Structure, surface morphology and electrical properties of evaporated Ni thin films: Effect of substrates, thickness and Cu underlayer
Identifieur interne : 000420 ( PascalFrancis/Curation ); précédent : 000419; suivant : 000421Structure, surface morphology and electrical properties of evaporated Ni thin films: Effect of substrates, thickness and Cu underlayer
Auteurs : M. Hemmous [Algérie] ; A. Layadi [Algérie] ; A. Guittoum [Algérie] ; N. Souami [Algérie] ; M. Mebarki [Algérie] ; N. Menni [Algérie]Source :
- Thin solid films [ 0040-6090 ] ; 2014.
Descripteurs français
- Pascal (Inist)
- Structure surface, Morphologie surface, Propriété électrique, Couche mince, Effet dimensionnel, Evaporation, Verre, RBS, Interface, Texture, Grosseur grain, Diffraction RX, Microscopie électronique balayage, Résistivité électrique, Mécanisme croissance, Effet contrainte, Valeur critique, Epaisseur couche, Nickel, Cuivre, Substrat mica, Substrat Al2O3, Substrat cuivre, Substrat silicium, 6855J, 7350, 6855A, 8115A.
- Wicri :
English descriptors
- KwdEn :
Abstract
Series of Ni thin films have been deposited by thermal evaporation onto glass, Si(111), Cu, mica and Al2O3 substrates with and without a Cu underlayer. The Ni thicknesses, t, are in the 4 to 163 nm range. The Cu underlayer has also been evaporated with a Cu thickness equal to 27, 52 and 90 nm. The effects of substrate, the Ni thickness and the Cu underlayer on the structural and electrical properties of Ni are investigated. Rutherford Backscattering Spectroscopy was used to probe the Ni/Substrate and Ni-Cu underlayer interfaces and to measure both Ni and Cu thicknesses. The texture, the strain and the grain size values were derived from X-ray diffraction experiments. The surface morphology is studied by means of a Scanning Electron Microscope. The electrical resistivity is measured by the four point probe. The Ni films grow with the <111> texture on all substrates. The Ni grain sizes D increase with increasing thickness for the glass, Si and mica substrates and decrease for the Cu one. The strain ε is positive for low thickness, decreases in magnitude and becomes negative as t increases. With the Cu underlayer, the growth mode goes through two phases: first, the stress (grain size) increases (decreases) up to a critical thickness tCr, then stress is relieved and grain size increases. All these results will be discussed and correlated.
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<term>Evaporation</term>
<term>Glass</term>
<term>Grain size</term>
<term>Growth mechanism</term>
<term>Interfaces</term>
<term>Layer thickness</term>
<term>Nickel</term>
<term>RBS</term>
<term>Scanning electron microscopy</term>
<term>Size effect</term>
<term>Stress effects</term>
<term>Surface morphology</term>
<term>Surface structure</term>
<term>Texture</term>
<term>Thin films</term>
<term>XRD</term>
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<keywords scheme="Pascal" xml:lang="fr"><term>Structure surface</term>
<term>Morphologie surface</term>
<term>Propriété électrique</term>
<term>Couche mince</term>
<term>Effet dimensionnel</term>
<term>Evaporation</term>
<term>Verre</term>
<term>RBS</term>
<term>Interface</term>
<term>Texture</term>
<term>Grosseur grain</term>
<term>Diffraction RX</term>
<term>Microscopie électronique balayage</term>
<term>Résistivité électrique</term>
<term>Mécanisme croissance</term>
<term>Effet contrainte</term>
<term>Valeur critique</term>
<term>Epaisseur couche</term>
<term>Nickel</term>
<term>Cuivre</term>
<term>Substrat mica</term>
<term>Substrat Al2O3</term>
<term>Substrat cuivre</term>
<term>Substrat silicium</term>
<term>6855J</term>
<term>7350</term>
<term>6855A</term>
<term>8115A</term>
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<front><div type="abstract" xml:lang="en">Series of Ni thin films have been deposited by thermal evaporation onto glass, Si(111), Cu, mica and Al<sub>2</sub>
O<sub>3</sub>
substrates with and without a Cu underlayer. The Ni thicknesses, t, are in the 4 to 163 nm range. The Cu underlayer has also been evaporated with a Cu thickness equal to 27, 52 and 90 nm. The effects of substrate, the Ni thickness and the Cu underlayer on the structural and electrical properties of Ni are investigated. Rutherford Backscattering Spectroscopy was used to probe the Ni/Substrate and Ni-Cu underlayer interfaces and to measure both Ni and Cu thicknesses. The texture, the strain and the grain size values were derived from X-ray diffraction experiments. The surface morphology is studied by means of a Scanning Electron Microscope. The electrical resistivity is measured by the four point probe. The Ni films grow with the <111> texture on all substrates. The Ni grain sizes D increase with increasing thickness for the glass, Si and mica substrates and decrease for the Cu one. The strain ε is positive for low thickness, decreases in magnitude and becomes negative as t increases. With the Cu underlayer, the growth mode goes through two phases: first, the stress (grain size) increases (decreases) up to a critical thickness t<sub>Cr</sub>
, then stress is relieved and grain size increases. All these results will be discussed and correlated.</div>
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<fA14 i1="01"><s1>L.E.S.I,M.S., Département de Physique, Université Ferhat Abbas, Sétif 1</s1>
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<fC01 i1="01" l="ENG"><s0>Series of Ni thin films have been deposited by thermal evaporation onto glass, Si(111), Cu, mica and Al<sub>2</sub>
O<sub>3</sub>
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<fC03 i1="12" i2="3" l="ENG"><s0>XRD</s0>
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<s5>29</s5>
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<s5>30</s5>
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<s5>30</s5>
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<fC03 i1="15" i2="X" l="SPA"><s0>Mecanismo crecimiento</s0>
<s5>30</s5>
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<s5>31</s5>
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<s5>31</s5>
</fC03>
<fC03 i1="17" i2="X" l="FRE"><s0>Valeur critique</s0>
<s5>32</s5>
</fC03>
<fC03 i1="17" i2="X" l="ENG"><s0>Critical value</s0>
<s5>32</s5>
</fC03>
<fC03 i1="17" i2="X" l="SPA"><s0>Valor crítico</s0>
<s5>32</s5>
</fC03>
<fC03 i1="18" i2="X" l="FRE"><s0>Epaisseur couche</s0>
<s5>33</s5>
</fC03>
<fC03 i1="18" i2="X" l="ENG"><s0>Layer thickness</s0>
<s5>33</s5>
</fC03>
<fC03 i1="18" i2="X" l="SPA"><s0>Espesor capa</s0>
<s5>33</s5>
</fC03>
<fC03 i1="19" i2="3" l="FRE"><s0>Nickel</s0>
<s2>NC</s2>
<s5>34</s5>
</fC03>
<fC03 i1="19" i2="3" l="ENG"><s0>Nickel</s0>
<s2>NC</s2>
<s5>34</s5>
</fC03>
<fC03 i1="20" i2="3" l="FRE"><s0>Cuivre</s0>
<s2>NC</s2>
<s5>35</s5>
</fC03>
<fC03 i1="20" i2="3" l="ENG"><s0>Copper</s0>
<s2>NC</s2>
<s5>35</s5>
</fC03>
<fC03 i1="21" i2="3" l="FRE"><s0>Substrat mica</s0>
<s4>INC</s4>
<s5>46</s5>
</fC03>
<fC03 i1="22" i2="3" l="FRE"><s0>Substrat Al2O3</s0>
<s4>INC</s4>
<s5>47</s5>
</fC03>
<fC03 i1="23" i2="3" l="FRE"><s0>Substrat cuivre</s0>
<s4>INC</s4>
<s5>48</s5>
</fC03>
<fC03 i1="24" i2="3" l="FRE"><s0>Substrat silicium</s0>
<s4>INC</s4>
<s5>49</s5>
</fC03>
<fC03 i1="25" i2="3" l="FRE"><s0>6855J</s0>
<s4>INC</s4>
<s5>71</s5>
</fC03>
<fC03 i1="26" i2="3" l="FRE"><s0>7350</s0>
<s4>INC</s4>
<s5>72</s5>
</fC03>
<fC03 i1="27" i2="3" l="FRE"><s0>6855A</s0>
<s4>INC</s4>
<s5>73</s5>
</fC03>
<fC03 i1="28" i2="3" l="FRE"><s0>8115A</s0>
<s4>INC</s4>
<s5>74</s5>
</fC03>
<fN21><s1>209</s1>
</fN21>
<fN44 i1="01"><s1>OTO</s1>
</fN44>
<fN82><s1>OTO</s1>
</fN82>
</pA>
</standard>
</inist>
</record>
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