Synthesis and magnetization studies of nanopowder Fe70Ni20Cr10 alloys prepared by high energy milling
Identifieur interne : 000377 ( PascalFrancis/Curation ); précédent : 000376; suivant : 000378Synthesis and magnetization studies of nanopowder Fe70Ni20Cr10 alloys prepared by high energy milling
Auteurs : R. Chater [Algérie] ; M. Bououdina [Bahreïn] ; D. Chaanbi [Algérie] ; H. Abbas [Bahreïn]Source :
- Journal of solid state chemistry : (Print) [ 0022-4596 ] ; 2013.
Descripteurs français
- Pascal (Inist)
- Aimantation saturation, Synthèse nanomatériau, Broyage poudre, Nanostructure, Nanocristal, Alliage mécanique, Broyeur boulet, Broyeur satellite, Diffraction RX, Cristallite, Paramètre cristallin, Structure cristalline, Dépendance temps, Grosseur grain, Fer, Nickel, Chrome, Morphologie, Microstructure, Microscopie électronique balayage, Champ coercitif, Force coercitive, Cycle hystérésis, Nanomatériau, Mesure magnétique, 8116, 6166, 8107.
- Wicri :
English descriptors
- KwdEn :
- Ball mill, Chromium, Coercive force, Crystal structure, Crystallites, Grain size, Hysteresis loop, Iron, Lattice parameters, Magnetic measurement, Mechanical alloying, Microstructure, Morphology, Nanocrystal, Nanomaterial synthesis, Nanostructured materials, Nanostructures, Nickel, Planetary mill, Powder grinding, Saturation magnetization, Scanning electron microscopy, Time dependence, XRD.
Abstract
Nanocrystalline Fe1-x-yNixCry (x=20, y=10% in Wt)) alloy samples were prepared by mechanical alloying process. Fe, Ni and Cr elemental powders have been ball milled in a planetary mill for various periods of time, up to 27 h. XRD analysis allowed the determination of the structure of the mixture, the average crystallite size and the lattice parameter as a function of milling time. The complete formation of FeNiCr is observed after 27 h milling. With increasing milling time from 0 to 27 h, it is observed that the lattice parameter increases from 0.3515 to 0.3593 nm as well as an increase of microstrain from 0.15 to 0.40%, whereas the grain size decreases from 48 to 13 nm. Grain morphology of the powders at different formation stages was examined using SEM. Saturation magnetization and coercive fields derived from the hysteresis curves are discussed as a function of milling time.
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Ni<sub>20</sub>
Cr<sub>10</sub>
alloys prepared by high energy milling</title>
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<front><div type="abstract" xml:lang="en">Nanocrystalline Fe<sub>1-x-y</sub>
Ni<sub>x</sub>
Cr<sub>y</sub>
(x=20, y=10% in Wt)) alloy samples were prepared by mechanical alloying process. Fe, Ni and Cr elemental powders have been ball milled in a planetary mill for various periods of time, up to 27 h. XRD analysis allowed the determination of the structure of the mixture, the average crystallite size and the lattice parameter as a function of milling time. The complete formation of FeNiCr is observed after 27 h milling. With increasing milling time from 0 to 27 h, it is observed that the lattice parameter increases from 0.3515 to 0.3593 nm as well as an increase of microstrain from 0.15 to 0.40%, whereas the grain size decreases from 48 to 13 nm. Grain morphology of the powders at different formation stages was examined using SEM. Saturation magnetization and coercive fields derived from the hysteresis curves are discussed as a function of milling time.</div>
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Cr<sub>10</sub>
alloys prepared by high energy milling</s1>
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<s5>72</s5>
</fC03>
<fC03 i1="28" i2="3" l="FRE"><s0>8107</s0>
<s4>INC</s4>
<s5>73</s5>
</fC03>
<fN21><s1>175</s1>
</fN21>
<fN44 i1="01"><s1>OTO</s1>
</fN44>
<fN82><s1>OTO</s1>
</fN82>
</pA>
</standard>
</inist>
</record>
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