NEW EXPERIMENTAL EVIDENCES ABOUT THE FORMATION AND CONSUMPTION OF KETOHYDROPEROXIDES
Identifieur interne : 000070 ( Pmc/Checkpoint ); précédent : 000069; suivant : 000071NEW EXPERIMENTAL EVIDENCES ABOUT THE FORMATION AND CONSUMPTION OF KETOHYDROPEROXIDES
Auteurs : Frédérique Battin-Leclerc [France] ; Olivier Herbinet [France] ; Pierre-Alexandre Glaude [France] ; René Fournet [France] ; Zhongyue Zhou [République populaire de Chine] ; Liulin Deng [République populaire de Chine] ; Huijun Guo [République populaire de Chine] ; Mingfeng Xie [République populaire de Chine] ; Fei Qi [République populaire de Chine]Source :
- Proceedings of the Combustion Institute. International Symposium on Combustion [ 1540-7489 ] ; 2011.
Abstract
The formation of hydroperoxides postulated in all the kinetic models for the low temperature oxidation of alkanes have been experimentally proved thanks to a new type of apparatus associating a quartz jet-stirred reactor through a molecular-beam sampling system to a reflectron time-of-flight mass spectrometer combined with tunable synchrotron vacuum ultraviolet photoionization. This apparatus has been used to investigate the low-temperature oxidation of
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DOI: 10.1016/j.proci.2010.05.001
PubMed: 23700382
PubMed Central: 3657720
Affiliations:
- France, République populaire de Chine
- Grand Est, Lorraine (région)
- Nancy
- Centre national de la recherche scientifique, Laboratoire réactions et génie des procédés, Nancy-Université, Université de Lorraine
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R. China.</nlm:aff><country xml:lang="fr" wicri:curation="lc">République populaire de Chine</country><wicri:regionArea>National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029</wicri:regionArea><wicri:noRegion>Anhui 230029</wicri:noRegion></affiliation></author><author><name sortKey="Deng, Liulin" sort="Deng, Liulin" uniqKey="Deng L" first="Liulin" last="Deng">Liulin Deng</name><affiliation wicri:level="1"><nlm:aff id="A2">National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029, P. R. China.</nlm:aff><country xml:lang="fr" wicri:curation="lc">République populaire de Chine</country><wicri:regionArea>National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029</wicri:regionArea><wicri:noRegion>Anhui 230029</wicri:noRegion></affiliation></author><author><name sortKey="Guo, Huijun" sort="Guo, Huijun" uniqKey="Guo H" first="Huijun" last="Guo">Huijun Guo</name><affiliation wicri:level="1"><nlm:aff id="A2">National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029, P. R. China.</nlm:aff><country xml:lang="fr" wicri:curation="lc">République populaire de Chine</country><wicri:regionArea>National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029</wicri:regionArea><wicri:noRegion>Anhui 230029</wicri:noRegion></affiliation></author><author><name sortKey="Xie, Mingfeng" sort="Xie, Mingfeng" uniqKey="Xie M" first="Mingfeng" last="Xie">Mingfeng Xie</name><affiliation wicri:level="1"><nlm:aff id="A2">National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029, P. R. China.</nlm:aff><country xml:lang="fr" wicri:curation="lc">République populaire de Chine</country><wicri:regionArea>National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029</wicri:regionArea><wicri:noRegion>Anhui 230029</wicri:noRegion></affiliation></author><author><name sortKey="Qi, Fei" sort="Qi, Fei" uniqKey="Qi F" first="Fei" last="Qi">Fei Qi</name><affiliation wicri:level="1"><nlm:aff id="A2">National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029, P. R. China.</nlm:aff><country xml:lang="fr" wicri:curation="lc">République populaire de Chine</country><wicri:regionArea>National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029</wicri:regionArea><wicri:noRegion>Anhui 230029</wicri:noRegion></affiliation></author></titleStmt><publicationStmt><idno type="wicri:source">PMC</idno><idno type="pmid">23700382</idno><idno type="pmc">3657720</idno><idno type="url">http://www.ncbi.nlm.nih.gov/pmc/articles/PMC3657720</idno><idno type="RBID">PMC:3657720</idno><idno type="doi">10.1016/j.proci.2010.05.001</idno><date when="2011">2011</date><idno type="wicri:Area/Pmc/Corpus">000150</idno><idno type="wicri:explorRef" wicri:stream="Pmc" wicri:step="Corpus" wicri:corpus="PMC">000150</idno><idno type="wicri:Area/Pmc/Curation">000150</idno><idno type="wicri:explorRef" wicri:stream="Pmc" wicri:step="Curation">000150</idno><idno type="wicri:Area/Pmc/Checkpoint">000070</idno><idno type="wicri:explorRef" wicri:stream="Pmc" wicri:step="Checkpoint">000070</idno></publicationStmt><sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">NEW EXPERIMENTAL EVIDENCES ABOUT THE FORMATION AND CONSUMPTION OF KETOHYDROPEROXIDES</title><author><name sortKey="Battin Leclerc, Frederique" sort="Battin Leclerc, Frederique" uniqKey="Battin Leclerc F" first="Frédérique" last="Battin-Leclerc">Frédérique Battin-Leclerc</name><affiliation wicri:level="4"><nlm:aff id="A1">Laboratoire Réactions et Génie des Procédés, CNRS, Nancy Université, ENSIC, 1, rue Grandville, BP 20451, 54001 Nancy Cedex, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Laboratoire Réactions et Génie des Procédés, CNRS, Nancy Université, ENSIC, 1, rue Grandville, BP 20451, 54001 Nancy Cedex</wicri:regionArea><placeName><region type="region" nuts="2">Grand Est</region><region type="old region" nuts="2">Lorraine (région)</region><settlement type="city">Nancy</settlement></placeName><orgName type="university">Nancy-Université</orgName><placeName><settlement type="city">Nancy</settlement><region type="region" nuts="2">Grand Est</region><region type="region" nuts="2">Lorraine (région)</region></placeName><orgName type="laboratoire" n="5">Laboratoire réactions et génie des procédés</orgName><orgName type="university">Université de Lorraine</orgName><orgName type="institution">Centre national de la recherche scientifique</orgName></affiliation></author><author><name sortKey="Herbinet, Olivier" sort="Herbinet, Olivier" uniqKey="Herbinet O" first="Olivier" last="Herbinet">Olivier Herbinet</name><affiliation wicri:level="4"><nlm:aff id="A1">Laboratoire Réactions et Génie des Procédés, CNRS, Nancy Université, ENSIC, 1, rue Grandville, BP 20451, 54001 Nancy Cedex, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Laboratoire Réactions et Génie des Procédés, CNRS, Nancy Université, ENSIC, 1, rue Grandville, BP 20451, 54001 Nancy Cedex</wicri:regionArea><placeName><region type="region" nuts="2">Grand Est</region><region type="old region" nuts="2">Lorraine (région)</region><settlement type="city">Nancy</settlement></placeName><orgName type="university">Nancy-Université</orgName></affiliation></author><author><name sortKey="Glaude, Pierre Alexandre" sort="Glaude, Pierre Alexandre" uniqKey="Glaude P" first="Pierre-Alexandre" last="Glaude">Pierre-Alexandre Glaude</name><affiliation wicri:level="4"><nlm:aff id="A1">Laboratoire Réactions et Génie des Procédés, CNRS, Nancy Université, ENSIC, 1, rue Grandville, BP 20451, 54001 Nancy Cedex, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Laboratoire Réactions et Génie des Procédés, CNRS, Nancy Université, ENSIC, 1, rue Grandville, BP 20451, 54001 Nancy Cedex</wicri:regionArea><placeName><region type="region" nuts="2">Grand Est</region><region type="old region" nuts="2">Lorraine (région)</region><settlement type="city">Nancy</settlement></placeName><orgName type="university">Nancy-Université</orgName></affiliation></author><author><name sortKey="Fournet, Rene" sort="Fournet, Rene" uniqKey="Fournet R" first="René" last="Fournet">René Fournet</name><affiliation wicri:level="4"><nlm:aff id="A1">Laboratoire Réactions et Génie des Procédés, CNRS, Nancy Université, ENSIC, 1, rue Grandville, BP 20451, 54001 Nancy Cedex, France</nlm:aff><country xml:lang="fr">France</country><wicri:regionArea>Laboratoire Réactions et Génie des Procédés, CNRS, Nancy Université, ENSIC, 1, rue Grandville, BP 20451, 54001 Nancy Cedex</wicri:regionArea><placeName><region type="region" nuts="2">Grand Est</region><region type="old region" nuts="2">Lorraine (région)</region><settlement type="city">Nancy</settlement></placeName><orgName type="university">Nancy-Université</orgName></affiliation></author><author><name sortKey="Zhou, Zhongyue" sort="Zhou, Zhongyue" uniqKey="Zhou Z" first="Zhongyue" last="Zhou">Zhongyue Zhou</name><affiliation wicri:level="1"><nlm:aff id="A2">National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029, P. R. China.</nlm:aff><country xml:lang="fr" wicri:curation="lc">République populaire de Chine</country><wicri:regionArea>National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029</wicri:regionArea><wicri:noRegion>Anhui 230029</wicri:noRegion></affiliation></author><author><name sortKey="Deng, Liulin" sort="Deng, Liulin" uniqKey="Deng L" first="Liulin" last="Deng">Liulin Deng</name><affiliation wicri:level="1"><nlm:aff id="A2">National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029, P. R. China.</nlm:aff><country xml:lang="fr" wicri:curation="lc">République populaire de Chine</country><wicri:regionArea>National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029</wicri:regionArea><wicri:noRegion>Anhui 230029</wicri:noRegion></affiliation></author><author><name sortKey="Guo, Huijun" sort="Guo, Huijun" uniqKey="Guo H" first="Huijun" last="Guo">Huijun Guo</name><affiliation wicri:level="1"><nlm:aff id="A2">National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029, P. R. China.</nlm:aff><country xml:lang="fr" wicri:curation="lc">République populaire de Chine</country><wicri:regionArea>National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029</wicri:regionArea><wicri:noRegion>Anhui 230029</wicri:noRegion></affiliation></author><author><name sortKey="Xie, Mingfeng" sort="Xie, Mingfeng" uniqKey="Xie M" first="Mingfeng" last="Xie">Mingfeng Xie</name><affiliation wicri:level="1"><nlm:aff id="A2">National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029, P. R. China.</nlm:aff><country xml:lang="fr" wicri:curation="lc">République populaire de Chine</country><wicri:regionArea>National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029</wicri:regionArea><wicri:noRegion>Anhui 230029</wicri:noRegion></affiliation></author><author><name sortKey="Qi, Fei" sort="Qi, Fei" uniqKey="Qi F" first="Fei" last="Qi">Fei Qi</name><affiliation wicri:level="1"><nlm:aff id="A2">National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029, P. R. China.</nlm:aff><country xml:lang="fr" wicri:curation="lc">République populaire de Chine</country><wicri:regionArea>National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029</wicri:regionArea><wicri:noRegion>Anhui 230029</wicri:noRegion></affiliation></author></analytic><series><title level="j">Proceedings of the Combustion Institute. International Symposium on Combustion</title><idno type="ISSN">1540-7489</idno><idno type="eISSN">1873-2704</idno><imprint><date when="2011">2011</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en"><p id="P1">The formation of hydroperoxides postulated in all the kinetic models for the low temperature oxidation of alkanes have been experimentally proved thanks to a new type of apparatus associating a quartz jet-stirred reactor through a molecular-beam sampling system to a reflectron time-of-flight mass spectrometer combined with tunable synchrotron vacuum ultraviolet photoionization. This apparatus has been used to investigate the low-temperature oxidation of <italic>n</italic>-butane and has allowed demonstrating the formation of different types of alkylhydroperoxides, namely methylhydroperoxide, ethylhydroperoxide and butylhydroperoxide, and of C<sub>4</sub> alkylhydroperoxides including a carbonyl function (ketohydroperoxides). In addition, the formation of products deriving from these ketohydroperoxides, such as C<sub>4</sub> molecules including either two carbonyl groups or one carbonyl and one alcohol functions, has been observed. Simulations using a detailed kinetic model have been performed to support some of the assumptions made in this work.</p></div></front></TEI><pmc article-type="research-article"><pmc-comment>The publisher of this article does not allow downloading of the full text in XML form.</pmc-comment>
<pmc-dir>properties manuscript</pmc-dir>
<front><journal-meta><journal-id journal-id-type="nlm-journal-id">101607410</journal-id><journal-id journal-id-type="pubmed-jr-id">41311</journal-id><journal-id journal-id-type="nlm-ta">Proc Combust Inst</journal-id><journal-id journal-id-type="iso-abbrev">Proc Combust Inst</journal-id><journal-title-group><journal-title>Proceedings of the Combustion Institute. International Symposium on Combustion</journal-title></journal-title-group><issn pub-type="ppub">1540-7489</issn><issn pub-type="epub">1873-2704</issn></journal-meta><article-meta><article-id pub-id-type="pmid">23700382</article-id><article-id pub-id-type="pmc">3657720</article-id><article-id pub-id-type="doi">10.1016/j.proci.2010.05.001</article-id><article-id pub-id-type="manuscript">EMS52437</article-id><article-categories><subj-group subj-group-type="heading"><subject>Article</subject></subj-group></article-categories><title-group><article-title>NEW EXPERIMENTAL EVIDENCES ABOUT THE FORMATION AND CONSUMPTION OF KETOHYDROPEROXIDES</article-title></title-group><contrib-group><contrib contrib-type="author"><name><surname>Battin-Leclerc</surname><given-names>Frédérique</given-names></name><xref ref-type="aff" rid="A1">1</xref><xref ref-type="corresp" rid="CR1">*</xref></contrib><contrib contrib-type="author"><name><surname>Herbinet</surname><given-names>Olivier</given-names></name><xref ref-type="aff" rid="A1">1</xref></contrib><contrib contrib-type="author"><name><surname>Glaude</surname><given-names>Pierre-Alexandre</given-names></name><xref ref-type="aff" rid="A1">1</xref></contrib><contrib contrib-type="author"><name><surname>Fournet</surname><given-names>René</given-names></name><xref ref-type="aff" rid="A1">1</xref></contrib><contrib contrib-type="author"><name><surname>Zhou</surname><given-names>Zhongyue</given-names></name><xref ref-type="aff" rid="A2">2</xref></contrib><contrib contrib-type="author"><name><surname>Deng</surname><given-names>Liulin</given-names></name><xref ref-type="aff" rid="A2">2</xref></contrib><contrib contrib-type="author"><name><surname>Guo</surname><given-names>Huijun</given-names></name><xref ref-type="aff" rid="A2">2</xref></contrib><contrib contrib-type="author"><name><surname>Xie</surname><given-names>Mingfeng</given-names></name><xref ref-type="aff" rid="A2">2</xref></contrib><contrib contrib-type="author"><name><surname>Qi</surname><given-names>Fei</given-names></name><xref ref-type="aff" rid="A2">2</xref><xref ref-type="corresp" rid="CR1">*</xref></contrib></contrib-group><aff id="A1"><label>1</label>Laboratoire Réactions et Génie des Procédés, CNRS, Nancy Université, ENSIC, 1, rue Grandville, BP 20451, 54001 Nancy Cedex, France</aff><aff id="A2"><label>2</label>National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei, Anhui 230029, P. R. China.</aff><author-notes><corresp id="CR1"><label>*</label>To whom correspondence should be addressed. <email>Frederique.Battin-Leclerc@ensic.inpl-nancy.fr</email>, <email>fqi@ustc.edu.cn</email>.</corresp></author-notes><pub-date pub-type="nihms-submitted"><day>13</day><month>5</month><year>2013</year></pub-date><pub-date pub-type="ppub"><month>12</month><year>2011</year></pub-date><pub-date pub-type="pmc-release"><day>20</day><month>5</month><year>2013</year></pub-date><volume>33</volume><issue>1</issue><fpage>325</fpage><lpage>331</lpage><self-uri xlink:href="http://www.sciencedirect.com/science/article/pii/S1540748910000027"></self-uri><abstract><p id="P1">The formation of hydroperoxides postulated in all the kinetic models for the low temperature oxidation of alkanes have been experimentally proved thanks to a new type of apparatus associating a quartz jet-stirred reactor through a molecular-beam sampling system to a reflectron time-of-flight mass spectrometer combined with tunable synchrotron vacuum ultraviolet photoionization. This apparatus has been used to investigate the low-temperature oxidation of <italic>n</italic>-butane and has allowed demonstrating the formation of different types of alkylhydroperoxides, namely methylhydroperoxide, ethylhydroperoxide and butylhydroperoxide, and of C<sub>4</sub> alkylhydroperoxides including a carbonyl function (ketohydroperoxides). In addition, the formation of products deriving from these ketohydroperoxides, such as C<sub>4</sub> molecules including either two carbonyl groups or one carbonyl and one alcohol functions, has been observed. Simulations using a detailed kinetic model have been performed to support some of the assumptions made in this work.</p></abstract><kwd-group><kwd>Jet-stirred reactor</kwd><kwd>molecular beam-mass spectrometry</kwd><kwd>low-temperature oxidation</kwd><kwd><italic>n</italic>-butane</kwd><kwd>hydroperoxides</kwd></kwd-group><funding-group><award-group><funding-source country="International">European Research Council : </funding-source><award-id>227669 || ERC_</award-id></award-group></funding-group></article-meta></front></pmc><affiliations><list><country><li>France</li><li>République populaire de Chine</li></country><region><li>Grand Est</li><li>Lorraine (région)</li></region><settlement><li>Nancy</li></settlement><orgName><li>Centre national de la recherche scientifique</li><li>Laboratoire réactions et génie des procédés</li><li>Nancy-Université</li><li>Université de Lorraine</li></orgName></list><tree><country name="France"><region name="Grand Est"><name sortKey="Battin Leclerc, Frederique" sort="Battin Leclerc, Frederique" uniqKey="Battin Leclerc F" first="Frédérique" last="Battin-Leclerc">Frédérique Battin-Leclerc</name></region><name sortKey="Fournet, Rene" sort="Fournet, Rene" uniqKey="Fournet R" first="René" last="Fournet">René Fournet</name><name sortKey="Glaude, Pierre Alexandre" sort="Glaude, Pierre Alexandre" uniqKey="Glaude P" first="Pierre-Alexandre" last="Glaude">Pierre-Alexandre Glaude</name><name sortKey="Herbinet, Olivier" sort="Herbinet, Olivier" uniqKey="Herbinet O" first="Olivier" last="Herbinet">Olivier Herbinet</name></country><country name="République populaire de Chine"><noRegion><name sortKey="Zhou, Zhongyue" sort="Zhou, Zhongyue" uniqKey="Zhou Z" first="Zhongyue" last="Zhou">Zhongyue Zhou</name></noRegion><name sortKey="Deng, Liulin" sort="Deng, Liulin" uniqKey="Deng L" first="Liulin" last="Deng">Liulin Deng</name><name sortKey="Guo, Huijun" sort="Guo, Huijun" uniqKey="Guo H" first="Huijun" last="Guo">Huijun Guo</name><name sortKey="Qi, Fei" sort="Qi, Fei" uniqKey="Qi F" first="Fei" last="Qi">Fei Qi</name><name sortKey="Xie, Mingfeng" sort="Xie, Mingfeng" uniqKey="Xie M" first="Mingfeng" last="Xie">Mingfeng Xie</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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