Combustion chemistry and flame structure of furan group biofuels using molecular-beam mass spectrometry and gas chromatography – Part III: 2,5-Dimethylfuran
Identifieur interne : 000171 ( Pmc/Curation ); précédent : 000170; suivant : 000172Combustion chemistry and flame structure of furan group biofuels using molecular-beam mass spectrometry and gas chromatography – Part III: 2,5-Dimethylfuran
Auteurs : Casimir Togbé [Allemagne] ; Luc-Sy Tran [France] ; Dong Liu [Allemagne] ; Daniel Felsmann [Allemagne] ; Patrick O Wald [Allemagne] ; Pierre-Alexandre Glaude [France] ; Baptiste Sirjean [France] ; René Fournet [France] ; Frédérique Battin-Leclerc [France] ; Katharina Kohse-Höinghaus [Allemagne]Source :
- Combustion and flame [ 0010-2180 ] ; 2014.
Abstract
This work is the third part of a study focusing on the combustion chemistry and flame structure of furan and selected alkylated derivatives, i.e. furan in Part I, 2-methylfuran (MF) in Part II, and 2,5-dimethylfuran (DMF) in the present work. Two premixed low-pressure (20 and 40 mbar) flat argon-diluted (50%) flames of DMF were studied with electron-ionization molecular-beam mass spectrometry (EI-MBMS) and gas chromatography (GC) under two equivalence ratios (φ=1.0 and 1.7). Mole fractions of reactants, products, and stable and radical intermediates were measured as a function of the distance to the burner. Kinetic modeling was performed using a reaction mechanism that was further developed in the present series, including Part I and Part II. A reasonable agreement between the present experimental results and the simulation is observed. The main reaction pathways of DMF consumption were derived from a reaction flow analysis. Also, a comparison of the key features for the three flames is presented, as well as a comparison between these flames of furanic compounds and those of other fuels. An a priori surprising ability of DMF to form soot precursors (e.g. 1,3-cyclopentadiene or benzene) compared to less substituted furans and to other fuels has been experimentally observed and is well explained in the model.
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DOI: 10.1016/j.combustflame.2013.05.026
PubMed: 24518851
PubMed Central: 3837207
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id="A2">Laboratoire Réactions et Génie des Procédés (LRGP), CNRS, Université de Lorraine, EN-SIC, 1 rue Grandville, BP 20451, 54001 Nancy Cedex, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Laboratoire Réactions et Génie des Procédés (LRGP), CNRS, Université de Lorraine, EN-SIC, 1 rue Grandville, BP 20451, 54001 Nancy Cedex</wicri:regionArea></affiliation></author><author><name sortKey="Battin Leclerc, Frederique" sort="Battin Leclerc, Frederique" uniqKey="Battin Leclerc F" first="Frédérique" last="Battin-Leclerc">Frédérique Battin-Leclerc</name><affiliation wicri:level="1"><nlm:aff id="A2">Laboratoire Réactions et Génie des Procédés (LRGP), CNRS, Université de Lorraine, EN-SIC, 1 rue Grandville, BP 20451, 54001 Nancy Cedex, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Laboratoire Réactions et Génie des Procédés (LRGP), CNRS, Université de Lorraine, EN-SIC, 1 rue Grandville, BP 20451, 54001 Nancy Cedex</wicri:regionArea></affiliation></author><author><name sortKey="Kohse Hoinghaus, Katharina" sort="Kohse Hoinghaus, Katharina" uniqKey="Kohse Hoinghaus K" first="Katharina" last="Kohse-Höinghaus">Katharina Kohse-Höinghaus</name><affiliation wicri:level="1"><nlm:aff id="A1">Department of Chemistry, Bielefeld University, Universitätsstraße 25, D-33615 Bielefeld, Germany</nlm:aff><country xml:lang="fr">Allemagne</country><wicri:regionArea>Department of Chemistry, Bielefeld University, Universitätsstraße 25, D-33615 Bielefeld</wicri:regionArea></affiliation></author></titleStmt><publicationStmt><idno type="wicri:source">PMC</idno><idno type="pmid">24518851</idno><idno type="pmc">3837207</idno><idno type="url">http://www.ncbi.nlm.nih.gov/pmc/articles/PMC3837207</idno><idno type="RBID">PMC:3837207</idno><idno type="doi">10.1016/j.combustflame.2013.05.026</idno><date when="2014">2014</date><idno type="wicri:Area/Pmc/Corpus">000171</idno><idno type="wicri:explorRef" wicri:stream="Pmc" 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first="Luc-Sy" last="Tran">Luc-Sy Tran</name><affiliation wicri:level="1"><nlm:aff id="A2">Laboratoire Réactions et Génie des Procédés (LRGP), CNRS, Université de Lorraine, EN-SIC, 1 rue Grandville, BP 20451, 54001 Nancy Cedex, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Laboratoire Réactions et Génie des Procédés (LRGP), CNRS, Université de Lorraine, EN-SIC, 1 rue Grandville, BP 20451, 54001 Nancy Cedex</wicri:regionArea></affiliation></author><author><name sortKey="Liu, Dong" sort="Liu, Dong" uniqKey="Liu D" first="Dong" last="Liu">Dong Liu</name><affiliation wicri:level="1"><nlm:aff id="A1">Department of Chemistry, Bielefeld University, Universitätsstraße 25, D-33615 Bielefeld, Germany</nlm:aff><country xml:lang="fr">Allemagne</country><wicri:regionArea>Department of Chemistry, Bielefeld University, Universitätsstraße 25, D-33615 Bielefeld</wicri:regionArea></affiliation></author><author><name sortKey="Felsmann, Daniel" sort="Felsmann, Daniel" uniqKey="Felsmann D" first="Daniel" last="Felsmann">Daniel Felsmann</name><affiliation wicri:level="1"><nlm:aff id="A1">Department of Chemistry, Bielefeld University, Universitätsstraße 25, D-33615 Bielefeld, Germany</nlm:aff><country xml:lang="fr">Allemagne</country><wicri:regionArea>Department of Chemistry, Bielefeld University, Universitätsstraße 25, D-33615 Bielefeld</wicri:regionArea></affiliation></author><author><name sortKey="O Wald, Patrick" sort="O Wald, Patrick" uniqKey="O Wald P" first="Patrick" last="O Wald">Patrick O Wald</name><affiliation wicri:level="1"><nlm:aff id="A1">Department of Chemistry, Bielefeld University, Universitätsstraße 25, D-33615 Bielefeld, Germany</nlm:aff><country xml:lang="fr">Allemagne</country><wicri:regionArea>Department of Chemistry, Bielefeld University, Universitätsstraße 25, D-33615 Bielefeld</wicri:regionArea></affiliation></author><author><name sortKey="Glaude, Pierre Alexandre" sort="Glaude, Pierre Alexandre" uniqKey="Glaude P" first="Pierre-Alexandre" last="Glaude">Pierre-Alexandre Glaude</name><affiliation wicri:level="1"><nlm:aff id="A2">Laboratoire Réactions et Génie des Procédés (LRGP), CNRS, Université de Lorraine, EN-SIC, 1 rue Grandville, BP 20451, 54001 Nancy Cedex, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Laboratoire Réactions et Génie des Procédés (LRGP), CNRS, Université de Lorraine, EN-SIC, 1 rue Grandville, BP 20451, 54001 Nancy Cedex</wicri:regionArea></affiliation></author><author><name sortKey="Sirjean, Baptiste" sort="Sirjean, Baptiste" uniqKey="Sirjean B" first="Baptiste" last="Sirjean">Baptiste Sirjean</name><affiliation wicri:level="1"><nlm:aff id="A2">Laboratoire Réactions et Génie des Procédés (LRGP), CNRS, Université de Lorraine, EN-SIC, 1 rue Grandville, BP 20451, 54001 Nancy Cedex, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Laboratoire Réactions et Génie des Procédés (LRGP), CNRS, Université de Lorraine, EN-SIC, 1 rue Grandville, BP 20451, 54001 Nancy Cedex</wicri:regionArea></affiliation></author><author><name sortKey="Fournet, Rene" sort="Fournet, Rene" uniqKey="Fournet R" first="René" last="Fournet">René Fournet</name><affiliation wicri:level="1"><nlm:aff id="A2">Laboratoire Réactions et Génie des Procédés (LRGP), CNRS, Université de Lorraine, EN-SIC, 1 rue Grandville, BP 20451, 54001 Nancy Cedex, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Laboratoire Réactions et Génie des Procédés (LRGP), CNRS, Université de Lorraine, EN-SIC, 1 rue Grandville, BP 20451, 54001 Nancy Cedex</wicri:regionArea></affiliation></author><author><name sortKey="Battin Leclerc, Frederique" sort="Battin Leclerc, Frederique" uniqKey="Battin Leclerc F" first="Frédérique" last="Battin-Leclerc">Frédérique Battin-Leclerc</name><affiliation wicri:level="1"><nlm:aff id="A2">Laboratoire Réactions et Génie des Procédés (LRGP), CNRS, Université de Lorraine, EN-SIC, 1 rue Grandville, BP 20451, 54001 Nancy Cedex, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Laboratoire Réactions et Génie des Procédés (LRGP), CNRS, Université de Lorraine, EN-SIC, 1 rue Grandville, BP 20451, 54001 Nancy Cedex</wicri:regionArea></affiliation></author><author><name sortKey="Kohse Hoinghaus, Katharina" sort="Kohse Hoinghaus, Katharina" uniqKey="Kohse Hoinghaus K" first="Katharina" last="Kohse-Höinghaus">Katharina Kohse-Höinghaus</name><affiliation wicri:level="1"><nlm:aff id="A1">Department of Chemistry, Bielefeld University, Universitätsstraße 25, D-33615 Bielefeld, Germany</nlm:aff><country xml:lang="fr">Allemagne</country><wicri:regionArea>Department of Chemistry, Bielefeld University, Universitätsstraße 25, D-33615 Bielefeld</wicri:regionArea></affiliation></author></analytic><series><title level="j">Combustion and flame</title><idno type="ISSN">0010-2180</idno><idno type="eISSN">1556-2921</idno><imprint><date when="2014">2014</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en"><p id="P2">This work is the third part of a study focusing on the combustion chemistry and flame structure of furan and selected alkylated derivatives, i.e. furan in Part I, 2-methylfuran (MF) in Part II, and 2,5-dimethylfuran (DMF) in the present work. Two premixed low-pressure (20 and 40 mbar) flat argon-diluted (50%) flames of DMF were studied with electron-ionization molecular-beam mass spectrometry (EI-MBMS) and gas chromatography (GC) under two equivalence ratios (φ=1.0 and 1.7). Mole fractions of reactants, products, and stable and radical intermediates were measured as a function of the distance to the burner. Kinetic modeling was performed using a reaction mechanism that was further developed in the present series, including Part I and Part II. A reasonable agreement between the present experimental results and the simulation is observed. The main reaction pathways of DMF consumption were derived from a reaction flow analysis. Also, a comparison of the key features for the three flames is presented, as well as a comparison between these flames of furanic compounds and those of other fuels. An a priori surprising ability of DMF to form soot precursors (e.g. 1,3-cyclopentadiene or benzene) compared to less substituted furans and to other fuels has been experimentally observed and is well explained in the model.</p></div></front></TEI><pmc article-type="research-article"><pmc-comment>The publisher of this article does not allow downloading of the full text in XML form.</pmc-comment>
<pmc-dir>properties manuscript</pmc-dir>
<front><journal-meta><journal-id journal-id-type="nlm-journal-id">9891739</journal-id><journal-id journal-id-type="pubmed-jr-id">41274</journal-id><journal-id journal-id-type="nlm-ta">Combust Flame</journal-id><journal-id journal-id-type="iso-abbrev">Combust Flame</journal-id><journal-title-group><journal-title>Combustion and flame</journal-title></journal-title-group><issn pub-type="ppub">0010-2180</issn><issn pub-type="epub">1556-2921</issn></journal-meta><article-meta><article-id pub-id-type="pmid">24518851</article-id><article-id pub-id-type="pmc">3837207</article-id><article-id pub-id-type="doi">10.1016/j.combustflame.2013.05.026</article-id><article-id pub-id-type="manuscript">EMS54902</article-id><article-categories><subj-group subj-group-type="heading"><subject>Article</subject></subj-group></article-categories><title-group><article-title>Combustion chemistry and flame structure of furan group biofuels using molecular-beam mass spectrometry and gas chromatography – Part III: 2,5-Dimethylfuran</article-title></title-group><contrib-group><contrib contrib-type="author"><name><surname>Togbé</surname><given-names>Casimir</given-names></name><xref ref-type="aff" rid="A1">1</xref></contrib><contrib contrib-type="author"><name><surname>Tran</surname><given-names>Luc-Sy</given-names></name><xref ref-type="aff" rid="A2">2</xref></contrib><contrib contrib-type="author"><name><surname>Liu</surname><given-names>Dong</given-names></name><xref ref-type="aff" rid="A1">1</xref></contrib><contrib contrib-type="author"><name><surname>Felsmann</surname><given-names>Daniel</given-names></name><xref ref-type="aff" rid="A1">1</xref></contrib><contrib contrib-type="author"><name><surname>Oßwald</surname><given-names>Patrick</given-names></name><xref ref-type="aff" rid="A1">1</xref><xref ref-type="author-notes" rid="FN1">#</xref></contrib><contrib contrib-type="author"><name><surname>Glaude</surname><given-names>Pierre-Alexandre</given-names></name><xref ref-type="aff" rid="A2">2</xref></contrib><contrib contrib-type="author"><name><surname>Sirjean</surname><given-names>Baptiste</given-names></name><xref ref-type="aff" rid="A2">2</xref></contrib><contrib contrib-type="author"><name><surname>Fournet</surname><given-names>René</given-names></name><xref ref-type="aff" rid="A2">2</xref></contrib><contrib contrib-type="author"><name><surname>Battin-Leclerc</surname><given-names>Frédérique</given-names></name><xref ref-type="aff" rid="A2">2</xref><xref ref-type="corresp" rid="CR1">*</xref></contrib><contrib contrib-type="author"><name><surname>Kohse-Höinghaus</surname><given-names>Katharina</given-names></name><xref ref-type="aff" rid="A1">1</xref><xref ref-type="corresp" rid="CR1">*</xref></contrib></contrib-group><aff id="A1"><label>1</label>Department of Chemistry, Bielefeld University, Universitätsstraße 25, D-33615 Bielefeld, Germany</aff><aff id="A2"><label>2</label>Laboratoire Réactions et Génie des Procédés (LRGP), CNRS, Université de Lorraine, EN-SIC, 1 rue Grandville, BP 20451, 54001 Nancy Cedex, France</aff><author-notes><corresp id="CR1"><label>*</label>Corresponding authors. Katharina Kohse-Höinghaus: <email>kkh@uni-bielefeld.de</email>, Phone: +49 521 106 2052, Fax: +49 521 106 6027; Frédérique Battin-Leclerc: <email>Frederique.battin-leclerc@univ-lorraine.fr</email>, Phone: +33 383175125, Fax: +33 383378120</corresp><fn fn-type="current-aff" id="FN1"><label>#</label><p id="P1">now at German Aerospace Center (DLR), Institute of Combustion Technology, Pfaffenwaldring 38-40, D-70569 Stuttgart, Germany</p></fn></author-notes><pub-date pub-type="nihms-submitted"><day>26</day><month>9</month><year>2013</year></pub-date><pub-date pub-type="ppub"><day>1</day><month>3</month><year>2014</year></pub-date><pub-date pub-type="pmc-release"><day>01</day><month>9</month><year>2015</year></pub-date><volume>161</volume><issue>3</issue><fpage>780</fpage><lpage>797</lpage><pmc-comment>elocation-id from pubmed: 10.1016/j.combustflame.2013.05.026</pmc-comment>
<self-uri xlink:href="http://www.sciencedirect.com/science/article/pii/S0010218013002198"></self-uri><abstract><p id="P2">This work is the third part of a study focusing on the combustion chemistry and flame structure of furan and selected alkylated derivatives, i.e. furan in Part I, 2-methylfuran (MF) in Part II, and 2,5-dimethylfuran (DMF) in the present work. Two premixed low-pressure (20 and 40 mbar) flat argon-diluted (50%) flames of DMF were studied with electron-ionization molecular-beam mass spectrometry (EI-MBMS) and gas chromatography (GC) under two equivalence ratios (φ=1.0 and 1.7). Mole fractions of reactants, products, and stable and radical intermediates were measured as a function of the distance to the burner. Kinetic modeling was performed using a reaction mechanism that was further developed in the present series, including Part I and Part II. A reasonable agreement between the present experimental results and the simulation is observed. The main reaction pathways of DMF consumption were derived from a reaction flow analysis. Also, a comparison of the key features for the three flames is presented, as well as a comparison between these flames of furanic compounds and those of other fuels. An a priori surprising ability of DMF to form soot precursors (e.g. 1,3-cyclopentadiene or benzene) compared to less substituted furans and to other fuels has been experimentally observed and is well explained in the model.</p></abstract><kwd-group><kwd>2,5-dimethylfuran</kwd><kwd>low-pressure flame</kwd><kwd>model</kwd><kwd>reaction mechanism</kwd><kwd>reaction flow analysis</kwd><kwd>molecular-beam mass spectrometry</kwd><kwd>gas chromatography</kwd></kwd-group><funding-group><award-group><funding-source country="International">European Research Council : </funding-source><award-id>227669 || ERC_</award-id></award-group></funding-group></article-meta></front></pmc></record>Pour manipuler ce document sous Unix (Dilib)
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