ThuliumV1, Hal, Checkpoint, bibRecord, 000029

Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation

Identifieur interne : 000029 ( Hal/Checkpoint ); précédent : 000028; suivant : 000030

Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation

Auteurs : Nicolas Freslon [France] ; Germain Bayon [France] ; Dominique Birot [France] ; Claire Bollinger [France] ; Jean-Alix Barrat [France]

Source :

Talanta [ 0039-9140 ] ; 2011-07-15.

RBID : Hal:insu-00617934

English descriptors

mix :
- ICP-MS, Mg(OH)2 co-precipitation, Rare earth elements (REE), Seawater, Thulium, Trace elements.

Abstract

This paper reports on a novel procedure for determining trace element abundances (REE and Y, Cr, Mn, Co) in seawater by inductively coupled plasma sector field mass spectrometry (ICP-SFMS). The procedure uses a combination of pre-concentration using co-precipitation onto magnesium hydroxides and addition of thulium spike. The validity of the method was assessed onto 25 ml volumes of certified reference materials (NASS- and CASS-4) and in house seawater standard. Procedural blanks were determined by applying the same procedure to aliquots of seawater previously depleted in trace elements by successive Mg(OH)2 co-precipitations, yielding estimated contributions to the studied samples better than 1.1% for all elements, with the exception of Cr (<3.3%) and Co (up to 8%). The reproducibility of the method over the six month duration of the study was smaller than 11% RSD for all the studied elements. Results obtained for NASS-5 and CASS-4 agree well with published working values for trace elements.

Url:

https://hal-insu.archives-ouvertes.fr/insu-00617934

DOI: 10.1016/j.talanta.2011.04.023

Links toward previous steps (curation, corpus...)

to stream Hal, to step Corpus: 000015
to stream Hal, to step Curation: 000015

Links to Exploration step

Hal:insu-00617934

Le document en format XML

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Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation

Determination of rare earth elements and other trace elements (Y, Mn, Co, Cr) in seawater using Tm addition and Mg(OH)2 co-precipitation

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