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Magmatic tempo of Earth’s youngest exposed plutons as revealed by detrital zircon U-Pb geochronology

Identifieur interne : 000006 ( Pmc/Corpus ); précédent : 000005; suivant : 000007

Magmatic tempo of Earth’s youngest exposed plutons as revealed by detrital zircon U-Pb geochronology

Auteurs : Hisatoshi Ito ; Christopher J. Spencer ; Martin Danišík ; Carl W. Hoiland

Source :

RBID : PMC:5622053

Abstract

Plutons are formed by protracted crystallization of magma bodies several kilometers deep within the crust. The temporal frequency (i.e. episodicity or ‘tempo’) of pluton formation is often poorly constrained as timescales of pluton formation are largely variable and may be difficult to resolve by traditional dating methods. The Hida Mountain Range of central Japan hosts the youngest exposed plutons on Earth and provides a unique opportunity to assess the temporal and spatial characteristics of pluton emplacement at high temporal resolution. Here we apply U-Pb geochronology to zircon from the Quaternary Kurobegawa Granite and Takidani Granodiorite in the Hida Mountain Range, and from modern river sediments whose fluvial catchments include these plutons in order to reconstruct their formation. The U-Pb data demonstrate that the Kurobegawa pluton experienced two magmatic pulses at ~2.3 Ma and ~0.9 Ma; whereas, to the south, the Takidani pluton experienced only one magmatic pulse at ~1.6 Ma. These data imply that each of these magmatic systems were both spatially and temporally distinct. The apparent ~0.7 Myr age gap between each of the three magmatic pulses potentially constrains the recharge duration of a single pluton within a larger arc plutonic complex.


Url:
DOI: 10.1038/s41598-017-12790-w
PubMed: 28963475
PubMed Central: 5622053

Links to Exploration step

PMC:5622053

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Perth, WA 6845 Australia</aff>
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<label>4</label>
<institution-wrap>
<institution-id institution-id-type="ISNI">0000000419368956</institution-id>
<institution-id institution-id-type="GRID">grid.168010.e</institution-id>
<institution>Department of Geological Sciences,</institution>
<institution>Stanford University,</institution>
</institution-wrap>
Stanford, CA 94305 USA</aff>
</contrib-group>
<pub-date pub-type="epub">
<day>29</day>
<month>9</month>
<year>2017</year>
</pub-date>
<pub-date pub-type="pmc-release">
<day>29</day>
<month>9</month>
<year>2017</year>
</pub-date>
<pub-date pub-type="collection">
<year>2017</year>
</pub-date>
<volume>7</volume>
<elocation-id>12457</elocation-id>
<history>
<date date-type="received">
<day>6</day>
<month>6</month>
<year>2017</year>
</date>
<date date-type="accepted">
<day>15</day>
<month>9</month>
<year>2017</year>
</date>
</history>
<permissions>
<copyright-statement>© The Author(s) 2017</copyright-statement>
<license license-type="OpenAccess">
<license-p>
<bold>Open Access</bold>
This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit
<ext-link ext-link-type="uri" xlink:href="http://creativecommons.org/licenses/by/4.0/">http://creativecommons.org/licenses/by/4.0/</ext-link>
.</license-p>
</license>
</permissions>
<abstract id="Abs1">
<p id="Par1">Plutons are formed by protracted crystallization of magma bodies several kilometers deep within the crust. The temporal frequency (i.e. episodicity or ‘tempo’) of pluton formation is often poorly constrained as timescales of pluton formation are largely variable and may be difficult to resolve by traditional dating methods. The Hida Mountain Range of central Japan hosts the youngest exposed plutons on Earth and provides a unique opportunity to assess the temporal and spatial characteristics of pluton emplacement at high temporal resolution. Here we apply U-Pb geochronology to zircon from the Quaternary Kurobegawa Granite and Takidani Granodiorite in the Hida Mountain Range, and from modern river sediments whose fluvial catchments include these plutons in order to reconstruct their formation. The U-Pb data demonstrate that the Kurobegawa pluton experienced two magmatic pulses at ~2.3 Ma and ~0.9 Ma; whereas, to the south, the Takidani pluton experienced only one magmatic pulse at ~1.6 Ma. These data imply that each of these magmatic systems were both spatially and temporally distinct. The apparent ~0.7 Myr age gap between each of the three magmatic pulses potentially constrains the recharge duration of a single pluton within a larger arc plutonic complex.</p>
</abstract>
<custom-meta-group>
<custom-meta>
<meta-name>issue-copyright-statement</meta-name>
<meta-value>© The Author(s) 2017</meta-value>
</custom-meta>
</custom-meta-group>
</article-meta>
</front>
<body>
<sec id="Sec1" sec-type="introduction">
<title>Introduction</title>
<p id="Par2">Zircon U-Pb geochronology is now widely used to decipher Earth’s evolution from the Hadean to the Quaternary
<sup>
<xref ref-type="bibr" rid="CR1">1</xref>
<xref ref-type="bibr" rid="CR3">3</xref>
</sup>
. Here we apply this methodology to further constrain the magmatic evolution of the Earth’s youngest exposed plutons, which reside in the Hida Mountain Range (HMR) of central Japan (Fig. 
<xref rid="Fig1" ref-type="fig">1</xref>
). In the northern HMR the Kurobegawa Granite has yielded zircon U-Pb ages of ~0.8 Ma, making it Earth’s youngest known pluton
<sup>
<xref ref-type="bibr" rid="CR3">3</xref>
</sup>
. In the central HMR the Takidani Granodiorite yielded a zircon U-Pb age of ~1.4 Ma
<sup>
<xref ref-type="bibr" rid="CR4">4</xref>
</sup>
(uncorrected for
<sup>230</sup>
Th disequilibrium).
<fig id="Fig1">
<label>Figure 1</label>
<caption>
<p>Simplified map of the Hida Mountain Range (HMR) with the sampling locations. Top panel: Location of the HMR on the island of Honshu, Japan. Bottom panels: simplified geological maps of Kurobegawa pluton modified after Wada
<italic>et al</italic>
.
<sup>
<xref ref-type="bibr" rid="CR22">22</xref>
</sup>
and Takidani pluton
<sup>
<xref ref-type="bibr" rid="CR20">20</xref>
,
<xref ref-type="bibr" rid="CR45">45</xref>
</sup>
. In the Kurobegawa pluton panel, U-Pb ages
<sup>
<xref ref-type="bibr" rid="CR3">3</xref>
</sup>
are shown and country rocks include pre-Quaternary granitic rocks. ISTL: Itoigawa-Shizuoka Tectonic Line, MTL: Median Tectonic Line. Maps were produced using Adobe Illustrator CC 2014 release (
<ext-link ext-link-type="uri" xlink:href="http://blogs.adobe.com/adobeillustrator/tag/2014-release">http://blogs.adobe.com/adobeillustrator/tag/2014-release</ext-link>
).</p>
</caption>
<graphic xlink:href="41598_2017_12790_Fig1_HTML" id="d29e297"></graphic>
</fig>
</p>
<p id="Par3">As single plutons can crystallize over a protracted period of time
<sup>
<xref ref-type="bibr" rid="CR5">5</xref>
<xref ref-type="bibr" rid="CR9">9</xref>
</sup>
, a single hand sample may miss the full crystallization history of an entire pluton. Detrital zircon from modern river sediments offers an alternative method from which zircon from an entire plutonic complex can be more accurately represented
<sup>
<xref ref-type="bibr" rid="CR10">10</xref>
<xref ref-type="bibr" rid="CR12">12</xref>
</sup>
. In order to better understand the dynamics of the Earth’s youngest plutons, we apply zircon U-Pb geochronology to both bedrock and detrital zircon from these plutons sampled from modern river sediments. We employ laser ablation-inductively coupled plasma-mass spectrometry (LA-ICP-MS)
<sup>
<xref ref-type="bibr" rid="CR13">13</xref>
,
<xref ref-type="bibr" rid="CR14">14</xref>
</sup>
because of its high throughput and adequate precision although isotope dilution thermal ionization mass spectrometry (ID-TIMS) has much higher precision and accuracy than LA-ICP-MS
<sup>
<xref ref-type="bibr" rid="CR15">15</xref>
</sup>
. We posit that the results presented herein constrain the timescale and spatial extent of individual plutonic systems and provide insight into the nature and tempo of subduction zone magmatism.</p>
</sec>
<sec id="Sec2">
<title>Geology and samples</title>
<p id="Par4">The HMR is one of the highest mountain ranges in Japan and is composed primarily of Late Cretaceous to Early Cenozoic plutonic rocks and Pleistocene to Holocene volcanic rocks
<sup>
<xref ref-type="bibr" rid="CR16">16</xref>
</sup>
. The HMR lies just to the west of the Itoigawa-Shizuoka Tectonic Line (i.e. the Eurasian-North American plate boundary), hosts a high density of conjugate reverse fault systems, and is recognized as one of the most active seismotectonic regions of the Japanese islands
<sup>
<xref ref-type="bibr" rid="CR17">17</xref>
,
<xref ref-type="bibr" rid="CR18">18</xref>
</sup>
. Exhumation within the HMR is achieved via a combination of structural and surficial denudation processes
<sup>
<xref ref-type="bibr" rid="CR19">19</xref>
<xref ref-type="bibr" rid="CR21">21</xref>
</sup>
.</p>
<p id="Par5">The Kurobegawa Granite is a plutonic complex exposed over an area of ~100 km
<sup>2</sup>
with vertical exposure from 700 m to 2900 m in elevation in the northern HMR. Although it is broadly referred to as a Neogene granite of 10–0.8 Ma
<sup>
<xref ref-type="bibr" rid="CR3">3</xref>
</sup>
, we follow a more common definition as a Quaternary granite
<sup>
<xref ref-type="bibr" rid="CR22">22</xref>
</sup>
. The Kurobegawa Granite is divided into three units (upper, middle, and lower) based on its geochemistry and texture
<sup>
<xref ref-type="bibr" rid="CR22">22</xref>
</sup>
and is intrusive into the Jiigatake Volcanic Rocks at its southeastern border, forming a volcanic-plutonic complex
<sup>
<xref ref-type="bibr" rid="CR16">16</xref>
</sup>
. At its southeastern border, the granite becomes leucocratic and contact-metamorphism is observable on the Jiigatake Volcanic Rocks
<sup>
<xref ref-type="bibr" rid="CR22">22</xref>
,
<xref ref-type="bibr" rid="CR23">23</xref>
</sup>
. The Jiigatake Volcanic Rocks are caldera-fill volcanic rocks of Quaternary age that extend 16 km in the north-south direction and are locally >3500 m in thickness
<sup>
<xref ref-type="bibr" rid="CR24">24</xref>
</sup>
.</p>
<p id="Par6">Sampling was performed in the middle unit of the northern rim of the Kurobegawa Granite (Fig. 
<xref rid="Fig1" ref-type="fig">1</xref>
). At the sampling site, densely concentrated mafic microgranular enclaves (MMEs) are present and so samples were collected from both the mafic and felsic part of the pluton and analyzed separately. River sands were also collected at the mouth of the west-flowing Jijidani River. Based on geologic mapping
<sup>
<xref ref-type="bibr" rid="CR22">22</xref>
</sup>
the catchment of the Jijidani River contains the middle and upper units of the Kurobegawa Granite (Fig. 
<xref rid="Fig1" ref-type="fig">1</xref>
).</p>
<p id="Par7">The Takidani Granodiorite is an elongated pluton (13 km × 4 km) with vertical exposure from 1450 m to 2670 m in elevation situated along a major axis of the central HMR (Fig. 
<xref rid="Fig1" ref-type="fig">1</xref>
). The pluton is vertically zoned from equigranular biotite-hornblende granodiorite in the deepest through hornblende-biotite granodiorite to hornblende-bearing porphyritic biotite granite at the shallowest level and tilts toward the east
<sup>
<xref ref-type="bibr" rid="CR20">20</xref>
,
<xref ref-type="bibr" rid="CR25">25</xref>
</sup>
. It intruded Paleozoic greenstones, a Jurassic accretionary complex, and late Mesozoic to early Cenozoic plutons on its western contact and the Early Pleistocene Hotaka Andesite on the east
<sup>
<xref ref-type="bibr" rid="CR25">25</xref>
</sup>
. The Hotaka Andesite and the Takidani Granodiorite were formed as a volcanic-plutonic complex with close genetic relations
<sup>
<xref ref-type="bibr" rid="CR20">20</xref>
</sup>
. The Hotaka Andesite is composed chiefly of an andesitic to dacitic welded-tuff sheet locally 1500 m in thickness, and subordinate lavas, collapse breccias, diorite porphyry sheets, and a granophyre dike, filling parts of an 18 km × 6 km caldera
<sup>
<xref ref-type="bibr" rid="CR20">20</xref>
</sup>
. The andesitic to dacitic welded-tuff sheet has been metamorphosed to hornblende hornfels within ~800 m, and to biotite hornfels between 800–1500 m from the western contact with the Takidani Granodiorite
<sup>
<xref ref-type="bibr" rid="CR20">20</xref>
</sup>
.</p>
<p id="Par8">A sample was collected on the southeastern margin of the pluton at its shallowest level. Fluvial sediment of the Azusa River was collected within 20 m distance of the plutonic
<italic>in situ</italic>
sample. The Azusa River catchment encompasses portions of the Takidani Granodiorite, Hotaka Andesite and early Cenozoic to late Mesozoic plutons (shown as ~65 Ma Granite in Fig. 
<xref rid="Fig1" ref-type="fig">1</xref>
) that are exposed to the east of the Hotaka Andesite.</p>
</sec>
<sec id="Sec3" sec-type="results">
<title>Results</title>
<sec id="Sec4">
<title>Takidani Granodiorite and Azusa River</title>
<p id="Par9">Zircon from the Takidani Granodiorite yielded an age of 1.58 ± 0.09 Ma (2σ, including systematic error) (Fig. 
<xref rid="Fig2" ref-type="fig">2A</xref>
). This is consistent with the initial
<sup>230</sup>
Th disequilibrium uncorrected U-Pb zircon age of 1.36 ± 0.23 Ma
<sup>
<xref ref-type="bibr" rid="CR4">4</xref>
</sup>
as
<sup>230</sup>
Th correction would shift the age ~0.1 Ma older than the reported age. It is noteworthy that the U-Pb ages of both the shallow (this study) and deep
<sup>
<xref ref-type="bibr" rid="CR4">4</xref>
,
<xref ref-type="bibr" rid="CR26">26</xref>
</sup>
levels of pluton emplacement showed nearly coeval age of ~1.6–1.5 Ma. Detrital zircon from the Azusa River show two age groups: ages with a peak of ~65 Ma and ages less than 10 Ma (Fig. 
<xref rid="Fig2" ref-type="fig">2B</xref>
). The age group of <10 Ma has a prominent peak of ~1.6 Ma (Fig. 
<xref rid="Fig2" ref-type="fig">2C</xref>
), which is in agreement with the age of the Takidani Granodiorite.
<fig id="Fig2">
<label>Figure 2</label>
<caption>
<p>(
<bold>A</bold>
) Weighted mean zircon
<sup>238</sup>
U/
<sup>206</sup>
Pb ages for the Kurobegawa Granite (top), a mafic enclave from the Kurobegawa Granite (middle), and Takidani Granodiorite (bottom). Purple boxes are excluded analyses. Weighted mean ages are shown with 2σ uncertainty and include analytical errors and systematic errors, respectively. (
<bold>B</bold>
,
<bold>C</bold>
) Zircon
<sup>238</sup>
U/
<sup>206</sup>
Pb age distributions (histograms, probability density plot (PDP), and kernel density estimation (KDE)) for detrital zircon from the Jijidani and Azusa river sand younger than 100 Ma (
<bold>B</bold>
) and 10 Ma (
<bold>C</bold>
). n = number of grains. Bandwidth for KDE is fixed at 0.25 Ma.</p>
</caption>
<graphic xlink:href="41598_2017_12790_Fig2_HTML" id="d29e502"></graphic>
</fig>
</p>
<p id="Par10">Chemically etched zircon grains revealed a unique feature (Supplementary Fig. 
<xref rid="MOESM1" ref-type="media">S2</xref>
). As is expected, Quaternary zircon has a low spontaneous fission-track density (Fig. 
<xref rid="MOESM1" ref-type="media">S2A</xref>
). The ~65 Ma zircons have two groups: those with low (Fig. 
<xref rid="MOESM1" ref-type="media">S2B</xref>
) and high (Fig. 
<xref rid="MOESM1" ref-type="media">S2C</xref>
) track densities. The ~65 Ma zircons with a low track density are interpreted as annealed xenocrystic zircons incorporated in the Takidani Granodiorite or Hotaka Andesite magmas whereas those with a high track density should be derived from the outcropping ~65 Ma granitic rocks.</p>
</sec>
<sec id="Sec5">
<title>Kurobegawa Granite and Jijidani River</title>
<p id="Par11">Zircon from the Kurobegawa Granite yielded 0.78 ± 0.06 Ma for the felsic part and 0.75 ± 0.05 Ma for a mafic enclave (Fig. 
<xref rid="Fig2" ref-type="fig">2A</xref>
). Therefore both the felsic and mafic parts of the granite formed almost coevally, consistent with evidence for local magma mingling
<sup>
<xref ref-type="bibr" rid="CR22">22</xref>
</sup>
. These ages are consistent with those obtained previously
<sup>
<xref ref-type="bibr" rid="CR3">3</xref>
</sup>
for the lower and middle units of the Kurobegawa Granite further to the south (Fig. 
<xref rid="Fig1" ref-type="fig">1</xref>
), reaffirming that the Kurobegawa Granite is the Earth’s youngest known exposed granitoid pluton.</p>
<p id="Par12">Detrital zircons from the Jijidani River show two age groups: ages with a small peak of ~65 Ma and ages with a large peak of less than 10 Ma (Fig. 
<xref rid="Fig2" ref-type="fig">2B</xref>
). The age group of <10 Ma has two major peaks of ~0.9 Ma and ~2.3 Ma (Fig. 
<xref rid="Fig2" ref-type="fig">2C</xref>
). This contrasts with the age distribution of zircon from the Azusa River, which has a single age population of ~1.6 Ma. We interpret these data as evidence that the Kurobegawa Granite experienced two intrusion episodes of ~0.9 Ma and ~2.3 Ma in contrast to the single ~1.6 Ma Takidani Granodiorite and Hotaka Andesite magmatism. Ref.
<sup>
<xref ref-type="bibr" rid="CR3">3</xref>
</sup>
reported age peaks of ~0.8 Ma and ~2.3 Ma for the Quaternary Kurobegawa Granite from the southern half of the pluton (Fig. 
<xref rid="Fig1" ref-type="fig">1</xref>
).</p>
</sec>
</sec>
<sec id="Sec6" sec-type="discussion">
<title>Discussion</title>
<p id="Par13">The data presented in this study are the youngest U-Pb zircon ages of any plutonic rock on Earth. The prodigious exhumation rates of the Japanese Alps provide a unique opportunity to probe the development of the Earth’s youngest known exposed pluton. In the case of the Takidani Granodiorite, the plutonic complex is genetically and temporally associated with the correlative volcanic unit of the Hotaka Andesite
<sup>
<xref ref-type="bibr" rid="CR20">20</xref>
</sup>
. A caldera-forming eruption of the Hotaka Andesite with an ~1.7 Ma eruption age of the outflow facies (Nyukawa Pyroclastic Flow Deposit) and correlated widespread tephra (Ho-Kd 39 Tephra) along with paleomagnetic and biostratigraphic studies
<sup>
<xref ref-type="bibr" rid="CR27">27</xref>
</sup>
support this volcanic-plutonic relationship. Furthermore, the near unimodal <10 Ma detrital zircon age peak from the Azusa River implies the Hotaka-Takidani volcanic-plutonic complex was formed within a single relatively contracted period of time.</p>
<p id="Par14">In contrast to the Takidani plutonic complex, the modern river draining the northern part of the Kurobegawa plutonic complex exhibits detrital zircon age spectra with two prominent age peaks at ~0.9 Ma and ~2.3 Ma with bedrock ages indistinguishable from the younger age peak. The ages of the felsic and mafic phases of the Kurobegawa Granite are within uncertainty of analysis and therefore cannot resolve relative timing. A petrologic assessment
<sup>
<xref ref-type="bibr" rid="CR22">22</xref>
</sup>
argues that mafic magma intruded into the host felsic magma, eventually forming MMEs.</p>
<p id="Par15">The Kurobegawa Granite and its surroundings host a great number of hot springs and geothermal activity
<sup>
<xref ref-type="bibr" rid="CR28">28</xref>
</sup>
. Its youngest intrusion (~0.8 Ma) is considerably younger than the Geysers Plutonic complex (1.8–1.1 Ma
<sup>
<xref ref-type="bibr" rid="CR29">29</xref>
</sup>
), which is the assumed heat source for the largest economically viable geothermal field on the planet. Due to its extremely elevated geothermal gradient
<sup>
<xref ref-type="bibr" rid="CR30">30</xref>
</sup>
and thus shallow brittle-ductile transition we posit that the Kurobegawa Granite may also provide economically viable geothermal energy using supercritical water
<sup>
<xref ref-type="bibr" rid="CR31">31</xref>
</sup>
.</p>
<p id="Par16">It has been proposed that a hierarchy of magmatic tempos is present at the various scales of volcanic arcs, volcanic-plutonic systems, individual plutons, caldera forming eruptions, to smaller near-steady state eruptions
<sup>
<xref ref-type="bibr" rid="CR5">5</xref>
,
<xref ref-type="bibr" rid="CR32">32</xref>
,
<xref ref-type="bibr" rid="CR33">33</xref>
</sup>
. If plutonic tempo can be approximated as average pluton volume divided by magmatic flux, then since pluton size is a function of several independent variables (e.g. composition, rheology, stress, and geothermal gradient) plutonic tempo is expected to vary widely between geologic settings and locales. The Quaternary plutonic complexes of the HMR – for which most of these variables are known – thus provide an important measure against which to test geophysical modeling of the mechanisms and timescales of pluton formation.</p>
<p id="Par17">Magmatic episodicity on the <1 Myr timescale described above has never before been documented in plutonic systems. Volcanic systems, however, do often exhibit episodic behavior on similar timescales with protracted zircon growth and marked periods of magmatic quiescence and form in spatially distinct patterns. For example, significant volcanic pulses separated by hundreds of thousands of years have been documented in the Central Andes
<sup>
<xref ref-type="bibr" rid="CR34">34</xref>
,
<xref ref-type="bibr" rid="CR35">35</xref>
</sup>
, Yellowstone
<sup>
<xref ref-type="bibr" rid="CR36">36</xref>
,
<xref ref-type="bibr" rid="CR37">37</xref>
</sup>
, Taupo
<sup>
<xref ref-type="bibr" rid="CR38">38</xref>
</sup>
, and Aegean Sea
<sup>
<xref ref-type="bibr" rid="CR13">13</xref>
</sup>
. The ~0.7 Myr hiatus of the HMR is unusual for plutonic rocks and implies the temporal hierarchy of individual plutonic systems is faster than previously thought. It should further be noted that as zircon crystallization is directly connected to zircon saturation, the zircon record provides a minimum estimate to the longevity of a magmatic system. The Quaternary plutons of the HMR provide unique insight into the hierarchy of magmatic tempo and highlight the need to examine these timescales within young plutonic systems wherein higher temporal resolution is achievable.</p>
</sec>
<sec id="Sec7" sec-type="materials|methods">
<title>Methods</title>
<p id="Par18">Zircon grains were extracted by conventional heavy liquid and magnetic separations, handpicked, embedded in a PFA Teflon sheet and polished in a similar fashion to fission-track studies
<sup>
<xref ref-type="bibr" rid="CR39">39</xref>
,
<xref ref-type="bibr" rid="CR40">40</xref>
</sup>
. LA-ICP-MS was employed to determine U-Pb ages in zircon (see
<italic>supplementary information</italic>
for complete description of methods). An initial assessment of the U-Pb ages revealed that a large proportion (>60%) were older than 10 Ma for the Azusa River sample. Therefore, to preferentially analyze young zircon associated with the Quaternary plutons, grains were etched in NaOH and KOH eutectic melt at ~210 °C for up to 20 hours to reveal spontaneous fission-tracks (Fig. 
<xref rid="MOESM1" ref-type="media">S2</xref>
). Zircon grains with low spontaneous fission-track density were mainly selected for further analyses as these were expected for Quaternary zircon
<sup>
<xref ref-type="bibr" rid="CR40">40</xref>
</sup>
. Some grains with high spontaneous track density were intentionally selected so as to date old zircon grains (JP3-2-101–JP3-2-110 in Table 
<xref rid="MOESM1" ref-type="media">S2</xref>
). U-Pb ages were obtained following procedures described in ref.
<sup>
<xref ref-type="bibr" rid="CR14">14</xref>
</sup>
with LA-ICP-MS equipment (a Thermo Fisher Scientific ELEMENT XR magnetic sector-field ICP-MS coupled to a New Wave Research UP-213 Nd-YAG laser) at the Central Research Institute of Electric Power Industry. All age data are shown in Table 
<xref rid="MOESM1" ref-type="media">S2</xref>
. Note that etching does not affect U-Pb ages as is demonstrated that the same age (~33.5 Ma) was obtained for secondary reference zircon of OD-3 (ref.
<sup>
<xref ref-type="bibr" rid="CR41">41</xref>
</sup>
) both for unetched and 13-hour-etched zircon (Table 
<xref rid="MOESM1" ref-type="media">S2</xref>
). Initial
<sup>230</sup>
Th disequilibrium correction was done assuming the (Th/U)
<sub>magma</sub>
was 5.0, which is essentially the same with the value of 4.8 that was employed in ref.
<sup>
<xref ref-type="bibr" rid="CR3">3</xref>
</sup>
for dating the Kurobegawa Granite. A systematic uncertainty of 5% was added quadratically to the weighted average uncertainty to account for the excess dispersion in the reference materials. Weighted means and reduced chi-squared statistics were calculated using KD
<italic>Χ</italic>
and assessed for over- and under-dispersion
<sup>
<xref ref-type="bibr" rid="CR42">42</xref>
,
<xref ref-type="bibr" rid="CR43">43</xref>
</sup>
. Age spectra were visualized using DensityPlotter
<sup>
<xref ref-type="bibr" rid="CR44">44</xref>
</sup>
.</p>
</sec>
<sec sec-type="supplementary-material">
<title>Electronic supplementary material</title>
<sec id="Sec8">
<p>
<supplementary-material content-type="local-data" id="MOESM1">
<media xlink:href="41598_2017_12790_MOESM1_ESM.pdf">
<caption>
<p>Supplementary information</p>
</caption>
</media>
</supplementary-material>
</p>
</sec>
</sec>
</body>
<back>
<fn-group>
<fn>
<p>
<bold>Electronic supplementary material</bold>
</p>
<p>
<bold>Supplementary information</bold>
accompanies this paper at 10.1038/s41598-017-12790-w.</p>
</fn>
<fn>
<p>
<bold>Publisher's note:</bold>
Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.</p>
</fn>
</fn-group>
<ack>
<title>Acknowledgements</title>
<p>We thank R. Ohki for providing assistance with U-Pb data acquisition. We also thank I. Williams and two anonymous reviewers, whose constructive comments significantly improved the manuscript. This work was partly supported by JSPS KAKENHI Grant Number JP16K05617. M.D. was supported by the AuScope NCRIS2 program, Australian Scientific Instruments Pty Ltd. and Australian Research Council (ARC) Discovery funding scheme (DP160102427), and C.S. and M.D. were supported by Curtin Research Fellowship.</p>
</ack>
<notes notes-type="author-contribution">
<title>Author Contributions</title>
<p>H.I. analyzed LA-ICP-MS U-Pb data and primarily wrote the manuscript. H.I. collected Kurobegawa samples and H.I., C.S., M.D. and C.H. collected Takidani samples. All authors contributed to writing the manuscript.</p>
</notes>
<notes notes-type="COI-statement">
<sec id="FPar1">
<title>Competing Interests</title>
<p id="Par19">The authors declare that they have no competing interests.</p>
</sec>
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