The Tb2(Cu0.47Al0.53)17 and Tb(Cu0.58Al0.42)11 aluminides and their crystal structures
Identifieur interne : 000016 ( Istex/Corpus ); précédent : 000015; suivant : 000017The Tb2(Cu0.47Al0.53)17 and Tb(Cu0.58Al0.42)11 aluminides and their crystal structures
Auteurs : B. M. Stel'Makhovych ; L. G. Aksel'Rud ; Yu. B. Kuz'MaSource :
- Journal of Alloys and Compounds [ 0925-8388 ] ; 1996.
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Abstract
Abstract: The crystal structure of the new compound Tb2(Cu0.47Al0.53)17 with Th2Zn17-type structure (space group R3m, a = 8.767(3), c = 12.824(3)Å) has been determined using single crystal X-ray diffraction leading to R = 0.036 for 407 independent Fhkl values. The crystal structure of Tb(Cu0.58Al0.42)11 has been established from X-ray powder data with atomic parameter refinement by the Rietveld method (space group Fddd, a = 14.2792(6), b = 14.8916(6), c = 6.5644(3)Å). Both structures are characterized by an icosahedral coordination of the smallest atoms.
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DOI: 10.1016/0925-8388(95)01944-8
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<front><div type="abstract" xml:lang="en">Abstract: The crystal structure of the new compound Tb2(Cu0.47Al0.53)17 with Th2Zn17-type structure (space group R3m, a = 8.767(3), c = 12.824(3)Å) has been determined using single crystal X-ray diffraction leading to R = 0.036 for 407 independent Fhkl values. The crystal structure of Tb(Cu0.58Al0.42)11 has been established from X-ray powder data with atomic parameter refinement by the Rietveld method (space group Fddd, a = 14.2792(6), b = 14.8916(6), c = 6.5644(3)Å). Both structures are characterized by an icosahedral coordination of the smallest atoms.</div>
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<abstract xml:lang="en"><p>The crystal structure of the new compound Tb2(Cu0.47Al0.53)17 with Th2Zn17-type structure (space group R3m, a = 8.767(3), c = 12.824(3)Å) has been determined using single crystal X-ray diffraction leading to R = 0.036 for 407 independent Fhkl values. The crystal structure of Tb(Cu0.58Al0.42)11 has been established from X-ray powder data with atomic parameter refinement by the Rietveld method (space group Fddd, a = 14.2792(6), b = 14.8916(6), c = 6.5644(3)Å). Both structures are characterized by an icosahedral coordination of the smallest atoms.</p>
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<item><term>TbCuAl compounds</term>
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<item><term>Single crystals</term>
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<item><term>Site preference</term>
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<head><ce:dochead><ce:textfn>Chemistry</ce:textfn>
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<ce:title>The Tb<ce:inf>2</ce:inf>
(Cu<ce:inf>0.47</ce:inf>
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and Tb(Cu<ce:inf>0.58</ce:inf>
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aluminides and their crystal structures</ce:title>
<ce:author-group><ce:author><ce:given-name>B.M.</ce:given-name>
<ce:surname>Stel'makhovych</ce:surname>
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<ce:author><ce:given-name>L.G.</ce:given-name>
<ce:surname>Aksel'rud</ce:surname>
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<ce:author><ce:given-name>Yu.B.</ce:given-name>
<ce:surname>Kuz'ma</ce:surname>
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<ce:affiliation><ce:textfn>Institute of Chemistry, L'viv State University, Kyryla and Mefodiya Str. 6, Lviv-5, Ukraine</ce:textfn>
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<ce:abstract><ce:section-title>Abstract</ce:section-title>
<ce:abstract-sec><ce:simple-para>The crystal structure of the new compound Tb<ce:inf>2</ce:inf>
(Cu<ce:inf>0.47</ce:inf>
Al<ce:inf>0.53</ce:inf>
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with Th<ce:inf>2</ce:inf>
Zn<ce:inf>17</ce:inf>
-type structure (space group <math altimg="si1.gif">R<ovl type="bar">3</ovl>
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, <ce:italic>c</ce:italic>
= 12.824(3)Å) has been determined using single crystal X-ray diffraction leading to <ce:italic>R</ce:italic>
= 0.036 for 407 independent <ce:italic>F</ce:italic>
<ce:inf><ce:italic>hkl</ce:italic>
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values. The crystal structure of Tb(Cu<ce:inf>0.58</ce:inf>
Al<ce:inf>0.42</ce:inf>
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has been established from X-ray powder data with atomic parameter refinement by the Rietveld method (space group <ce:italic>Fddd</ce:italic>
, <ce:italic>a</ce:italic>
= 14.2792(6), <ce:italic>b</ce:italic>
= 14.8916(6), <ce:italic>c</ce:italic>
= 6.5644(3)Å). Both structures are characterized by an icosahedral coordination of the smallest atoms.</ce:simple-para>
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<ce:keywords><ce:section-title>Keywords</ce:section-title>
<ce:keyword><ce:text>TbCuAl compounds</ce:text>
</ce:keyword>
<ce:keyword><ce:text>Single crystals</ce:text>
</ce:keyword>
<ce:keyword><ce:text>Crystal structure</ce:text>
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<ce:keyword><ce:text>Site preference</ce:text>
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<abstract lang="en">Abstract: The crystal structure of the new compound Tb2(Cu0.47Al0.53)17 with Th2Zn17-type structure (space group R3m, a = 8.767(3), c = 12.824(3)Å) has been determined using single crystal X-ray diffraction leading to R = 0.036 for 407 independent Fhkl values. The crystal structure of Tb(Cu0.58Al0.42)11 has been established from X-ray powder data with atomic parameter refinement by the Rietveld method (space group Fddd, a = 14.2792(6), b = 14.8916(6), c = 6.5644(3)Å). Both structures are characterized by an icosahedral coordination of the smallest atoms.</abstract>
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<topic>Crystal structure</topic>
<topic>Site preference</topic>
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