Nanocrystalline Ni0.8Zn0.2Fe2O4 films prepared by spray deposition from polyol-mediated sol: Microstructural and magnetic characterization
Identifieur interne : 000279 ( PascalFrancis/Curation ); précédent : 000278; suivant : 000280Nanocrystalline Ni0.8Zn0.2Fe2O4 films prepared by spray deposition from polyol-mediated sol: Microstructural and magnetic characterization
Auteurs : Z. Beji [France, Tunisie] ; L. S. Smiri [Tunisie] ; M.-J. Vaulay [France] ; F. Herbst [France] ; S. Ammar [France] ; F. Fievet [France]Source :
- Thin solid films [ 0040-6090 ] ; 2010.
Descripteurs français
- Pascal (Inist)
- Nanostructure, Nanocristal, Couche mince, Microstructure, Propriété magnétique, Diffraction RX, Microscopie électronique balayage, Mesure magnétique, Interférence, Nanoparticule, Nanomatériau, Effet contrainte, Hystérésis, Joint grain, Nickel, Ferrites, Défaut cristallin, Aimantation saturation, Superparamagnétisme, Polyol, Substrat verre, 8107, 6855J.
- Wicri :
- topic : Nickel.
English descriptors
- KwdEn :
- Crystal defects, Ferrites, Grain boundaries, Hysteresis, Interference, Magnetic measurement, Magnetic properties, Microstructure, Nanocrystal, Nanoparticles, Nanostructured materials, Nanostructures, Nickel, Saturation magnetization, Scanning electron microscopy, Stress effects, Superparamagnetism, Thin films, XRD.
Abstract
Nanocrystalline films were directly prepared by spray deposition of a preformed polyol-based Ni0.8Zn0.2Fe2O4 sol on a moderately heated glass substrate. The microstructural and magnetic properties of these films are investigated by X-ray diffraction, scanning electron microscopy and magnetic measurements on a Super Quanducting Interference Devices magnetometer. They are compared with those of nanoparticles precipitated from the sol, and with those of film subsequently annealed in air at 400 °C. The films and the powder exhibit superparamagnetic behaviour with a blocking temperature which increases from the powder to the as-produced film to the annealed film, in agreement with increasing stress and/or crystal size. They are ferrimagnetic at low temperature with a hysteresis feature strongly dependent on the synthesis conditions.The stresses induced in the film upon deposition undoubtedly correlate with a large grain boundaries volume which contributes to the Hc, the coercitive field, increase and Msat, the saturation magnetization, decrease.
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Zn<sub>0.2</sub>
Fe<sub>2</sub>
O<sub>4</sub>
films prepared by spray deposition from polyol-mediated sol: Microstructural and magnetic characterization</title>
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Zn<sub>0.2</sub>
Fe<sub>2</sub>
O<sub>4</sub>
films prepared by spray deposition from polyol-mediated sol: Microstructural and magnetic characterization</title>
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<term>Ferrites</term>
<term>Grain boundaries</term>
<term>Hysteresis</term>
<term>Interference</term>
<term>Magnetic measurement</term>
<term>Magnetic properties</term>
<term>Microstructure</term>
<term>Nanocrystal</term>
<term>Nanoparticles</term>
<term>Nanostructured materials</term>
<term>Nanostructures</term>
<term>Nickel</term>
<term>Saturation magnetization</term>
<term>Scanning electron microscopy</term>
<term>Stress effects</term>
<term>Superparamagnetism</term>
<term>Thin films</term>
<term>XRD</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Nanostructure</term>
<term>Nanocristal</term>
<term>Couche mince</term>
<term>Microstructure</term>
<term>Propriété magnétique</term>
<term>Diffraction RX</term>
<term>Microscopie électronique balayage</term>
<term>Mesure magnétique</term>
<term>Interférence</term>
<term>Nanoparticule</term>
<term>Nanomatériau</term>
<term>Effet contrainte</term>
<term>Hystérésis</term>
<term>Joint grain</term>
<term>Nickel</term>
<term>Ferrites</term>
<term>Défaut cristallin</term>
<term>Aimantation saturation</term>
<term>Superparamagnétisme</term>
<term>Polyol</term>
<term>Substrat verre</term>
<term>8107</term>
<term>6855J</term>
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<front><div type="abstract" xml:lang="en">Nanocrystalline films were directly prepared by spray deposition of a preformed polyol-based Ni<sub>0.8</sub>
Zn<sub>0.2</sub>
Fe<sub>2</sub>
O<sub>4</sub>
sol on a moderately heated glass substrate. The microstructural and magnetic properties of these films are investigated by X-ray diffraction, scanning electron microscopy and magnetic measurements on a Super Quanducting Interference Devices magnetometer. They are compared with those of nanoparticles precipitated from the sol, and with those of film subsequently annealed in air at 400 °C. The films and the powder exhibit superparamagnetic behaviour with a blocking temperature which increases from the powder to the as-produced film to the annealed film, in agreement with increasing stress and/or crystal size. They are ferrimagnetic at low temperature with a hysteresis feature strongly dependent on the synthesis conditions.The stresses induced in the film upon deposition undoubtedly correlate with a large grain boundaries volume which contributes to the H<sub>c</sub>
, the coercitive field, increase and M<sub>sat</sub>
, the saturation magnetization, decrease.</div>
</front>
</TEI>
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<fA08 i1="01" i2="1" l="ENG"><s1>Nanocrystalline Ni<sub>0.8</sub>
Zn<sub>0.2</sub>
Fe<sub>2</sub>
O<sub>4</sub>
films prepared by spray deposition from polyol-mediated sol: Microstructural and magnetic characterization</s1>
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<fA11 i1="01" i2="1"><s1>BEJI (Z.)</s1>
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<fA11 i1="02" i2="1"><s1>SMIRI (L. S.)</s1>
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<fA11 i1="03" i2="1"><s1>VAULAY (M.-J.)</s1>
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<fA11 i1="04" i2="1"><s1>HERBST (F.)</s1>
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<fA11 i1="05" i2="1"><s1>AMMAR (S.)</s1>
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<fA11 i1="06" i2="1"><s1>FIEVET (F.)</s1>
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<fA14 i1="01"><s1>ITODYS, UMR-CNRS 7086, Université Paris 7, 2 Place Jussieu</s1>
<s2>75251 Paris</s2>
<s3>FRA</s3>
<sZ>1 aut.</sZ>
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<fA14 i1="02"><s1>Unité de Recherche 99/UR12-30, Faculté des Sciences de Bizerte</s1>
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<fC01 i1="01" l="ENG"><s0>Nanocrystalline films were directly prepared by spray deposition of a preformed polyol-based Ni<sub>0.8</sub>
Zn<sub>0.2</sub>
Fe<sub>2</sub>
O<sub>4</sub>
sol on a moderately heated glass substrate. The microstructural and magnetic properties of these films are investigated by X-ray diffraction, scanning electron microscopy and magnetic measurements on a Super Quanducting Interference Devices magnetometer. They are compared with those of nanoparticles precipitated from the sol, and with those of film subsequently annealed in air at 400 °C. The films and the powder exhibit superparamagnetic behaviour with a blocking temperature which increases from the powder to the as-produced film to the annealed film, in agreement with increasing stress and/or crystal size. They are ferrimagnetic at low temperature with a hysteresis feature strongly dependent on the synthesis conditions.The stresses induced in the film upon deposition undoubtedly correlate with a large grain boundaries volume which contributes to the H<sub>c</sub>
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<s2>NC</s2>
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<fC03 i1="16" i2="3" l="FRE"><s0>Ferrites</s0>
<s5>16</s5>
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<fC03 i1="16" i2="3" l="ENG"><s0>Ferrites</s0>
<s5>16</s5>
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<fC03 i1="17" i2="3" l="FRE"><s0>Défaut cristallin</s0>
<s5>29</s5>
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<fC03 i1="17" i2="3" l="ENG"><s0>Crystal defects</s0>
<s5>29</s5>
</fC03>
<fC03 i1="18" i2="X" l="FRE"><s0>Aimantation saturation</s0>
<s5>30</s5>
</fC03>
<fC03 i1="18" i2="X" l="ENG"><s0>Saturation magnetization</s0>
<s5>30</s5>
</fC03>
<fC03 i1="18" i2="X" l="SPA"><s0>Imanación saturación</s0>
<s5>30</s5>
</fC03>
<fC03 i1="19" i2="3" l="FRE"><s0>Superparamagnétisme</s0>
<s5>31</s5>
</fC03>
<fC03 i1="19" i2="3" l="ENG"><s0>Superparamagnetism</s0>
<s5>31</s5>
</fC03>
<fC03 i1="20" i2="3" l="FRE"><s0>Polyol</s0>
<s4>INC</s4>
<s5>46</s5>
</fC03>
<fC03 i1="21" i2="3" l="FRE"><s0>Substrat verre</s0>
<s4>INC</s4>
<s5>47</s5>
</fC03>
<fC03 i1="22" i2="3" l="FRE"><s0>8107</s0>
<s4>INC</s4>
<s5>71</s5>
</fC03>
<fC03 i1="23" i2="3" l="FRE"><s0>6855J</s0>
<s4>INC</s4>
<s5>72</s5>
</fC03>
<fN21><s1>109</s1>
</fN21>
<fN44 i1="01"><s1>OTO</s1>
</fN44>
<fN82><s1>OTO</s1>
</fN82>
</pA>
</standard>
</inist>
</record>
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