</s0>
</fA45>
<fA47 i1="01" i2="1"><s0>97-0363417</s0>
</fA47>
<fA60><s1>P</s1>
</fA60>
<fA61><s0>A</s0>
</fA61>
<fA64 i1="01" i2="1"><s0>Journal of crystal growth</s0>
</fA64>
<fA66 i1="01"><s0>NLD</s0>
</fA66>
<fC01 i1="01" l="ENG"><s0>New information on the defects in high temperature (HT) grown YAG (Y<sub>3</sub>
Al<sub>5</sub>
O<sub>12</sub>
) and GGG(Gd<sub>3</sub>
Ga<sub>5</sub>
O<sub>12</sub>
) obtained from X-ray and optical spectroscopy of various rare earth dopants are presented. Low intensity {2 2 2} X-ray reflections, forbidden in the cubic garnet Ia3d space group, with equivalent intensities for the four [1 1 1] directions are observed in both crystals. Structural arguments in connection with optical spectroscopy data on various ions (Nd<sup>3+</sup>
, Tm<sup>3+</sup>
, Pr<sup>3+</sup>
) allow us to assign these reflections (absent in flux grown crystals) to local reduction of symmetry introduced by nonstoichiometric random occupancy of octahedral sites by Y<sup>3+</sup>
 or Gd<sup>3+</sup>
 ions in HT garnets.</s0>
</fC01>
<fC02 i1="01" i2="3"><s0>001B60A72F</s0>
</fC02>
<fC03 i1="01" i2="3" l="FRE"><s0>Etude expérimentale</s0>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="3" l="ENG"><s0>Experimental study</s0>
<s5>01</s5>
</fC03>
<fC03 i1="02" i2="3" l="FRE"><s0>Défaut cristallin</s0>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="3" l="ENG"><s0>Crystal defects</s0>
<s5>02</s5>
</fC03>
<fC03 i1="03" i2="3" l="FRE"><s0>Grenats</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="3" l="ENG"><s0>Garnets</s0>
<s5>03</s5>
</fC03>
<fC03 i1="04" i2="3" l="FRE"><s0>Impureté</s0>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="3" l="ENG"><s0>Impurities</s0>
<s5>04</s5>
</fC03>
<fC03 i1="05" i2="3" l="FRE"><s0>Spectrométrie RX</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="3" l="ENG"><s0>X-ray spectroscopy</s0>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="X" l="FRE"><s0>Spectrométrie optique</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="ENG"><s0>Optical spectrometry</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="SPA"><s0>Espectrometría óptica</s0>
<s5>06</s5>
</fC03>
<fC03 i1="07" i2="3" l="FRE"><s0>Addition néodyme</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="3" l="ENG"><s0>Neodymium additions</s0>
<s5>07</s5>
</fC03>
<fC03 i1="08" i2="3" l="FRE"><s0>Addition thulium</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="3" l="ENG"><s0>Thulium additions</s0>
<s5>08</s5>
</fC03>
<fC03 i1="09" i2="3" l="FRE"><s0>Addition praséodyme</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="3" l="ENG"><s0>Praseodymium additions</s0>
<s5>09</s5>
</fC03>
<fC03 i1="10" i2="3" l="FRE"><s0>Composé ternaire</s0>
<s5>11</s5>
</fC03>
<fC03 i1="10" i2="3" l="ENG"><s0>Ternary compounds</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="3" l="FRE"><s0>Yttrium oxyde</s0>
<s2>NK</s2>
<s5>13</s5>
</fC03>
<fC03 i1="11" i2="3" l="ENG"><s0>Yttrium oxides</s0>
<s2>NK</s2>
<s5>13</s5>
</fC03>
<fC03 i1="12" i2="3" l="FRE"><s0>Aluminium oxyde</s0>
<s2>NK</s2>
<s5>14</s5>
</fC03>
<fC03 i1="12" i2="3" l="ENG"><s0>Aluminium oxides</s0>
<s2>NK</s2>
<s5>14</s5>
</fC03>
<fC03 i1="13" i2="3" l="FRE"><s0>Gadolinium oxyde</s0>
<s2>NK</s2>
<s5>16</s5>
</fC03>
<fC03 i1="13" i2="3" l="ENG"><s0>Gadolinium oxides</s0>
<s2>NK</s2>
<s5>16</s5>
</fC03>
<fC03 i1="14" i2="3" l="FRE"><s0>Gallium oxyde</s0>
<s2>NK</s2>
<s5>17</s5>
</fC03>
<fC03 i1="14" i2="3" l="ENG"><s0>Gallium oxides</s0>
<s2>NK</s2>
<s5>17</s5>
</fC03>
<fC03 i1="15" i2="3" l="FRE"><s0>Matériau laser</s0>
<s5>18</s5>
</fC03>
<fC03 i1="15" i2="3" l="ENG"><s0>Laser materials</s0>
<s5>18</s5>
</fC03>
<fC03 i1="16" i2="3" l="FRE"><s0>6172F</s0>
<s2>PAC</s2>
<s4>INC</s4>
<s5>56</s5>
</fC03>
<fC03 i1="17" i2="3" l="FRE"><s0>Y3Al5O12</s0>
<s4>INC</s4>
<s5>92</s5>
</fC03>
<fC03 i1="18" i2="3" l="FRE"><s0>Al O Y</s0>
<s4>INC</s4>
<s5>93</s5>
</fC03>
<fC03 i1="19" i2="3" l="FRE"><s0>Gd3Ga5O12</s0>
<s4>INC</s4>
<s5>94</s5>
</fC03>
<fC03 i1="20" i2="3" l="FRE"><s0>Ga Gd O</s0>
<s4>INC</s4>
<s5>95</s5>
</fC03>
<fC07 i1="01" i2="3" l="FRE"><s0>Composé minéral</s0>
<s5>10</s5>
</fC07>
<fC07 i1="01" i2="3" l="ENG"><s0>Inorganic compounds</s0>
<s5>10</s5>
</fC07>
<fC07 i1="02" i2="3" l="FRE"><s0>Métal transition composé</s0>
<s5>12</s5>
</fC07>
<fC07 i1="02" i2="3" l="ENG"><s0>Transition element compounds</s0>
<s5>12</s5>
</fC07>
<fC07 i1="03" i2="3" l="FRE"><s0>Lanthanide composé</s0>
<s5>15</s5>
</fC07>
<fC07 i1="03" i2="3" l="ENG"><s0>Rare earth compounds</s0>
<s5>15</s5>
</fC07>
<fN21><s1>216</s1>
</fN21>
</pA>
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   |texte=   X-ray and spectral characterization of defects in garnets
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X-ray and spectral characterization of defects in garnets

X-ray and spectral characterization of defects in garnets

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