X-Ray Detected Magnetic Resonance: A Unique Probe of the Precession Dynamics of Orbital Magnetization Components
Identifieur interne : 000543 ( Ncbi/Merge ); précédent : 000542; suivant : 000544X-Ray Detected Magnetic Resonance: A Unique Probe of the Precession Dynamics of Orbital Magnetization Components
Auteurs : Jo E Goulon [France] ; Andrei Rogalev [France] ; Gérard Goujon [France] ; Fabrice Wilhelm [France] ; Jamal Ben Youssef [France] ; Claude Gros [France] ; Jean-Michel Barbe [France] ; Roger Guilard [France]Source :
- International Journal of Molecular Sciences [ 1422-0067 ] ; 2011.
Abstract
X-ray Detected Magnetic Resonance (XDMR) is a novel spectroscopy in which X-ray Magnetic Circular Dichroism (XMCD) is used to probe the resonant precession of
Url:
DOI: 10.3390/ijms12128797
PubMed: 22272105
PubMed Central: 3257102
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nuts="2">Auvergne-Rhône-Alpes</region><region type="old region" nuts="2">Rhône-Alpes</region><settlement type="city">Grenoble</settlement></placeName></affiliation></author><author><name sortKey="Ben Youssef, Jamal" sort="Ben Youssef, Jamal" uniqKey="Ben Youssef J" first="Jamal" last="Ben Youssef">Jamal Ben Youssef</name><affiliation wicri:level="3"><nlm:aff id="af2-ijms-12-08797">Laboratoire de Magńetisme de Bretagne, CNRS FRE 2697, UFR Sciences et Techniques, F-29328 Brest Cedex, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Laboratoire de Magńetisme de Bretagne, CNRS FRE 2697, UFR Sciences et Techniques, F-29328 Brest Cedex</wicri:regionArea><placeName><region type="region" nuts="2">Région Bretagne</region><settlement type="city">Brest</settlement></placeName></affiliation></author><author><name sortKey="Gros, Claude" sort="Gros, Claude" uniqKey="Gros C" first="Claude" last="Gros">Claude Gros</name><affiliation wicri:level="4"><nlm:aff id="af3-ijms-12-08797">Institut de Chimie Moĺeculaire de l’Université de Bourgogne, UMR CNRS 5260, Groupe LIMRES, 9 Avenue Alain Savary, BP 47870, F-21078 Dijon Cedex, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Institut de Chimie Moĺeculaire de l’Université de Bourgogne, UMR CNRS 5260, Groupe LIMRES, 9 Avenue Alain Savary, BP 47870, F-21078 Dijon Cedex</wicri:regionArea><placeName><region type="region" nuts="2">Bourgogne-Franche-Comté</region><region type="old region" nuts="2">Bourgogne</region><settlement type="city">Dijon</settlement><settlement type="city">Dijon</settlement></placeName><orgName type="university">Université de Bourgogne</orgName></affiliation></author><author><name sortKey="Barbe, Jean Michel" sort="Barbe, Jean Michel" uniqKey="Barbe J" first="Jean-Michel" last="Barbe">Jean-Michel Barbe</name><affiliation wicri:level="4"><nlm:aff id="af3-ijms-12-08797">Institut de Chimie Moĺeculaire de l’Université de Bourgogne, UMR CNRS 5260, Groupe LIMRES, 9 Avenue Alain Savary, BP 47870, F-21078 Dijon Cedex, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Institut de Chimie Moĺeculaire de l’Université de Bourgogne, UMR CNRS 5260, Groupe LIMRES, 9 Avenue Alain Savary, BP 47870, F-21078 Dijon Cedex</wicri:regionArea><wicri:noRegion>21078 Dijon Cedex</wicri:noRegion><orgName type="university">Université de Bourgogne</orgName><placeName><settlement type="city">Dijon</settlement><region type="region" nuts="2">Région Bourgogne</region></placeName></affiliation></author><author><name sortKey="Guilard, Roger" sort="Guilard, Roger" uniqKey="Guilard R" first="Roger" last="Guilard">Roger Guilard</name><affiliation wicri:level="4"><nlm:aff id="af3-ijms-12-08797">Institut de Chimie Moĺeculaire de l’Université de Bourgogne, UMR CNRS 5260, Groupe LIMRES, 9 Avenue Alain Savary, BP 47870, F-21078 Dijon Cedex, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Institut de Chimie Moĺeculaire de l’Université de Bourgogne, UMR CNRS 5260, Groupe LIMRES, 9 Avenue Alain Savary, BP 47870, F-21078 Dijon Cedex</wicri:regionArea><wicri:noRegion>21078 Dijon Cedex</wicri:noRegion><orgName type="university">Université de Bourgogne</orgName><placeName><settlement type="city">Dijon</settlement><region type="region" nuts="2">Région Bourgogne</region></placeName></affiliation></author></analytic><series><title level="j">International Journal of Molecular Sciences</title><idno type="eISSN">1422-0067</idno><imprint><date when="2011">2011</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en"><p>X-ray Detected Magnetic Resonance (XDMR) is a novel spectroscopy in which X-ray Magnetic Circular Dichroism (XMCD) is used to probe the resonant precession of <italic>local</italic> magnetization components in a strong microwave pump field. We review the conceptual bases of XDMR and recast them in the general framework of the linear and nonlinear theories of ferromagnetic resonance (FMR). Emphasis is laid on the information content of XDMR spectra which offer a unique opportunity to disentangle the precession dynamics of spin and orbital magnetization components at given absorbing sites. For the sake of illustration, we focus on selected examples in which marked differences were found between FMR and XDMR spectra simultaneously recorded on ferrimagnetically ordered iron garnets. With pumping capabilities extended up to sub-THz frequencies, high-field XDMR should allow us to probe the precession of orbital magnetization components in paramagnetic organometallic complexes with large zero-field splitting. Even more challenging, we suggest that XDMR spectra might be recorded on selected antiferromagnetic crystals for which orbital magnetism is most often ignored in the absence of any supporting experimental evidence.</p></div></front><back><div1 type="bibliography"><listBibl><biblStruct><analytic><author><name sortKey="Thole, B T" uniqKey="Thole B">B.T. Thole</name></author><author><name sortKey="Carra, P" uniqKey="Carra P">P. Carra</name></author><author><name sortKey="Sette, F" uniqKey="Sette F">F. Sette</name></author><author><name sortKey="Van Der Laan, G" uniqKey="Van Der Laan G">G. van der Laan</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Carra, P" uniqKey="Carra P">P. Carra</name></author><author><name sortKey="Thole, B T" uniqKey="Thole B">B.T. Thole</name></author><author><name sortKey="Altarelli, M" uniqKey="Altarelli M">M. Altarelli</name></author><author><name sortKey="Wang, X" uniqKey="Wang X">X. 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<front><journal-meta><journal-id journal-id-type="nlm-ta">Int J Mol Sci</journal-id><journal-id journal-id-type="publisher-id">ijms</journal-id><journal-title-group><journal-title>International Journal of Molecular Sciences</journal-title></journal-title-group><issn pub-type="epub">1422-0067</issn><publisher><publisher-name>Molecular Diversity Preservation International (MDPI)</publisher-name></publisher></journal-meta><article-meta><article-id pub-id-type="pmid">22272105</article-id><article-id pub-id-type="pmc">3257102</article-id><article-id pub-id-type="doi">10.3390/ijms12128797</article-id><article-id pub-id-type="publisher-id">ijms-12-08797</article-id><article-categories><subj-group subj-group-type="heading"><subject>Review</subject></subj-group></article-categories><title-group><article-title>X-Ray Detected Magnetic Resonance: A Unique Probe of the Precession Dynamics of <italic>Orbital</italic> Magnetization Components</article-title></title-group><contrib-group><contrib contrib-type="author"><name><surname>Goulon</surname><given-names>Jośe</given-names></name><xref ref-type="aff" rid="af1-ijms-12-08797">1</xref><xref ref-type="corresp" rid="c1-ijms-12-08797">*</xref></contrib><contrib contrib-type="author"><name><surname>Rogalev</surname><given-names>Andrei</given-names></name><xref ref-type="aff" rid="af1-ijms-12-08797">1</xref></contrib><contrib contrib-type="author"><name><surname>Goujon</surname><given-names>Gérard</given-names></name><xref ref-type="aff" rid="af1-ijms-12-08797">1</xref></contrib><contrib contrib-type="author"><name><surname>Wilhelm</surname><given-names>Fabrice</given-names></name><xref ref-type="aff" rid="af1-ijms-12-08797">1</xref></contrib><contrib contrib-type="author"><name><surname>Ben Youssef</surname><given-names>Jamal</given-names></name><xref ref-type="aff" rid="af2-ijms-12-08797">2</xref></contrib><contrib contrib-type="author"><name><surname>Gros</surname><given-names>Claude</given-names></name><xref ref-type="aff" rid="af3-ijms-12-08797">3</xref></contrib><contrib contrib-type="author"><name><surname>Barbe</surname><given-names>Jean-Michel</given-names></name><xref ref-type="aff" rid="af3-ijms-12-08797">3</xref></contrib><contrib contrib-type="author"><name><surname>Guilard</surname><given-names>Roger</given-names></name><xref ref-type="aff" rid="af3-ijms-12-08797">3</xref></contrib></contrib-group><aff id="af1-ijms-12-08797"><label>1</label>European Synchrotron Radiation Facility, B.P. 220, F-38043 Grenoble Cedex, France</aff><aff id="af2-ijms-12-08797"><label>2</label>Laboratoire de Magńetisme de Bretagne, CNRS FRE 2697, UFR Sciences et Techniques, F-29328 Brest Cedex, France</aff><aff id="af3-ijms-12-08797"><label>3</label>Institut de Chimie Moĺeculaire de l’Université de Bourgogne, UMR CNRS 5260, Groupe LIMRES, 9 Avenue Alain Savary, BP 47870, F-21078 Dijon Cedex, France</aff><author-notes><corresp id="c1-ijms-12-08797"><label>*</label>Author to whom correspondence should be addressed; E-Mail: <email>goulon@esrf.fr</email>; Tel.: +33-04-76-88-2021, Fax: +33-04-76-88-2160.</corresp></author-notes><pub-date pub-type="collection"><year>2011</year></pub-date><pub-date pub-type="epub"><day>02</day><month>12</month><year>2011</year></pub-date><volume>12</volume><issue>12</issue><fpage>8797</fpage><lpage>8835</lpage><history><date date-type="received"><day>11</day><month>10</month><year>2011</year></date><date date-type="rev-recd"><day>12</day><month>11</month><year>2011</year></date><date date-type="accepted"><day>15</day><month>11</month><year>2011</year></date></history><permissions><copyright-statement>© 2011 by the authors; licensee MDPI, Basel, Switzerland.</copyright-statement><copyright-year>2011</copyright-year><license license-type="open-access" xlink:href="http://creativecommons.org/licenses/by/3.0"><license-p><pmc-comment>CREATIVE COMMONS</pmc-comment>This article is an open-access article distributed under the terms and conditions of the Creative Commons Attribution license (<ext-link ext-link-type="uri" xlink:href="http://creativecommons.org/licenses/by/3.0/">http://creativecommons.org/licenses/by/3.0/</ext-link>).</license-p></license></permissions><abstract><p>X-ray Detected Magnetic Resonance (XDMR) is a novel spectroscopy in which X-ray Magnetic Circular Dichroism (XMCD) is used to probe the resonant precession of <italic>local</italic> magnetization components in a strong microwave pump field. We review the conceptual bases of XDMR and recast them in the general framework of the linear and nonlinear theories of ferromagnetic resonance (FMR). Emphasis is laid on the information content of XDMR spectra which offer a unique opportunity to disentangle the precession dynamics of spin and orbital magnetization components at given absorbing sites. For the sake of illustration, we focus on selected examples in which marked differences were found between FMR and XDMR spectra simultaneously recorded on ferrimagnetically ordered iron garnets. With pumping capabilities extended up to sub-THz frequencies, high-field XDMR should allow us to probe the precession of orbital magnetization components in paramagnetic organometallic complexes with large zero-field splitting. Even more challenging, we suggest that XDMR spectra might be recorded on selected antiferromagnetic crystals for which orbital magnetism is most often ignored in the absence of any supporting experimental evidence.</p></abstract><kwd-group><kwd>XDMR</kwd><kwd>XMCD</kwd><kwd>FMR</kwd><kwd>high field EPR</kwd><kwd>AFMR</kwd></kwd-group></article-meta></front><floats-group><fig id="f1-ijms-12-08797" position="float"><label>Figure 1</label><caption><p>(<bold>A</bold>) <italic>Ab initio</italic> simulations of the spin polarized DOS projected on the irreducible representations of groups
<inline-graphic xlink:href="ijms-12-08797f16.jpg"></inline-graphic> and <italic>S</italic><sub>6</sub> at the Fe (24d) and Fe (16a) crystal sites in YIG: opposite signs were expected due to the antiferromagnetic coupling of the Fe cations in (24d) and (16a) sites; (<bold>B</bold>) Simulated XMCD spectra in the energy range of the Fe K-edge pre-peak. Note that the XMCD signal due to electric dipole transitions (<italic>E</italic>1) is much stronger at the tetrahedral (
<inline-graphic xlink:href="ijms-12-08797f16.jpg"></inline-graphic>) than at the octahedral (
<inline-graphic xlink:href="ijms-12-08797f17.jpg"></inline-graphic>) coordination sites. The contributions of electric quadrupole transitions (<italic>E</italic>2) are one order of magnitude weaker.</p></caption><graphic xlink:href="ijms-12-08797f1"></graphic></fig><fig id="f2-ijms-12-08797" position="float"><label>Figure 2</label><caption><p>XDMR in transverse pumping mode with either longitudinal or transverse detection geometries for near perpendicular magnetization. The precession cone angle <italic>θ</italic><sub>0</sub> never exceeds a few degrees and was exaggerated for clarity. As compared to <italic>m</italic><sub>⊥</sub>, <italic>m</italic><italic><sub>z</sub></italic> is only a second order perturbation.</p></caption><graphic xlink:href="ijms-12-08797f2"></graphic></fig><fig id="f3-ijms-12-08797" position="float"><label>Figure 3</label><caption><p>(<bold>A</bold>) First- and (<bold>B</bold>) second-order instability processes resulting in a conversion of uniform magnons into degenerated non-uniform magnons in transverse pumping geometry; (<bold>C</bold>) Parallel pumping geometry: direct excitation of a pair of non-uniform magnons with opposite wavevectors (<italic>k</italic>,<italic>–k</italic>) and opposite helicities. This non-linear, 2nd order process may contribute to a non-vanishing XDMR signal <italic>only</italic> in the longitudinal detection geometry (LOD).</p></caption><graphic xlink:href="ijms-12-08797f3"></graphic></fig><fig id="f4-ijms-12-08797" position="float"><label>Figure 4</label><caption><p>(<bold>A</bold>) Complex vector XDMR spectrum of film <bold>1</bold> recorded in transverse detection geometry (TRD) with a pumping power of 10mW. Arrows point to weak satellite resonances assigned to magnetostatic modes; (<bold>B</bold>) Comparison of FMR and XDMR PSD spectra that were simultaneously recorded again in TRD geometry but with a pumping power of only 1 mW. Note the fairly different lineshapes of the main resonances assigned to the uniform mode. Moreover, there is only a very weak contribution of the magnetostatic modes (BMSW) satellites in XDMR.</p></caption><graphic xlink:href="ijms-12-08797f4"></graphic></fig><fig id="f5-ijms-12-08797" position="float"><label>Figure 5</label><caption><p>(<bold>A</bold>) Foldover distorted XDMR and FMR spectra of film <bold>2</bold> showing hysteretic profiles when the bias field is scanned up and down; the XDMR spectrum was recorded in longitudinal detection geometry (LOD) under a pumping power of 630 mW. Note the very sharp increase of the XDMR signal just before the foldover jump whereas the FMR spectrum seems to saturate; (<bold>B</bold>) Modified Kasuya–LeCraw relaxation mechanisms involving an orbiton either in a 3-boson de-excitation (<bold>a</bold>) or excitation (<bold>b</bold>) process.</p></caption><graphic xlink:href="ijms-12-08797f5"></graphic></fig><fig id="f6-ijms-12-08797" position="float"><label>Figure 6</label><caption><p>Complex vector XDMR spectra recorded in transverse detection geometry (TRD) with a thin single crystal platelet of GdIG cut parallel to the (110) plane: (<bold>A</bold>) <italic>Below</italic> the compensation point, <italic>i.e.</italic>, at <italic>T ≃</italic> 150 K <italic>< T</italic><italic><sub>cp</sub></italic> = 286 K; (<bold>B</bold>) <italic>Above</italic> the compensation point, at <italic>T</italic> = 450 K <italic>> T</italic><italic><sub>cp</sub></italic>. Note the very weak intensity of the absorptive part (<italic>Re{</italic>XDMR<italic>}</italic>) and the heavily distorted lineshape of the modulus spectrum (<italic>|</italic>XDMR<italic>|</italic>); (<bold>C</bold>) Complex vector XDMR spectra typically expected for two magnetization components precessing in phase but with opposite helicity. Note that the absorptive part (<italic>Re{</italic>XDMR<italic>}</italic>) again tends to vanish whereas the modulus spectrum (<italic>|</italic>XDMR<italic>|</italic>) exhibits a characteristic “dip” at resonance as also observed in (<bold>B</bold>).</p></caption><graphic xlink:href="ijms-12-08797f6"></graphic></fig><fig id="f7-ijms-12-08797" position="float"><label>Figure 7</label><caption><p>(<bold>A</bold>) Vector Components and PSD XDMR spectra of the YIG film <bold>1</bold> recorded in the frequency doubling mode and longitudinal detection geometry (LOD); the pumping frequency was 4.226 GHz but the XDMR signal was oscillating at 8.452 GHz. Note that the 2 <italic>× F</italic> XDMR PSD spectrum does not reproduce the foldover lineshape of the FMR PSD spectrum. Regarding the vector 2 <italic>× F</italic> XDMR spectra, it seems that resonance may also take place at lower field; (<bold>B</bold>) Parallel pumping PSD XDMR spectrum of the Y-La-LuIG film <bold>2</bold> recorded in LOD geometry under high pumping power at 8.452 GHz. Whereas the microwave absorption spectrum due to the parametric excitation of exchange spin waves extends down to very low fields, this is not the case for the XDMR spectrum which exhibits only a sharp peak at <italic>H</italic><italic><sub>max</sub></italic>.</p></caption><graphic xlink:href="ijms-12-08797f7"></graphic></fig><fig id="f8-ijms-12-08797" position="float"><label>Figure 8</label><caption><p>(<bold>A</bold>) XANES and XMCD spectra recorded at the Co K-edge for a powdered pellet of <bold>3</bold> = TPP:Co; (<bold>B</bold>) XANES and XMCD spectra recorded at the Re L<sub>2</sub><italic><sub>,</sub></italic><sub>3</sub>-edges for a powdered pellet of <bold>4</bold> = [Re(CN)<sub>7</sub>](Bu<sub>4</sub>N)<sub>3</sub>. Note that the XMCD signal measured at the Re L-edges is much stronger than at the Co K-edge.</p></caption><graphic xlink:href="ijms-12-08797f8"></graphic></fig><fig id="f9-ijms-12-08797" position="float"><label>Figure 9</label><caption><p>Precession modes in an antiferromagnet with an easy axis of anisotropy: (<bold>A</bold>) and (<bold>B</bold>) refer to an antiparallel ground state; (<bold>C</bold>) is for a noncollinear ground state (spin-flop mode). Since the precession cone angles <italic>θ</italic><sub>1</sub> and <italic>θ</italic><sub>2</sub> are unequal in configurations (<bold>A</bold>) and (<bold>B</bold>), a weak XDMR signal may still be detectable in the transverse detection geometry (TRD).</p></caption><graphic xlink:href="ijms-12-08797f9"></graphic></fig></floats-group></pmc><affiliations><list><country><li>France</li></country><region><li>Auvergne-Rhône-Alpes</li><li>Bourgogne</li><li>Bourgogne-Franche-Comté</li><li>Rhône-Alpes</li><li>Région Bourgogne</li><li>Région Bretagne</li></region><settlement><li>Brest</li><li>Dijon</li><li>Grenoble</li></settlement><orgName><li>Université de Bourgogne</li></orgName></list><tree><country name="France"><region name="Auvergne-Rhône-Alpes"><name sortKey="Goulon, Jo E" sort="Goulon, Jo E" uniqKey="Goulon J" first="Jo E" last="Goulon">Jo E Goulon</name></region><name sortKey="Barbe, Jean Michel" sort="Barbe, Jean Michel" uniqKey="Barbe J" first="Jean-Michel" last="Barbe">Jean-Michel Barbe</name><name sortKey="Ben Youssef, Jamal" sort="Ben Youssef, Jamal" uniqKey="Ben Youssef J" first="Jamal" last="Ben Youssef">Jamal Ben Youssef</name><name sortKey="Goujon, Gerard" sort="Goujon, Gerard" uniqKey="Goujon G" first="Gérard" last="Goujon">Gérard Goujon</name><name sortKey="Gros, Claude" sort="Gros, Claude" uniqKey="Gros C" first="Claude" last="Gros">Claude Gros</name><name sortKey="Guilard, Roger" sort="Guilard, Roger" uniqKey="Guilard R" first="Roger" last="Guilard">Roger Guilard</name><name sortKey="Rogalev, Andrei" sort="Rogalev, Andrei" uniqKey="Rogalev A" first="Andrei" last="Rogalev">Andrei Rogalev</name><name sortKey="Wilhelm, Fabrice" sort="Wilhelm, Fabrice" uniqKey="Wilhelm F" first="Fabrice" last="Wilhelm">Fabrice Wilhelm</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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