Mechanical Properties and Crystallization Behavior of GeS2–Sb2S3–In2S3 Chalcogenide Glass
Identifieur interne : 003131 ( Istex/Corpus ); précédent : 003130; suivant : 003132Mechanical Properties and Crystallization Behavior of GeS2–Sb2S3–In2S3 Chalcogenide Glass
Auteurs : Lei Ying ; Changgui Lin ; Qiuhua Nie ; Zhuobin Li ; Yinsheng Xu ; Feifei Chen ; Shixun DaiSource :
- Journal of the American Ceramic Society [ 0002-7820 ] ; 2012-04.
English descriptors
- KwdEn :
- Activation energy, Base glass, Bulk samples, Calvez, Ceramics, Chalcogenide, Chalcogenide glass, Chalcogenide glasses, Characteristic temperatures, Crystal phase, Crystal phases, Crystallization, Crystallization behavior, Crystallization kinetics, Crystallization mechanism, Crystallization process, Crystallization rate, Exothermic peak, Gaussian functions, Ges2, Ges2 crystals, Ges2 phase, Glass ceramics, Glass formation, Glass matrix, Glass network, Glasses ceramics, Glasses heattreated, Glassy matrix, Heating rate, Heating rates, Jcpds card, Kinetic parameters, Matrix, Mechanical properties, Metallic halide, Natural science foundation, Ningbo, Ningbo city, Ningbo university, Optical properties, Raman, Raman spectra, Room temperature, Several peaks, Spectral region, Thermal imaging, Total crystallization, Transmission spectra, Zhang.
- Teeft :
- Activation energy, Base glass, Bulk samples, Calvez, Ceramics, Chalcogenide, Chalcogenide glass, Chalcogenide glasses, Characteristic temperatures, Crystal phase, Crystal phases, Crystallization, Crystallization behavior, Crystallization kinetics, Crystallization mechanism, Crystallization process, Crystallization rate, Exothermic peak, Gaussian functions, Ges2, Ges2 crystals, Ges2 phase, Glass ceramics, Glass formation, Glass matrix, Glass network, Glasses ceramics, Glasses heattreated, Glassy matrix, Heating rate, Heating rates, Jcpds card, Kinetic parameters, Matrix, Mechanical properties, Metallic halide, Natural science foundation, Ningbo, Ningbo city, Ningbo university, Optical properties, Raman, Raman spectra, Room temperature, Several peaks, Spectral region, Thermal imaging, Total crystallization, Transmission spectra, Zhang.
Abstract
54GeS2–36Sb2S3–10In2S3 glass‐ceramics were prepared by heat‐treating the base glass above Tg for different durations. The results of Raman spectra and XRD patterns show that the first precipitated crystals during the heat treatment are In2S3 and the crystallization of the Sb2S3 and GeS2 subsequently occurs. Bulk samples heat‐treated at 295°C for different heating rates and durations are used to study the crystallization mechanism and evolution of the three crystallization peaks (CPs). It is found that three CPs partly overlap with each other and then separate with increasing heat‐treating durations.
Url:
DOI: 10.1111/j.1551-2916.2012.05117.x
Links to Exploration step
ISTEX:DF0BB478205AFDACB615A4DA6FC69D51CAF57AE9Le document en format XML
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Nie</name><affiliation><mods:affiliation>The School of Information Science and Engineering, Ningbo University, 315211, Ningbo, China</mods:affiliation></affiliation></author><author><name sortKey="Li, Zhuobin" sort="Li, Zhuobin" uniqKey="Li Z" first="Zhuobin" last="Li">Zhuobin Li</name><affiliation><mods:affiliation>The School of Information Science and Engineering, Ningbo University, 315211, Ningbo, China</mods:affiliation></affiliation></author><author><name sortKey="Xu, Yinsheng" sort="Xu, Yinsheng" uniqKey="Xu Y" first="Yinsheng" last="Xu">Yinsheng Xu</name><affiliation><mods:affiliation>The School of Materials Science and Chemical Engineering, Ningbo University, 315211, Ningbo, China</mods:affiliation></affiliation></author><author><name sortKey="Chen, Feifei" sort="Chen, Feifei" uniqKey="Chen F" first="Feifei" last="Chen">Feifei Chen</name><affiliation><mods:affiliation>The School of Information Science and Engineering, Ningbo University, 315211, Ningbo, China</mods:affiliation></affiliation></author><author><name sortKey="Dai, Shixun" sort="Dai, Shixun" uniqKey="Dai S" first="Shixun" last="Dai">Shixun Dai</name><affiliation><mods:affiliation>The School of Information Science and Engineering, Ningbo University, 315211, Ningbo, China</mods:affiliation></affiliation><affiliation><mods:affiliation>E-mail: linchanggui@nbu.edu.cn</mods:affiliation></affiliation></author></titleStmt><publicationStmt><idno type="wicri:source">ISTEX</idno><idno type="RBID">ISTEX:DF0BB478205AFDACB615A4DA6FC69D51CAF57AE9</idno><date when="2012" year="2012">2012</date><idno type="doi">10.1111/j.1551-2916.2012.05117.x</idno><idno type="url">https://api.istex.fr/document/DF0BB478205AFDACB615A4DA6FC69D51CAF57AE9/fulltext/pdf</idno><idno type="wicri:Area/Istex/Corpus">003131</idno><idno type="wicri:explorRef" wicri:stream="Istex" wicri:step="Corpus" wicri:corpus="ISTEX">003131</idno></publicationStmt><sourceDesc><biblStruct><analytic><title level="a" type="main">Mechanical Properties and Crystallization Behavior of <hi rend="fc"><hi rend="fr">GeS</hi></hi><hi rend="subscript">2</hi>–<hi rend="fc"><hi rend="fr">Sb</hi></hi><hi rend="subscript">2</hi><hi rend="fc"><hi rend="fr">S</hi></hi><hi rend="subscript">3</hi>–<hi rend="fc"><hi rend="fr">In</hi></hi><hi rend="subscript">2</hi><hi rend="fc"><hi rend="fr">S</hi></hi><hi rend="subscript">3</hi> Chalcogenide Glass</title><author><name sortKey="Ying, Lei" sort="Ying, Lei" uniqKey="Ying L" first="Lei" last="Ying">Lei Ying</name><affiliation><mods:affiliation>The School of Information Science and Engineering, Ningbo University, 315211, Ningbo, China</mods:affiliation></affiliation></author><author><name sortKey="Lin, Changgui" sort="Lin, Changgui" uniqKey="Lin C" first="Changgui" last="Lin">Changgui Lin</name><affiliation><mods:affiliation>The School of Materials Science and Chemical Engineering, Ningbo University, 315211, Ningbo, China</mods:affiliation></affiliation><affiliation><mods:affiliation>E-mail: linchanggui@nbu.edu.cn</mods:affiliation></affiliation></author><author><name sortKey="Nie, Qiuhua" sort="Nie, Qiuhua" uniqKey="Nie Q" first="Qiuhua" last="Nie">Qiuhua Nie</name><affiliation><mods:affiliation>The School of Information Science and Engineering, Ningbo University, 315211, Ningbo, China</mods:affiliation></affiliation></author><author><name sortKey="Li, Zhuobin" sort="Li, Zhuobin" uniqKey="Li Z" first="Zhuobin" last="Li">Zhuobin Li</name><affiliation><mods:affiliation>The School of Information Science and Engineering, Ningbo University, 315211, Ningbo, China</mods:affiliation></affiliation></author><author><name sortKey="Xu, Yinsheng" sort="Xu, Yinsheng" uniqKey="Xu Y" first="Yinsheng" last="Xu">Yinsheng Xu</name><affiliation><mods:affiliation>The School of Materials Science and Chemical Engineering, Ningbo University, 315211, Ningbo, China</mods:affiliation></affiliation></author><author><name sortKey="Chen, Feifei" sort="Chen, Feifei" uniqKey="Chen F" first="Feifei" last="Chen">Feifei Chen</name><affiliation><mods:affiliation>The School of Information Science and Engineering, Ningbo University, 315211, Ningbo, China</mods:affiliation></affiliation></author><author><name sortKey="Dai, Shixun" sort="Dai, Shixun" uniqKey="Dai S" first="Shixun" last="Dai">Shixun Dai</name><affiliation><mods:affiliation>The School of Information Science and Engineering, Ningbo University, 315211, Ningbo, China</mods:affiliation></affiliation><affiliation><mods:affiliation>E-mail: linchanggui@nbu.edu.cn</mods:affiliation></affiliation></author></analytic><monogr></monogr><series><title level="j" type="main">Journal of the American Ceramic Society</title><title level="j" type="alt">JOURNAL OF THE AMERICAN CERAMIC SOCIETY</title><idno type="ISSN">0002-7820</idno><idno type="eISSN">1551-2916</idno><imprint><biblScope unit="vol">95</biblScope><biblScope unit="issue">4</biblScope><biblScope unit="page" from="1320">1320</biblScope><biblScope unit="page" to="1325">1325</biblScope><biblScope unit="page-count">6</biblScope><date type="published" when="2012-04">2012-04</date></imprint><idno type="ISSN">0002-7820</idno></series></biblStruct></sourceDesc><seriesStmt><idno type="ISSN">0002-7820</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Activation energy</term><term>Base glass</term><term>Bulk samples</term><term>Calvez</term><term>Ceramics</term><term>Chalcogenide</term><term>Chalcogenide glass</term><term>Chalcogenide glasses</term><term>Characteristic temperatures</term><term>Crystal phase</term><term>Crystal phases</term><term>Crystallization</term><term>Crystallization behavior</term><term>Crystallization kinetics</term><term>Crystallization mechanism</term><term>Crystallization process</term><term>Crystallization rate</term><term>Exothermic peak</term><term>Gaussian functions</term><term>Ges2</term><term>Ges2 crystals</term><term>Ges2 phase</term><term>Glass ceramics</term><term>Glass formation</term><term>Glass matrix</term><term>Glass network</term><term>Glasses ceramics</term><term>Glasses heattreated</term><term>Glassy matrix</term><term>Heating rate</term><term>Heating rates</term><term>Jcpds card</term><term>Kinetic parameters</term><term>Matrix</term><term>Mechanical properties</term><term>Metallic halide</term><term>Natural science foundation</term><term>Ningbo</term><term>Ningbo city</term><term>Ningbo university</term><term>Optical properties</term><term>Raman</term><term>Raman spectra</term><term>Room temperature</term><term>Several peaks</term><term>Spectral region</term><term>Thermal imaging</term><term>Total crystallization</term><term>Transmission spectra</term><term>Zhang</term></keywords><keywords scheme="Teeft" xml:lang="en"><term>Activation energy</term><term>Base glass</term><term>Bulk samples</term><term>Calvez</term><term>Ceramics</term><term>Chalcogenide</term><term>Chalcogenide glass</term><term>Chalcogenide glasses</term><term>Characteristic temperatures</term><term>Crystal phase</term><term>Crystal phases</term><term>Crystallization</term><term>Crystallization behavior</term><term>Crystallization kinetics</term><term>Crystallization mechanism</term><term>Crystallization process</term><term>Crystallization rate</term><term>Exothermic peak</term><term>Gaussian functions</term><term>Ges2</term><term>Ges2 crystals</term><term>Ges2 phase</term><term>Glass ceramics</term><term>Glass formation</term><term>Glass matrix</term><term>Glass network</term><term>Glasses ceramics</term><term>Glasses heattreated</term><term>Glassy matrix</term><term>Heating rate</term><term>Heating rates</term><term>Jcpds card</term><term>Kinetic parameters</term><term>Matrix</term><term>Mechanical properties</term><term>Metallic halide</term><term>Natural science foundation</term><term>Ningbo</term><term>Ningbo city</term><term>Ningbo university</term><term>Optical properties</term><term>Raman</term><term>Raman spectra</term><term>Room temperature</term><term>Several peaks</term><term>Spectral region</term><term>Thermal imaging</term><term>Total crystallization</term><term>Transmission spectra</term><term>Zhang</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract">54GeS2–36Sb2S3–10In2S3 glass‐ceramics were prepared by heat‐treating the base glass above Tg for different durations. The results of Raman spectra and XRD patterns show that the first precipitated crystals during the heat treatment are In2S3 and the crystallization of the Sb2S3 and GeS2 subsequently occurs. Bulk samples heat‐treated at 295°C for different heating rates and durations are used to study the crystallization mechanism and evolution of the three crystallization peaks (CPs). It is found that three CPs partly overlap with each other and then separate with increasing heat‐treating durations.</div></front></TEI><istex><corpusName>wiley</corpusName><editor><json:item><name>J. 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The results of Raman spectra and XRD patterns show that the first precipitated crystals during the heat treatment are In2S3 and the crystallization of the Sb2S3 and GeS2 subsequently occurs. Bulk samples heat‐treated at 295°C for different heating rates and durations are used to study the crystallization mechanism and evolution of the three crystallization peaks (CPs). It is found that three CPs partly overlap with each other and then separate with increasing heat‐treating durations.</abstract><qualityIndicators><score>4.615</score><pdfVersion>1.3</pdfVersion><pdfPageSize>595.276 x 782.362 pts</pdfPageSize><refBibsNative>true</refBibsNative><abstractCharCount>606</abstractCharCount><pdfWordCount>3559</pdfWordCount><pdfCharCount>22137</pdfCharCount><pdfPageCount>6</pdfPageCount><abstractWordCount>88</abstractWordCount></qualityIndicators><title>Mechanical Properties and Crystallization Behavior of GeS2–Sb2S3–In2S3 Chalcogenide Glass</title><genre><json:string>article</json:string></genre><host><title>Journal of the American Ceramic Society</title><language><json:string>unknown</json:string></language><doi><json:string>10.1111/(ISSN)1551-2916</json:string></doi><issn><json:string>0002-7820</json:string></issn><eissn><json:string>1551-2916</json:string></eissn><publisherId><json:string>JACE</json:string></publisherId><volume>95</volume><issue>4</issue><pages><first>1320</first><last>1325</last><total>6</total></pages><genre><json:string>journal</json:string></genre><subject><json:item><value>Article</value></json:item></subject></host><categories><wos><json:string>science</json:string><json:string>materials science, ceramics</json:string></wos><scienceMetrix><json:string>applied sciences</json:string><json:string>enabling & strategic technologies</json:string><json:string>materials</json:string></scienceMetrix></categories><publicationDate>2012</publicationDate><copyrightDate>2012</copyrightDate><doi><json:string>10.1111/j.1551-2916.2012.05117.x</json:string></doi><id>DF0BB478205AFDACB615A4DA6FC69D51CAF57AE9</id><score>1</score><fulltext><json:item><extension>pdf</extension><original>true</original><mimetype>application/pdf</mimetype><uri>https://api.istex.fr/document/DF0BB478205AFDACB615A4DA6FC69D51CAF57AE9/fulltext/pdf</uri></json:item><json:item><extension>zip</extension><original>false</original><mimetype>application/zip</mimetype><uri>https://api.istex.fr/document/DF0BB478205AFDACB615A4DA6FC69D51CAF57AE9/fulltext/zip</uri></json:item><istex:fulltextTEI uri="https://api.istex.fr/document/DF0BB478205AFDACB615A4DA6FC69D51CAF57AE9/fulltext/tei"><teiHeader><fileDesc><titleStmt><title level="a" type="main">Mechanical Properties and Crystallization Behavior of <hi rend="fc"><hi rend="fr">GeS</hi></hi><hi rend="subscript">2</hi>–<hi rend="fc"><hi rend="fr">Sb</hi></hi><hi rend="subscript">2</hi><hi rend="fc"><hi rend="fr">S</hi></hi><hi rend="subscript">3</hi>–<hi rend="fc"><hi rend="fr">In</hi></hi><hi rend="subscript">2</hi><hi rend="fc"><hi rend="fr">S</hi></hi><hi rend="subscript">3</hi> Chalcogenide Glass</title></titleStmt><publicationStmt><authority>ISTEX</authority><publisher>Wiley Publishing Ltd</publisher><availability><licence>© 2012 The American Ceramic Society</licence></availability><date type="published" when="2012-04"></date></publicationStmt><notesStmt><note type="content-type" subtype="article" source="article" scheme="https://content-type.data.istex.fr/ark:/67375/XTP-6N5SZHKN-D">article</note><note type="publication-type" subtype="journal" scheme="https://publication-type.data.istex.fr/ark:/67375/JMC-0GLKJH51-B">journal</note></notesStmt><sourceDesc><biblStruct type="article"><analytic><title level="a" type="main">Mechanical Properties and Crystallization Behavior of <hi rend="fc"><hi rend="fr">GeS</hi></hi><hi rend="subscript">2</hi>–<hi rend="fc"><hi rend="fr">Sb</hi></hi><hi rend="subscript">2</hi><hi rend="fc"><hi rend="fr">S</hi></hi><hi rend="subscript">3</hi>–<hi rend="fc"><hi rend="fr">In</hi></hi><hi rend="subscript">2</hi><hi rend="fc"><hi rend="fr">S</hi></hi><hi rend="subscript">3</hi> Chalcogenide Glass</title><author xml:id="author-0000"><persName><forename type="first">Lei</forename><surname>Ying</surname></persName><affiliation><orgName>The School of Information Science and Engineering</orgName><orgName>Ningbo University</orgName><address><settlement type="city">Ningbo</settlement><postCode>315211</postCode><country key="CN">China</country></address></affiliation></author><author xml:id="author-0001" role="corresp"><persName><forename type="first">Changgui</forename><surname>Lin</surname></persName><affiliation><orgName>The School of Materials Science and Chemical Engineering</orgName><orgName>Ningbo University</orgName><address><settlement type="city">Ningbo</settlement><region>315211</region><country key="CN">China</country></address></affiliation><affiliation>Authors to whom correspondence should be addressed. e‐mails: linchanggui@nbu.edu.cn and daishixun@nbu.edu.cn</affiliation></author><author xml:id="author-0002"><persName><forename type="first">Qiuhua</forename><surname>Nie</surname></persName><affiliation><orgName>The School of Information Science and Engineering</orgName><orgName>Ningbo University</orgName><address><settlement type="city">Ningbo</settlement><postCode>315211</postCode><country key="CN">China</country></address></affiliation></author><author xml:id="author-0003"><persName><forename type="first">Zhuobin</forename><surname>Li</surname></persName><affiliation><orgName>The School of Information Science and Engineering</orgName><orgName>Ningbo University</orgName><address><settlement type="city">Ningbo</settlement><postCode>315211</postCode><country key="CN">China</country></address></affiliation></author><author xml:id="author-0004"><persName><forename type="first">Yinsheng</forename><surname>Xu</surname></persName><affiliation><orgName>The School of Materials Science and Chemical Engineering</orgName><orgName>Ningbo University</orgName><address><settlement type="city">Ningbo</settlement><region>315211</region><country key="CN">China</country></address></affiliation></author><author xml:id="author-0005"><persName><forename type="first">Feifei</forename><surname>Chen</surname></persName><affiliation><orgName>The School of Information Science and Engineering</orgName><orgName>Ningbo University</orgName><address><settlement type="city">Ningbo</settlement><postCode>315211</postCode><country key="CN">China</country></address></affiliation></author><author xml:id="author-0006" role="corresp"><persName><forename type="first">Shixun</forename><surname>Dai</surname></persName><affiliation><orgName>The School of Information Science and Engineering</orgName><orgName>Ningbo University</orgName><address><settlement type="city">Ningbo</settlement><postCode>315211</postCode><country key="CN">China</country></address></affiliation><affiliation>Authors to whom correspondence should be addressed. e‐mails: linchanggui@nbu.edu.cn and daishixun@nbu.edu.cn</affiliation></author><editor xml:id="editor-0007"><persName><forename type="first">J.</forename><surname>Heo</surname></persName></editor><idno type="istex">DF0BB478205AFDACB615A4DA6FC69D51CAF57AE9</idno><idno type="ark">ark:/67375/WNG-KV7VDL9P-K</idno><idno type="DOI">10.1111/j.1551-2916.2012.05117.x</idno><idno type="unit">JACE5117</idno><idno type="toTypesetVersion">file:JACE.JACE5117.pdf</idno></analytic><monogr><title level="j" type="main">Journal of the American Ceramic Society</title><title level="j" type="alt">JOURNAL OF THE AMERICAN CERAMIC SOCIETY</title><idno type="pISSN">0002-7820</idno><idno type="eISSN">1551-2916</idno><idno type="book-DOI">10.1111/(ISSN)1551-2916</idno><idno type="book-part-DOI">10.1111/jace.2012.95.issue-4</idno><idno type="product">JACE</idno><imprint><biblScope unit="vol">95</biblScope><biblScope unit="issue">4</biblScope><biblScope unit="page" from="1320">1320</biblScope><biblScope unit="page" to="1325">1325</biblScope><biblScope unit="page-count">6</biblScope><date type="published" when="2012-04"></date></imprint></monogr></biblStruct></sourceDesc></fileDesc><profileDesc><abstract style="main" xml:id="jace5117-abs-0001"><p>54<hi rend="fc"><hi rend="fr">GeS</hi></hi><hi rend="subscript">2</hi>–36<hi rend="fc"><hi rend="fr">Sb</hi></hi><hi rend="subscript">2</hi><hi rend="fc"><hi rend="fr">S</hi></hi><hi rend="subscript">3</hi>–10<hi rend="fc"><hi rend="fr">In</hi></hi><hi rend="subscript">2</hi><hi rend="fc"><hi rend="fr">S</hi></hi><hi rend="subscript">3</hi> glass‐ceramics were prepared by heat‐treating the base glass above <hi rend="fc"><hi rend="fi">T<hi rend="subscript">g</hi></hi></hi> for different durations. The results of Raman spectra and <hi rend="fc">XRD</hi> patterns show that the first precipitated crystals during the heat treatment are <hi rend="fc"><hi rend="fr">In</hi></hi><hi rend="subscript">2</hi><hi rend="fc"><hi rend="fr">S</hi></hi><hi rend="subscript">3</hi> and the crystallization of the <hi rend="fc"><hi rend="fr">Sb</hi></hi><hi rend="subscript">2</hi><hi rend="fc"><hi rend="fr">S</hi></hi><hi rend="subscript">3</hi> and <hi rend="fc"><hi rend="fr">GeS</hi></hi><hi rend="subscript">2</hi> subsequently occurs. Bulk samples heat‐treated at 295°C for different heating rates and durations are used to study the crystallization mechanism and evolution of the three crystallization peaks (CPs). It is found that three CPs partly overlap with each other and then separate with increasing heat‐treating durations.</p></abstract><textClass><keywords rend="articleCategory"><term>Article</term></keywords><keywords rend="tocHeading1"><term>Articles</term></keywords><keywords rend="tocHeading2"><term>Glass Science</term></keywords></textClass><langUsage><language ident="en"></language></langUsage></profileDesc></teiHeader></istex:fulltextTEI><json:item><extension>txt</extension><original>false</original><mimetype>text/plain</mimetype><uri>https://api.istex.fr/document/DF0BB478205AFDACB615A4DA6FC69D51CAF57AE9/fulltext/txt</uri></json:item></fulltext><metadata><istex:metadataXml wicri:clean="Wiley, elements deleted: body"><istex:xmlDeclaration>version="1.0" encoding="UTF-8" standalone="yes"</istex:xmlDeclaration><istex:document><component type="serialArticle" version="2.0" xml:id="jace5117" xml:lang="en"><header><publicationMeta level="product"><doi origin="wiley" registered="yes">10.1111/(ISSN)1551-2916</doi><issn type="print">0002-7820</issn><issn type="electronic">1551-2916</issn><idGroup><id type="product" value="JACE"></id></idGroup><titleGroup><title sort="JOURNAL OF THE AMERICAN CERAMIC SOCIETY" type="main">Journal of the American Ceramic Society</title><title type="short">J. Am. Ceram. Soc.</title></titleGroup></publicationMeta><publicationMeta level="part" position="04104"><doi origin="wiley">10.1111/jace.2012.95.issue-4</doi><copyright ownership="thirdParty">© 2012 American Ceramic Society</copyright><numberingGroup><numbering type="journalVolume" number="95">95</numbering><numbering type="journalIssue">4</numbering></numberingGroup><coverDate startDate="2012-04">April 2012</coverDate></publicationMeta><publicationMeta level="unit" position="310" status="forIssue" type="article"><doi>10.1111/j.1551-2916.2012.05117.x</doi><idGroup><id type="unit" value="JACE5117"></id></idGroup><countGroup><count number="6" type="pageTotal"></count></countGroup><titleGroup><title type="articleCategory">Article</title><title type="tocHeading1">Articles</title><title type="tocHeading2"><i>Glass Science</i></title></titleGroup><copyright ownership="thirdParty">© 2012 The American Ceramic Society</copyright><eventGroup><event date="2011-08-21" type="manuscriptReceived"></event><event date="2012-01-18" type="manuscriptAccepted"></event><event agent="SPS" date="2012-02-03" type="xmlCreated"></event><event type="publishedOnlineEarlyUnpaginated" date="2012-03-01"></event><event type="publishedOnlineFinalForm" date="2012-04-04"></event><event type="firstOnline" date="2012-03-01"></event><event type="xmlConverted" agent="Converter:WILEY_ML3G_TO_WILEY_ML3GV2 version:4.0.1" date="2014-03-19"></event><event type="xmlConverted" agent="Converter:WML3G_To_WML3G version:4.3.4 mode:FullText" date="2015-02-25"></event></eventGroup><numberingGroup><numbering type="pageFirst">1320</numbering><numbering type="pageLast">1325</numbering></numberingGroup><correspondenceTo>Authors to whom correspondence should be addressed. e‐mails: <email>linchanggui@nbu.edu.cn</email> and <email>daishixun@nbu.edu.cn</email></correspondenceTo><linkGroup><link type="toTypesetVersion" href="file:JACE.JACE5117.pdf"></link></linkGroup></publicationMeta><contentMeta><titleGroup><title type="main">Mechanical Properties and Crystallization Behavior of <fc><fr>GeS</fr></fc><sub>2</sub>–<fc><fr>Sb</fr></fc><sub>2</sub><fc><fr>S</fr></fc><sub>3</sub>–<fc><fr>In</fr></fc><sub>2</sub><fc><fr>S</fr></fc><sub>3</sub> Chalcogenide Glass</title><title type="shortAuthors">Ying <i>et al</i>.</title></titleGroup><creators><creator affiliationRef="#jace5117-aff-0001" creatorRole="author" xml:id="jace5117-cr-0001"><personName><givenNames>Lei</givenNames> <familyName>Ying</familyName></personName></creator><creator affiliationRef="#jace5117-aff-0002" corresponding="yes" creatorRole="author" xml:id="jace5117-cr-0002"><personName><givenNames>Changgui</givenNames> <familyName>Lin</familyName></personName></creator><creator affiliationRef="#jace5117-aff-0001" creatorRole="author" xml:id="jace5117-cr-0003"><personName><givenNames>Qiuhua</givenNames> <familyName>Nie</familyName></personName></creator><creator affiliationRef="#jace5117-aff-0001" creatorRole="author" xml:id="jace5117-cr-0004"><personName><givenNames>Zhuobin</givenNames> <familyName>Li</familyName></personName></creator><creator affiliationRef="#jace5117-aff-0002" creatorRole="author" xml:id="jace5117-cr-0005"><personName><givenNames>Yinsheng</givenNames> <familyName>Xu</familyName></personName></creator><creator affiliationRef="#jace5117-aff-0001" creatorRole="author" xml:id="jace5117-cr-0006"><personName><givenNames>Feifei</givenNames> <familyName>Chen</familyName></personName></creator><creator affiliationRef="#jace5117-aff-0001" corresponding="yes" creatorRole="author" xml:id="jace5117-cr-0007"><personName><givenNames>Shixun</givenNames> <familyName>Dai</familyName></personName></creator><creator creatorRole="editor" xml:id="jace5117-cr-0008"><personName><givenNames>J.</givenNames> <familyName>Heo</familyName></personName></creator></creators><affiliationGroup><affiliation countryCode="CN" type="organization" xml:id="jace5117-aff-0001"><orgDiv>The School of Information Science and Engineering</orgDiv> <orgName>Ningbo University</orgName> <address><city>Ningbo</city> <postCode>315211</postCode> <country>China</country></address></affiliation><affiliation countryCode="CN" type="organization" xml:id="jace5117-aff-0002"><orgDiv>The School of Materials Science and Chemical Engineering</orgDiv> <orgName>Ningbo University</orgName> <address><city>Ningbo</city> <countryPart>315211</countryPart> <country>China</country></address></affiliation></affiliationGroup><fundingInfo><fundingAgency>Natural Science Foundation of China</fundingAgency><fundingNumber>61108057</fundingNumber></fundingInfo><fundingInfo><fundingAgency>Zhejiang Provincial Natural Science Foundation of China</fundingAgency><fundingNumber>R1101263</fundingNumber><fundingNumber>Y4110322</fundingNumber></fundingInfo><fundingInfo><fundingAgency>Program for Innovative Research Team in Ningbo City</fundingAgency><fundingNumber>2009B21007</fundingNumber></fundingInfo><fundingInfo><fundingAgency>Natural Science Foundation of Ningbo City</fundingAgency><fundingNumber>2011A610091</fundingNumber></fundingInfo><fundingInfo><fundingAgency>Program for New Century Excellent Talents in University</fundingAgency><fundingNumber>NCET‐10‐0976</fundingNumber></fundingInfo><fundingInfo><fundingAgency>Dissertation Engagement Foundation of Graduate School of Ningbo University</fundingAgency><fundingNumber>PY20100010</fundingNumber></fundingInfo><abstractGroup><abstract type="main" xml:id="jace5117-abs-0001"><p>54<fc><fr>GeS</fr></fc><sub>2</sub>–36<fc><fr>Sb</fr></fc><sub>2</sub><fc><fr>S</fr></fc><sub>3</sub>–10<fc><fr>In</fr></fc><sub>2</sub><fc><fr>S</fr></fc><sub>3</sub> glass‐ceramics were prepared by heat‐treating the base glass above <fc><fi>T<sub>g</sub></fi></fc> for different durations. The results of Raman spectra and <fc>XRD</fc> patterns show that the first precipitated crystals during the heat treatment are <fc><fr>In</fr></fc><sub>2</sub><fc><fr>S</fr></fc><sub>3</sub> and the crystallization of the <fc><fr>Sb</fr></fc><sub>2</sub><fc><fr>S</fr></fc><sub>3</sub> and <fc><fr>GeS</fr></fc><sub>2</sub> subsequently occurs. Bulk samples heat‐treated at 295°C for different heating rates and durations are used to study the crystallization mechanism and evolution of the three crystallization peaks (CPs). It is found that three CPs partly overlap with each other and then separate with increasing heat‐treating durations.</p></abstract></abstractGroup></contentMeta></header></component></istex:document></istex:metadataXml><mods version="3.6"><titleInfo lang="en"><title>Mechanical Properties and Crystallization Behavior of GeS2–Sb2S3–In2S3 Chalcogenide Glass</title></titleInfo><titleInfo type="alternative" contentType="CDATA" lang="en"><title>Mechanical Properties and Crystallization Behavior of GeS2–Sb2S3–In2S3 Chalcogenide Glass</title></titleInfo><name type="personal"><namePart type="given">Lei</namePart><namePart type="family">Ying</namePart><affiliation>The School of Information Science and Engineering, Ningbo University, 315211, Ningbo, China</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Changgui</namePart><namePart type="family">Lin</namePart><affiliation>The School of Materials Science and Chemical Engineering, Ningbo University, 315211, Ningbo, China</affiliation><affiliation>E-mail: linchanggui@nbu.edu.cn</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Qiuhua</namePart><namePart type="family">Nie</namePart><affiliation>The School of Information Science and Engineering, Ningbo University, 315211, Ningbo, China</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Zhuobin</namePart><namePart type="family">Li</namePart><affiliation>The School of Information Science and Engineering, Ningbo University, 315211, Ningbo, China</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Yinsheng</namePart><namePart type="family">Xu</namePart><affiliation>The School of Materials Science and Chemical Engineering, Ningbo University, 315211, Ningbo, China</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Feifei</namePart><namePart type="family">Chen</namePart><affiliation>The School of Information Science and Engineering, Ningbo University, 315211, Ningbo, China</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Shixun</namePart><namePart type="family">Dai</namePart><affiliation>The School of Information Science and Engineering, Ningbo University, 315211, Ningbo, China</affiliation><affiliation>E-mail: linchanggui@nbu.edu.cn</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">J.</namePart><namePart type="family">Heo</namePart><role><roleTerm type="text">editor</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="article" displayLabel="article" authority="ISTEX" authorityURI="https://content-type.data.istex.fr" valueURI="https://content-type.data.istex.fr/ark:/67375/XTP-6N5SZHKN-D">article</genre><originInfo><publisher>Blackwell Publishing Ltd</publisher><dateIssued encoding="w3cdtf">2012-04</dateIssued><dateCreated encoding="w3cdtf">2012-02-03</dateCreated><dateCaptured encoding="w3cdtf">2011-08-21</dateCaptured><dateValid encoding="w3cdtf">2012-01-18</dateValid><copyrightDate encoding="w3cdtf">2012</copyrightDate></originInfo><language><languageTerm type="code" authority="rfc3066">en</languageTerm><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><abstract>54GeS2–36Sb2S3–10In2S3 glass‐ceramics were prepared by heat‐treating the base glass above Tg for different durations. The results of Raman spectra and XRD patterns show that the first precipitated crystals during the heat treatment are In2S3 and the crystallization of the Sb2S3 and GeS2 subsequently occurs. Bulk samples heat‐treated at 295°C for different heating rates and durations are used to study the crystallization mechanism and evolution of the three crystallization peaks (CPs). It is found that three CPs partly overlap with each other and then separate with increasing heat‐treating durations.</abstract><note type="funding">Natural Science Foundation of China - No. 61108057; </note><note type="funding">Zhejiang Provincial Natural Science Foundation of China - No. R1101263; No. Y4110322; </note><note type="funding">Program for Innovative Research Team in Ningbo City - No. 2009B21007; </note><note type="funding">Natural Science Foundation of Ningbo City - No. 2011A610091; </note><note type="funding">Program for New Century Excellent Talents in University - No. NCET‐10‐0976; </note><note type="funding">Dissertation Engagement Foundation of Graduate School of Ningbo University - No. PY20100010; </note><relatedItem type="host"><titleInfo><title>Journal of the American Ceramic Society</title></titleInfo><titleInfo type="abbreviated"><title>J. Am. Ceram. Soc.</title></titleInfo><genre type="journal" authority="ISTEX" authorityURI="https://publication-type.data.istex.fr" valueURI="https://publication-type.data.istex.fr/ark:/67375/JMC-0GLKJH51-B">journal</genre><subject><genre>article-category</genre><topic>Article</topic></subject><identifier type="ISSN">0002-7820</identifier><identifier type="eISSN">1551-2916</identifier><identifier type="DOI">10.1111/(ISSN)1551-2916</identifier><identifier type="PublisherID">JACE</identifier><part><date>2012</date><detail type="volume"><caption>vol.</caption><number>95</number></detail><detail type="issue"><caption>no.</caption><number>4</number></detail><extent unit="pages"><start>1320</start><end>1325</end><total>6</total></extent></part></relatedItem><identifier type="istex">DF0BB478205AFDACB615A4DA6FC69D51CAF57AE9</identifier><identifier type="ark">ark:/67375/WNG-KV7VDL9P-K</identifier><identifier type="DOI">10.1111/j.1551-2916.2012.05117.x</identifier><identifier type="ArticleID">JACE5117</identifier><accessCondition type="use and reproduction" contentType="copyright">© 2012 American Ceramic Society© 2012 The American Ceramic Society</accessCondition><recordInfo><recordContentSource authority="ISTEX" authorityURI="https://loaded-corpus.data.istex.fr" valueURI="https://loaded-corpus.data.istex.fr/ark:/67375/XBH-L0C46X92-X">wiley</recordContentSource></recordInfo></mods><json:item><extension>json</extension><original>false</original><mimetype>application/json</mimetype><uri>https://api.istex.fr/document/DF0BB478205AFDACB615A4DA6FC69D51CAF57AE9/metadata/json</uri></json:item></metadata><serie></serie></istex></record>Pour manipuler ce document sous Unix (Dilib)
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