Polymorphism under pressure of the disilicates of the heavier lanthanoids Ln 2Si2O7 ( Ln = Tm, Yb, Lu)
Identifieur interne : 002711 ( Istex/Corpus ); précédent : 002710; suivant : 002712Polymorphism under pressure of the disilicates of the heavier lanthanoids Ln 2Si2O7 ( Ln = Tm, Yb, Lu)
Auteurs : G. Bocquillon ; C. Chateau ; C. Loriers ; J. LoriersSource :
- Journal of Solid State Chemistry [ 0022-4596 ] ; 1977.
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- KwdEn :
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Abstract
Abstract: A study of the phase diagram of thulium, ytterbium, and lutecium disilicates Ln2Si2O7 in the ranges 0–70 kbar and 20–1600°C shows the extended polymorphism under high pressure of these compounds of which only one form was previously known at ambient pressure. The monoclinic D form appears at temperatures much lower than for the neighboring members of the series and its stability field is restricted to a rather narrow pressure interval around 20 kbar. The triclinic B form appears at pressures which increase from 20 to 40 kbar from Tm to Lu. A new tetragonal X form so far unknown in the disilicate series and isostructural with Er2Ge2O7 is obtained for the three compounds. Compared to the B form it is a low temperature, low pressure form. The crystal data of the nine high pressure phases are given.
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DOI: 10.1016/0022-4596(77)90060-3
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<front><div type="abstract" xml:lang="en">Abstract: A study of the phase diagram of thulium, ytterbium, and lutecium disilicates Ln2Si2O7 in the ranges 0–70 kbar and 20–1600°C shows the extended polymorphism under high pressure of these compounds of which only one form was previously known at ambient pressure. The monoclinic D form appears at temperatures much lower than for the neighboring members of the series and its stability field is restricted to a rather narrow pressure interval around 20 kbar. The triclinic B form appears at pressures which increase from 20 to 40 kbar from Tm to Lu. A new tetragonal X form so far unknown in the disilicate series and isostructural with Er2Ge2O7 is obtained for the three compounds. Compared to the B form it is a low temperature, low pressure form. The crystal data of the nine high pressure phases are given.</div>
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<abstract lang="en">Abstract: A study of the phase diagram of thulium, ytterbium, and lutecium disilicates Ln2Si2O7 in the ranges 0–70 kbar and 20–1600°C shows the extended polymorphism under high pressure of these compounds of which only one form was previously known at ambient pressure. The monoclinic D form appears at temperatures much lower than for the neighboring members of the series and its stability field is restricted to a rather narrow pressure interval around 20 kbar. The triclinic B form appears at pressures which increase from 20 to 40 kbar from Tm to Lu. A new tetragonal X form so far unknown in the disilicate series and isostructural with Er2Ge2O7 is obtained for the three compounds. Compared to the B form it is a low temperature, low pressure form. The crystal data of the nine high pressure phases are given.</abstract>
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