NickelMaghrebV1, PascalFrancis, Checkpoint, bibRecord, 000538

Electrochemical investigation of Ni-P autocatalytic deposition in ammoniacal solutions

Identifieur interne : 000538 ( PascalFrancis/Checkpoint ); précédent : 000537; suivant : 000539

Electrochemical investigation of Ni-P autocatalytic deposition in ammoniacal solutions

Auteurs : M. Ebn Touhami [Maroc] ; M. Cherkaoui [Maroc] ; A. Srhiri [Maroc] ; A. Ben Bachir [Maroc] ; E. Chassaing [France]

Source :

Journal of applied electrochemistry [ 0021-891X ] ; 1996.

RBID : Pascal:96-0285211

Descripteurs français

Pascal (Inist)
- Etude expérimentale, Dépôt électrolytique, Réaction électrochimique, Autocatalyse, Mécanisme réaction, Electrode, Carbone, Etat vitreux, Nickel, Acier doux, Ammoniac, Nickel Sulfate, Sodium Hypophosphite, Condition opératoire, Impédance électrique, Nickel Alliage, Phosphore Alliage, Alliage binaire.
Wicri :
- topic : Carbone, Nickel.

English descriptors

KwdEn :
- Ammonia, Autocatalysis, Binary alloy, Carbon, Electrical impedance, Electrochemical reaction, Electrodes, Electroplating, Experimental study, Glassy state, Mild steel, Nickel, Nickel Alloys, Nickel Sulfates, Operating conditions, Phosphorus Alloys, Reaction mechanism, Sodium Hypophosphites.

Abstract

The kinetics of Ni-P autocatalytic deposition in ammoniacal solutions was investigated by means of cyclic voltammetry and electrochemical impedance spectroscopy. The effect of the solution constituents (hypophosphite, nickel salt and pH) was examined. Strong interactions between the cathodic and anodic processes occur. The metal discharge is enhanced by the oxidation of hypophosphite, which is the predominant reaction in this process. The nickel deposition also affects the anodic process. With increasing pH the nickel discharge is progressively inhibited due to the change in the nature of the Ni(II) complexes. In contrast, in the presence of Ni(II) species, due to the opposite effect of the two partial processes, the plating rate increases for pH values up to 9 and then decreases for higher pH values.

Affiliations:

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Le document en format XML

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<front><div type="abstract" xml:lang="en">The kinetics of Ni-P autocatalytic deposition in ammoniacal solutions was investigated by means of cyclic voltammetry and electrochemical impedance spectroscopy. The effect of the solution constituents (hypophosphite, nickel salt and pH) was examined. Strong interactions between the cathodic and anodic processes occur. The metal discharge is enhanced by the oxidation of hypophosphite, which is the predominant reaction in this process. The nickel deposition also affects the anodic process. With increasing pH the nickel discharge is progressively inhibited due to the change in the nature of the Ni(II) complexes. In contrast, in the presence of Ni(II) species, due to the opposite effect of the two partial processes, the plating rate increases for pH values up to 9 and then decreases for higher pH values.</div>
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<fC03 i1="14" i2="X" l="ENG"><s0>Operating conditions</s0>
<s5>16</s5>
</fC03>
<fC03 i1="14" i2="X" l="SPA"><s0>Condición operatoria</s0>
<s5>16</s5>
</fC03>
<fC03 i1="15" i2="X" l="FRE"><s0>Impédance électrique</s0>
<s5>17</s5>
</fC03>
<fC03 i1="15" i2="X" l="ENG"><s0>Electrical impedance</s0>
<s5>17</s5>
</fC03>
<fC03 i1="15" i2="X" l="SPA"><s0>Impedancia eléctrica</s0>
<s5>17</s5>
</fC03>
<fC03 i1="16" i2="X" l="FRE"><s0>Nickel Alliage</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>FX</s2>
<s2>NA</s2>
<s5>19</s5>
</fC03>
<fC03 i1="16" i2="X" l="ENG"><s0>Nickel Alloys</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>FX</s2>
<s2>NA</s2>
<s5>19</s5>
</fC03>
<fC03 i1="16" i2="X" l="SPA"><s0>Niquel Aleación</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>FX</s2>
<s2>NA</s2>
<s5>19</s5>
</fC03>
<fC03 i1="17" i2="X" l="FRE"><s0>Phosphore Alliage</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>20</s5>
</fC03>
<fC03 i1="17" i2="X" l="ENG"><s0>Phosphorus Alloys</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>20</s5>
</fC03>
<fC03 i1="17" i2="X" l="SPA"><s0>Fósforo Aleación</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>20</s5>
</fC03>
<fC03 i1="18" i2="X" l="FRE"><s0>Alliage binaire</s0>
<s5>21</s5>
</fC03>
<fC03 i1="18" i2="X" l="ENG"><s0>Binary alloy</s0>
<s5>21</s5>
</fC03>
<fC03 i1="18" i2="X" l="SPA"><s0>Aleación binaria</s0>
<s5>21</s5>
</fC03>
<fC07 i1="01" i2="X" l="FRE"><s0>Métal transition</s0>
<s2>NC</s2>
<s5>10</s5>
</fC07>
<fC07 i1="01" i2="X" l="ENG"><s0>Transition metal</s0>
<s2>NC</s2>
<s5>10</s5>
</fC07>
<fC07 i1="01" i2="X" l="GER"><s0>Uebergangsmetalle</s0>
<s2>NC</s2>
<s5>10</s5>
</fC07>
<fC07 i1="01" i2="X" l="SPA"><s0>Metal transición</s0>
<s2>NC</s2>
<s5>10</s5>
</fC07>
<fN21><s1>198</s1>
</fN21>
</pA>
</standard>
</inist>
<affiliations><list><country><li>France</li>
<li>Maroc</li>
</country>
<region><li>Île-de-France</li>
</region>
<settlement><li>Vitry-sur-Seine</li>
</settlement>
</list>
<tree><country name="Maroc"><noRegion><name sortKey="Ebn Touhami, M" sort="Ebn Touhami, M" uniqKey="Ebn Touhami M" first="M." last="Ebn Touhami">M. Ebn Touhami</name>
</noRegion>
<name sortKey="Ben Bachir, A" sort="Ben Bachir, A" uniqKey="Ben Bachir A" first="A." last="Ben Bachir">A. Ben Bachir</name>
<name sortKey="Cherkaoui, M" sort="Cherkaoui, M" uniqKey="Cherkaoui M" first="M." last="Cherkaoui">M. Cherkaoui</name>
<name sortKey="Srhiri, A" sort="Srhiri, A" uniqKey="Srhiri A" first="A." last="Srhiri">A. Srhiri</name>
</country>
<country name="France"><region name="Île-de-France"><name sortKey="Chassaing, E" sort="Chassaing, E" uniqKey="Chassaing E" first="E." last="Chassaing">E. Chassaing</name>
</region>
</country>
</tree>
</affiliations>
</record>

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	Serveur d'exploration sur le nickel au Maghreb
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Serveur d'exploration sur le nickel au Maghreb

Electrochemical investigation of Ni-P autocatalytic deposition in ammoniacal solutions

Electrochemical investigation of Ni-P autocatalytic deposition in ammoniacal solutions

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