Poly[aqua(μ3‐benzene‐1,2‐dicarboxylato)bis(μ3‐hydroxido)bis(μ2‐isonicotinato)dierbium(III) monohydrate] and the thulium analogue
Identifieur interne : 002957 ( Istex/Corpus ); précédent : 002956; suivant : 002958Poly[aqua(μ3‐benzene‐1,2‐dicarboxylato)bis(μ3‐hydroxido)bis(μ2‐isonicotinato)dierbium(III) monohydrate] and the thulium analogue
Auteurs : Guo-Ming Wang ; Hai-Lan Huang ; Hui Li ; Qing-Hua ZhengSource :
- Acta Crystallographica Section C [ 0108-2701 ] ; 2007-11.
English descriptors
- KwdEn :
- Acta, Acta cryst, Adjacent chains, Aqua ligand, Bond lengths, Bruker, Carboxylate, Chem, Coordination polymers, Cryst, Crystal structures, Data collection siemems, Different coordination environments, Diffractometer absorption correction, Eddaoudi, Hydrogen bonds, Inorg, Intensity measurements, Ligand, Parameters parameters, Polymer, Sheldrick, Symmetry codes, Title compounds, Tmin tmax, Wang, Zhang.
- Teeft :
- Acta, Acta cryst, Adjacent chains, Aqua ligand, Bond lengths, Bruker, Carboxylate, Chem, Coordination polymers, Cryst, Crystal structures, Data collection siemems, Different coordination environments, Diffractometer absorption correction, Eddaoudi, Hydrogen bonds, Inorg, Intensity measurements, Ligand, Parameters parameters, Polymer, Sheldrick, Symmetry codes, Title compounds, Tmin tmax, Wang, Zhang.
Abstract
The two isomorphous lanthanide coordination polymers, {[Ln2(C6H4NO2)2(C8H4O4)(OH)2(H2O)]·H2O}n (Ln = Er and Tm), contain two crystallographically independent Ln ions which are both eight‐coordinated by O atoms, but with quite different coordination environments. In both crystal structures, adjacent Ln atoms are bridged by μ3‐OH groups and carboxylate groups of isonicotinate and benzene‐1,2‐dicarboxylate ligands, forming infinite chains in which the Er...Er and Tm...Tm distances are in the ranges 3.622 (3)–3.894 (4) and 3.599 (7)–3.873 (1) Å, respectively. Adjacent chains are further connected through hydrogen bonds and π–π interactions into a three‐dimensional supramolecular framework.
Url:
DOI: 10.1107/S0108270107047403
Links to Exploration step
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<front><div type="abstract" xml:lang="en">The two isomorphous lanthanide coordination polymers, {[Ln2(C6H4NO2)2(C8H4O4)(OH)2(H2O)]·H2O}n (Ln = Er and Tm), contain two crystallographically independent Ln ions which are both eight‐coordinated by O atoms, but with quite different coordination environments. In both crystal structures, adjacent Ln atoms are bridged by μ3‐OH groups and carboxylate groups of isonicotinate and benzene‐1,2‐dicarboxylate ligands, forming infinite chains in which the Er...Er and Tm...Tm distances are in the ranges 3.622 (3)–3.894 (4) and 3.599 (7)–3.873 (1) Å, respectively. Adjacent chains are further connected through hydrogen bonds and π–π interactions into a three‐dimensional supramolecular framework.</div>
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<title level="a" type="short">[Er2(C6H4NO2)2(C8H4O4)(OH)2(H2O)]·H2O and [Tm2(C6H4NO2)2(C8H4O4)(OH)2(H2O)]·H2O</title>
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<profileDesc><abstract xml:lang="en" style="main"><p>The two isomorphous lanthanide coordination polymers, {[Ln<hi rend="subscript">2</hi>
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<titleGroup><title type="main">Poly[aqua(μ<sub>3</sub>
‐benzene‐1,2‐dicarboxylato)bis(μ<sub>3</sub>
‐hydroxido)bis(μ<sub>2</sub>
‐isonicotinato)dierbium(III) monohydrate] and the thulium analogue</title>
<title type="shortAuthors">Wang <i>et al.</i>
</title>
<title type="short">[Er<sub>2</sub>
(C<sub>6</sub>
H<sub>4</sub>
NO<sub>2</sub>
)<sub>2</sub>
(C<sub>8</sub>
H<sub>4</sub>
O<sub>4</sub>
)(OH)<sub>2</sub>
(H<sub>2</sub>
O)]·H<sub>2</sub>
O and [Tm<sub>2</sub>
(C<sub>6</sub>
H<sub>4</sub>
NO<sub>2</sub>
)<sub>2</sub>
(C<sub>8</sub>
H<sub>4</sub>
O<sub>4</sub>
)(OH)<sub>2</sub>
(H<sub>2</sub>
O)]·H<sub>2</sub>
O</title>
</titleGroup>
<creators><creator creatorRole="author" xml:id="cr1" affiliationRef="#a1"><personName><givenNames>Guo‐Ming</givenNames>
<familyName>Wang</familyName>
</personName>
</creator>
<creator creatorRole="author" xml:id="cr2" affiliationRef="#a1"><personName><givenNames>Hai‐Lan</givenNames>
<familyName>Huang</familyName>
</personName>
</creator>
<creator creatorRole="author" xml:id="cr3" affiliationRef="#a1"><personName><givenNames>Hui</givenNames>
<familyName>Li</familyName>
</personName>
</creator>
<creator creatorRole="author" xml:id="cr4" affiliationRef="#a1"><personName><givenNames>Qing‐Hua</givenNames>
<familyName>Zheng</familyName>
</personName>
</creator>
</creators>
<affiliationGroup><affiliation xml:id="a1" countryCode="CN"><unparsedAffiliation>Department of Chemistry, Teachers' College of Qingdao University, Qingdao, Shandong 266071, People's Republic of China</unparsedAffiliation>
</affiliation>
</affiliationGroup>
<abstractGroup><abstract type="main" xml:lang="en"><p>The two isomorphous lanthanide coordination polymers, {[Ln<sub>2</sub>
(C<sub>6</sub>
H<sub>4</sub>
NO<sub>2</sub>
)<sub>2</sub>
(C<sub>8</sub>
H<sub>4</sub>
O<sub>4</sub>
)(OH)<sub>2</sub>
(H<sub>2</sub>
O)]·H<sub>2</sub>
O}<sub><i>n</i>
</sub>
(Ln = Er and Tm), contain two crystallographically independent Ln ions which are both eight‐coordinated by O atoms, but with quite different coordination environments. In both crystal structures, adjacent Ln atoms are bridged by μ<sub>3</sub>
‐OH groups and carboxylate groups of isonicotinate and benzene‐1,2‐dicarboxylate ligands, forming infinite chains in which the Er...Er and Tm...Tm distances are in the ranges 3.622 (3)–3.894 (4) and 3.599 (7)–3.873 (1) Å, respectively. Adjacent chains are further connected through hydrogen bonds and π–π interactions into a three‐dimensional supramolecular framework.</p>
</abstract>
</abstractGroup>
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<mods version="3.6"><titleInfo lang="en"><title>Poly[aqua(μ3‐benzene‐1,2‐dicarboxylato)bis(μ3‐hydroxido)bis(μ2‐isonicotinato)dierbium(III) monohydrate] and the thulium analogue</title>
</titleInfo>
<titleInfo type="abbreviated" lang="en"><title>[Er2(C6H4NO2)2(C8H4O4)(OH)2(H2O)]·H2O and [Tm2(C6H4NO2)2(C8H4O4)(OH)2(H2O)]·H2O</title>
</titleInfo>
<titleInfo type="alternative" contentType="CDATA" lang="en"><title>Poly[aqua(μ3‐benzene‐1,2‐dicarboxylato)bis(μ3‐hydroxido)bis(μ2‐isonicotinato)dierbium(III) monohydrate] and the thulium analogue</title>
</titleInfo>
<name type="personal"><namePart type="given">Guo‐Ming</namePart>
<namePart type="family">Wang</namePart>
<affiliation>Department of Chemistry, Teachers' College of Qingdao University, Qingdao, Shandong 266071, People's Republic of China</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">Hai‐Lan</namePart>
<namePart type="family">Huang</namePart>
<affiliation>Department of Chemistry, Teachers' College of Qingdao University, Qingdao, Shandong 266071, People's Republic of China</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">Hui</namePart>
<namePart type="family">Li</namePart>
<affiliation>Department of Chemistry, Teachers' College of Qingdao University, Qingdao, Shandong 266071, People's Republic of China</affiliation>
<role><roleTerm type="text">author</roleTerm>
</role>
</name>
<name type="personal"><namePart type="given">Qing‐Hua</namePart>
<namePart type="family">Zheng</namePart>
<affiliation>Department of Chemistry, Teachers' College of Qingdao University, Qingdao, Shandong 266071, People's Republic of China</affiliation>
<role><roleTerm type="text">author</roleTerm>
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<place><placeTerm type="text">5 Abbey Square, Chester, Cheshire CH1 2HU, England</placeTerm>
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<dateIssued encoding="w3cdtf">2007-11</dateIssued>
<edition>Received 5 September 2007, accepted 26 September 2007</edition>
<copyrightDate encoding="w3cdtf">2007</copyrightDate>
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<abstract lang="en">The two isomorphous lanthanide coordination polymers, {[Ln2(C6H4NO2)2(C8H4O4)(OH)2(H2O)]·H2O}n (Ln = Er and Tm), contain two crystallographically independent Ln ions which are both eight‐coordinated by O atoms, but with quite different coordination environments. In both crystal structures, adjacent Ln atoms are bridged by μ3‐OH groups and carboxylate groups of isonicotinate and benzene‐1,2‐dicarboxylate ligands, forming infinite chains in which the Er...Er and Tm...Tm distances are in the ranges 3.622 (3)–3.894 (4) and 3.599 (7)–3.873 (1) Å, respectively. Adjacent chains are further connected through hydrogen bonds and π–π interactions into a three‐dimensional supramolecular framework.</abstract>
<relatedItem type="host"><titleInfo><title>Acta Crystallographica Section C</title>
</titleInfo>
<titleInfo type="abbreviated"><title>Acta Cryst. C</title>
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<genre type="journal" authority="ISTEX" authorityURI="https://publication-type.data.istex.fr" valueURI="https://publication-type.data.istex.fr/ark:/67375/JMC-0GLKJH51-B">journal</genre>
<identifier type="ISSN">0108-2701</identifier>
<identifier type="eISSN">1600-5759</identifier>
<identifier type="DOI">10.1111/(ISSN)1600-5759</identifier>
<identifier type="PublisherID">AYC</identifier>
<part><date>2007</date>
<detail type="volume"><caption>vol.</caption>
<number>63</number>
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<detail type="issue"><caption>no.</caption>
<number>11</number>
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