NickelMaghrebV1, PascalFrancis, Curation, bibRecord, 000237

Copolymerization of Methyl Methacrylate with 4-VinylPyridine Initiated by a Novel Ni(II)a-Benzoinoxime Complex

Identifieur interne : 000237 ( PascalFrancis/Curation ); précédent : 000236; suivant : 000238

Copolymerization of Methyl Methacrylate with 4-VinylPyridine Initiated by a Novel Ni(II)a-Benzoinoxime Complex

Auteurs : Hafida Harrar-Ferfera [Algérie]

Source :

Journal of applied polymer science [ 0021-8995 ] ; 2008.

RBID : Pascal:09-0163317

Descripteurs français

Pascal (Inist)
- Méthacrylate de méthyle copolymère, Pyridine(4-vinyl)copolymère, Rapport réactivité, Distribution séquence, Copolymérisation solution, Copolymérisation radicalaire, Nickel II Complexe, Relation composition propriété, Stabilité thermique, Etude expérimentale, Microstructure, Polymérisation transfert atome, Propriété thermique, Copolymérisation transfert atome.

English descriptors

KwdEn :
- Atom transfer polymerization, Experimental study, Methyl methacrylate copolymer, Microstructure, Nickel II Complexes, Property composition relationship, Pyridine(4-vinyl) copolymer, Radical copolymerization, Reactivity ratio, Sequence distribution, Solution copolymerization, Thermal properties, Thermal stability.

Abstract

Copolymerizations of methyl methacrylate (MMA) with 4-vinylpyridine (4VP) were performed from different monomer feed ratios in 1,4-dioxan at 30°C under free radical initiation experimental conditions, using Ni(II)a-Benzoinoxime complex as initiator. The obtained copolymers (PMMA4VP) were examined by FTIR and ¹H NMR spectroscopies. The composition of these copolymers was calculated, using ¹H NMR spectra and elemental analysis. Monomer reactivity ratios were estimated from Fineman-Ross (FR, r_m = 0.550, r_v = 1.165) and Kelen-Tudos (KT, r_m = 0.559, r_v = 1.286) linearization methods, as well as nonlinear error in variables model (EVM) method using the RREVM computer program (RREVM, r_m = 0.559, r_v = 1.264). These values suggest that MMA-4VP pair copolymerizes randomly. ¹H NMR spectra provide information about the stereochemistry of the copolymers in terms of sequence distributions and configurations. These results showed that the age of the Ni complex has an impact not only on its activity towards polymerization reactions but also on the features of the corresponding copolymers, whereas the chemical composition was insensitive to this prominent factor. The mechanism of MMA-4VP copolymerization is consistent with a radical process as supported by microstructure and molecular weight distribution studies. Thermal behaviours of these copolymers were investigated by differential scanning calorimetry and thermogravimetric analysis.

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A03		`1`		`@0 J. appl. polym. sci.`
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A08	`01`	`1`	`ENG`	`@1 Copolymerization of Methyl Methacrylate with 4-VinylPyridine Initiated by a Novel Ni(II)a-Benzoinoxime Complex`
A11	`01`	`1`		`@1 HARRAR-FERFERA (Hafida)`
A14	`01`			`@1 Laboratoire de Chimie des Polymères, Faculty of Chemistry, University of Sciences and Technology Houari Boumediene @3 DZA @Z 1 aut.`
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A61				`@0 A`
A64	`01`	`1`		`@0 Journal of applied polymer science`
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C01	`01`		`ENG`	@0 Copolymerizations of methyl methacrylate (MMA) with 4-vinylpyridine (4VP) were performed from different monomer feed ratios in 1,4-dioxan at 30°C under free radical initiation experimental conditions, using Ni(II)a-Benzoinoxime complex as initiator. The obtained copolymers (PMMA4VP) were examined by FTIR and ¹H NMR spectroscopies. The composition of these copolymers was calculated, using ¹H NMR spectra and elemental analysis. Monomer reactivity ratios were estimated from Fineman-Ross (FR, r_m = 0.550, r_v = 1.165) and Kelen-Tudos (KT, r_m = 0.559, r_v = 1.286) linearization methods, as well as nonlinear error in variables model (EVM) method using the RREVM computer program (RREVM, r_m = 0.559, r_v = 1.264). These values suggest that MMA-4VP pair copolymerizes randomly. ¹H NMR spectra provide information about the stereochemistry of the copolymers in terms of sequence distributions and configurations. These results showed that the age of the Ni complex has an impact not only on its activity towards polymerization reactions but also on the features of the corresponding copolymers, whereas the chemical composition was insensitive to this prominent factor. The mechanism of MMA-4VP copolymerization is consistent with a radical process as supported by microstructure and molecular weight distribution studies. Thermal behaviours of these copolymers were investigated by differential scanning calorimetry and thermogravimetric analysis.
C02	`01`	`X`		`@0 001D09D02C`
C03	`01`	`X`	`FRE`	`@0 Méthacrylate de méthyle copolymère @2 NK @5 01`
C03	`01`	`X`	`ENG`	`@0 Methyl methacrylate copolymer @2 NK @5 01`
C03	`01`	`X`	`SPA`	`@0 Metacrilato de metilo copolímero @2 NK @5 01`
C03	`02`	`X`	`FRE`	`@0 Pyridine(4-vinyl)copolymère @2 NK @5 02`
C03	`02`	`X`	`ENG`	`@0 Pyridine(4-vinyl) copolymer @2 NK @5 02`
C03	`02`	`X`	`SPA`	`@0 Piridina(4-vinil) copolímero @2 NK @5 02`
C03	`03`	`X`	`FRE`	`@0 Rapport réactivité @5 03`
C03	`03`	`X`	`ENG`	`@0 Reactivity ratio @5 03`
C03	`03`	`X`	`SPA`	`@0 Relación reactividad @5 03`
C03	`04`	`X`	`FRE`	`@0 Distribution séquence @5 04`
C03	`04`	`X`	`ENG`	`@0 Sequence distribution @5 04`
C03	`04`	`X`	`SPA`	`@0 Distribución secuencia @5 04`
C03	`05`	`X`	`FRE`	`@0 Copolymérisation solution @5 05`
C03	`05`	`X`	`ENG`	`@0 Solution copolymerization @5 05`
C03	`05`	`X`	`SPA`	`@0 Copolimerización solución @5 05`
C03	`06`	`X`	`FRE`	`@0 Copolymérisation radicalaire @5 06`
C03	`06`	`X`	`ENG`	`@0 Radical copolymerization @5 06`
C03	`06`	`X`	`SPA`	`@0 Copolimerización radical @5 06`
C03	`07`	`X`	`FRE`	`@0 Nickel II Complexe @1 ACT @2 NC @2 NA @5 07`
C03	`07`	`X`	`ENG`	`@0 Nickel II Complexes @1 ACT @2 NC @2 NA @5 07`
C03	`07`	`X`	`SPA`	`@0 Niquel II Complejo @1 ACT @2 NC @2 NA @5 07`
C03	`08`	`X`	`FRE`	`@0 Relation composition propriété @5 08`
C03	`08`	`X`	`ENG`	`@0 Property composition relationship @5 08`
C03	`08`	`X`	`SPA`	`@0 Relación composición propiedad @5 08`
C03	`09`	`X`	`FRE`	`@0 Stabilité thermique @5 09`
C03	`09`	`X`	`ENG`	`@0 Thermal stability @5 09`
C03	`09`	`X`	`SPA`	`@0 Estabilidad térmica @5 09`
C03	`10`	`X`	`FRE`	`@0 Etude expérimentale @5 10`
C03	`10`	`X`	`ENG`	`@0 Experimental study @5 10`
C03	`10`	`X`	`SPA`	`@0 Estudio experimental @5 10`
C03	`11`	`X`	`FRE`	`@0 Microstructure @5 31`
C03	`11`	`X`	`ENG`	`@0 Microstructure @5 31`
C03	`11`	`X`	`SPA`	`@0 Microestructura @5 31`
C03	`12`	`X`	`FRE`	`@0 Polymérisation transfert atome @5 32`
C03	`12`	`X`	`ENG`	`@0 Atom transfer polymerization @5 32`
C03	`12`	`X`	`SPA`	`@0 Polimerización transferencia atomo @5 32`
C03	`13`	`X`	`FRE`	`@0 Propriété thermique @5 33`
C03	`13`	`X`	`ENG`	`@0 Thermal properties @5 33`
C03	`13`	`X`	`SPA`	`@0 Propiedad térmica @5 33`
C03	`14`	`X`	`FRE`	`@0 Copolymérisation transfert atome @4 INC @5 41`
N21				`@1 117`

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Le document en format XML

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<author><name sortKey="Harrar Ferfera, Hafida" sort="Harrar Ferfera, Hafida" uniqKey="Harrar Ferfera H" first="Hafida" last="Harrar-Ferfera">Hafida Harrar-Ferfera</name>
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<term>Microstructure</term>
<term>Nickel II Complexes</term>
<term>Property composition relationship</term>
<term>Pyridine(4-vinyl) copolymer</term>
<term>Radical copolymerization</term>
<term>Reactivity ratio</term>
<term>Sequence distribution</term>
<term>Solution copolymerization</term>
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<keywords scheme="Pascal" xml:lang="fr"><term>Méthacrylate de méthyle copolymère</term>
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<term>Distribution séquence</term>
<term>Copolymérisation solution</term>
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<front><div type="abstract" xml:lang="en">Copolymerizations of methyl methacrylate (MMA) with 4-vinylpyridine (4VP) were performed from different monomer feed ratios in 1,4-dioxan at 30°C under free radical initiation experimental conditions, using Ni(II)a-Benzoinoxime complex as initiator. The obtained copolymers (PMMA4VP) were examined by FTIR and <sup>1</sup>
H NMR spectroscopies. The composition of these copolymers was calculated, using <sup>1</sup>
H NMR spectra and elemental analysis. Monomer reactivity ratios were estimated from Fineman-Ross (FR, r<sub>m</sub>
 = 0.550, r<sub>v</sub>
 = 1.165) and Kelen-Tudos (KT, r<sub>m</sub>
 = 0.559, r<sub>v</sub>
 = 1.286) linearization methods, as well as nonlinear error in variables model (EVM) method using the RREVM computer program (RREVM, r<sub>m</sub>
 = 0.559, r<sub>v</sub>
 = 1.264). These values suggest that MMA-4VP pair copolymerizes randomly. <sup>1</sup>
H NMR spectra provide information about the stereochemistry of the copolymers in terms of sequence distributions and configurations. These results showed that the age of the Ni complex has an impact not only on its activity towards polymerization reactions but also on the features of the corresponding copolymers, whereas the chemical composition was insensitive to this prominent factor. The mechanism of MMA-4VP copolymerization is consistent with a radical process as supported by microstructure and molecular weight distribution studies. Thermal behaviours of these copolymers were investigated by differential scanning calorimetry and thermogravimetric analysis.</div>
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<fC01 i1="01" l="ENG"><s0>Copolymerizations of methyl methacrylate (MMA) with 4-vinylpyridine (4VP) were performed from different monomer feed ratios in 1,4-dioxan at 30°C under free radical initiation experimental conditions, using Ni(II)a-Benzoinoxime complex as initiator. The obtained copolymers (PMMA4VP) were examined by FTIR and <sup>1</sup>
H NMR spectroscopies. The composition of these copolymers was calculated, using <sup>1</sup>
H NMR spectra and elemental analysis. Monomer reactivity ratios were estimated from Fineman-Ross (FR, r<sub>m</sub>
 = 0.550, r<sub>v</sub>
 = 1.165) and Kelen-Tudos (KT, r<sub>m</sub>
 = 0.559, r<sub>v</sub>
 = 1.286) linearization methods, as well as nonlinear error in variables model (EVM) method using the RREVM computer program (RREVM, r<sub>m</sub>
 = 0.559, r<sub>v</sub>
 = 1.264). These values suggest that MMA-4VP pair copolymerizes randomly. <sup>1</sup>
H NMR spectra provide information about the stereochemistry of the copolymers in terms of sequence distributions and configurations. These results showed that the age of the Ni complex has an impact not only on its activity towards polymerization reactions but also on the features of the corresponding copolymers, whereas the chemical composition was insensitive to this prominent factor. The mechanism of MMA-4VP copolymerization is consistent with a radical process as supported by microstructure and molecular weight distribution studies. Thermal behaviours of these copolymers were investigated by differential scanning calorimetry and thermogravimetric analysis.</s0>
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<s5>09</s5>
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<s5>09</s5>
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<s5>09</s5>
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<s5>10</s5>
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<s5>10</s5>
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<s5>31</s5>
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<s5>31</s5>
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<s5>31</s5>
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<s5>32</s5>
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<s5>32</s5>
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<s5>32</s5>
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<s5>33</s5>
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<s5>33</s5>
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<s5>33</s5>
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<s5>41</s5>
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   |type=    RBID
   |clé=     Pascal:09-0163317
   |texte=   Copolymerization of Methyl Methacrylate with 4-VinylPyridine Initiated by a Novel Ni(II)a-Benzoinoxime Complex
}}

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	Serveur d'exploration sur le nickel au Maghreb
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Serveur d'exploration sur le nickel au Maghreb

Copolymerization of Methyl Methacrylate with 4-VinylPyridine Initiated by a Novel Ni(II)a-Benzoinoxime Complex

Copolymerization of Methyl Methacrylate with 4-VinylPyridine Initiated by a Novel Ni(II)a-Benzoinoxime Complex

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