The Origin of Molecular Mobility During Biomass Pyrolysis as Revealed by In situ 1H NMR Spectroscopy
Identifieur interne : 000886 ( Main/Exploration ); précédent : 000885; suivant : 000887The Origin of Molecular Mobility During Biomass Pyrolysis as Revealed by In situ 1H NMR Spectroscopy
Auteurs : Anthony Dufour (génie des procédés) [France, Royaume-Uni] ; Miguel Castro-Diaz [Royaume-Uni] ; Nicolas Brosse [France] ; Mohamed Bouroukba [France] ; Colin Snape [Royaume-Uni]Source :
- ChemSusChem [ 1864-5631 ] ; 2012-07.
Descripteurs français
- KwdFr :
- MESH :
- métabolisme : Biopolymères, Cellulose, Lignine, Minéraux, Xylanes.
- Wicri :
English descriptors
- KwdEn :
- Anal, Angew, Appl, Biomass, Biomass pyrolysis, Biopolymers (chemistry), Biopolymers (metabolism), Cellulose, Cellulose (chemistry), Cellulose (metabolism), Cellulose pyrolysis, Chem, Chemsuschem, Energy fuels, Extraction procedure, First time, Fluidity, Fluidity development, Glass transition phase, Gmbh, Heating rate, Holocelluloses, Kgaa, Lignin, Lignin (chemistry), Lignin (metabolism), Lorentzian, Lower temperature, Magnetic Resonance Spectroscopy, Mass loss, Maximum fluidity, Maximum mass loss rate, Maximum weight loss, Microgranular cellulose, Minerals (chemistry), Minerals (metabolism), Miscanthus, Miscanthus cellulose, Mobile hydrogen fraction, Mobile phase, Mobility, Mobility development, Molecular mobility, Native biomass network, Native miscanthus, Native network, Poaceae (chemistry), Polym, Polymer, Proton, Protons, Pyrolysis, Pyrolysis products, Relaxation time, Snape, Synthetic blend, Temperature, Thermogravimetric analysis, Verlag, Verlag gmbh, Weinheim, Weinheim chemsuschem, Xylan, Xylan pyrolysis, Xylans (chemistry), Xylans (metabolism).
- MESH :
- Teeft :
- Anal, Angew, Appl, Biomass, Biomass pyrolysis, Cellulose, Cellulose pyrolysis, Chem, Chemsuschem, Energy fuels, Extraction procedure, First time, Fluidity, Fluidity development, Glass transition phase, Gmbh, Heating rate, Holocelluloses, Kgaa, Lignin, Lorentzian, Lower temperature, Magnetic Resonance Spectroscopy, Mass loss, Maximum fluidity, Maximum mass loss rate, Maximum weight loss, Microgranular cellulose, Miscanthus, Miscanthus cellulose, Mobile hydrogen fraction, Mobile phase, Mobility, Mobility development, Molecular mobility, Native biomass network, Native miscanthus, Native network, Polym, Polymer, Proton, Protons, Pyrolysis, Pyrolysis products, Relaxation time, Snape, Synthetic blend, Temperature, Thermogravimetric analysis, Verlag, Verlag gmbh, Weinheim, Weinheim chemsuschem, Xylan, Xylan pyrolysis.
- mix :
Abstract
The thermochemical conversion of lignocellulosic biomass feedstocks offers an important potential route for the production of biofuels and value‐added green chemicals. Pyrolysis is the first phenomenon involved in all biomass thermochemical processes and it controls to a major extent the product composition. The composition of pyrolysis products can be affected markedly by the extent of softening that occurs. In spite of extensive work on biomass pyrolysis, the development of fluidity during the pyrolysis of biomass has not been quantified. This paper provides the first experimental investigation of proton mobility during biomass pyrolysis by in situ 1H NMR spectroscopy. The origin of mobility is discussed for cellulose, lignin and xylan. The effect of minerals on cellulose mobility is also investigated. Interactions between polymers in the native biomass network are revealed by in situ 1H NMR analysis.
Url:
- https://api.istex.fr/document/DAF9621D2A776ED03D29BE856D164EB4A7D0181B/fulltext/pdf
- https://hal.archives-ouvertes.fr/hal-00777023
DOI: 10.1002/cssc.201100442
Affiliations:
- France, Royaume-Uni
- Angleterre, Grand Est, Lorraine (région), Nottinghamshire
- Nancy, Nottingham
- Centre national de la recherche scientifique, Laboratoire réactions et génie des procédés, Nancy-Université, Université de Lorraine, Université de Nottingham
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Le document en format XML
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xml:lang="en"><term>Anal</term><term>Angew</term><term>Appl</term><term>Biomass</term><term>Biomass pyrolysis</term><term>Biopolymers (chemistry)</term><term>Biopolymers (metabolism)</term><term>Cellulose</term><term>Cellulose (chemistry)</term><term>Cellulose (metabolism)</term><term>Cellulose pyrolysis</term><term>Chem</term><term>Chemsuschem</term><term>Energy fuels</term><term>Extraction procedure</term><term>First time</term><term>Fluidity</term><term>Fluidity development</term><term>Glass transition phase</term><term>Gmbh</term><term>Heating rate</term><term>Holocelluloses</term><term>Kgaa</term><term>Lignin</term><term>Lignin (chemistry)</term><term>Lignin (metabolism)</term><term>Lorentzian</term><term>Lower temperature</term><term>Magnetic Resonance Spectroscopy</term><term>Mass loss</term><term>Maximum fluidity</term><term>Maximum mass loss rate</term><term>Maximum weight loss</term><term>Microgranular cellulose</term><term>Minerals (chemistry)</term><term>Minerals (metabolism)</term><term>Miscanthus</term><term>Miscanthus cellulose</term><term>Mobile hydrogen fraction</term><term>Mobile phase</term><term>Mobility</term><term>Mobility development</term><term>Molecular mobility</term><term>Native biomass network</term><term>Native miscanthus</term><term>Native network</term><term>Poaceae (chemistry)</term><term>Polym</term><term>Polymer</term><term>Proton</term><term>Protons</term><term>Pyrolysis</term><term>Pyrolysis products</term><term>Relaxation time</term><term>Snape</term><term>Synthetic blend</term><term>Temperature</term><term>Thermogravimetric analysis</term><term>Verlag</term><term>Verlag gmbh</term><term>Weinheim</term><term>Weinheim chemsuschem</term><term>Xylan</term><term>Xylan pyrolysis</term><term>Xylans (chemistry)</term><term>Xylans (metabolism)</term></keywords><keywords scheme="KwdFr" xml:lang="fr"><term>Biomasse</term><term>Biopolymères ()</term><term>Biopolymères (métabolisme)</term><term>Cellulose ()</term><term>Cellulose (métabolisme)</term><term>Lignine ()</term><term>Lignine (métabolisme)</term><term>Minéraux ()</term><term>Minéraux (métabolisme)</term><term>Poaceae ()</term><term>Protons</term><term>Spectroscopie par résonance magnétique</term><term>Température</term><term>Xylanes ()</term><term>Xylanes (métabolisme)</term></keywords><keywords scheme="MESH" type="chemical" qualifier="chemistry" xml:lang="en"><term>Biopolymers</term><term>Cellulose</term><term>Lignin</term><term>Minerals</term><term>Xylans</term></keywords><keywords scheme="MESH" type="chemical" qualifier="metabolism" xml:lang="en"><term>Biopolymers</term><term>Cellulose</term><term>Lignin</term><term>Minerals</term><term>Xylans</term></keywords><keywords scheme="MESH" qualifier="chemistry" xml:lang="en"><term>Poaceae</term></keywords><keywords scheme="MESH" qualifier="métabolisme" xml:lang="fr"><term>Biopolymères</term><term>Cellulose</term><term>Lignine</term><term>Minéraux</term><term>Xylanes</term></keywords><keywords scheme="Teeft" xml:lang="en"><term>Anal</term><term>Angew</term><term>Appl</term><term>Biomass</term><term>Biomass pyrolysis</term><term>Cellulose</term><term>Cellulose pyrolysis</term><term>Chem</term><term>Chemsuschem</term><term>Energy fuels</term><term>Extraction procedure</term><term>First time</term><term>Fluidity</term><term>Fluidity development</term><term>Glass transition phase</term><term>Gmbh</term><term>Heating rate</term><term>Holocelluloses</term><term>Kgaa</term><term>Lignin</term><term>Lorentzian</term><term>Lower temperature</term><term>Magnetic Resonance Spectroscopy</term><term>Mass loss</term><term>Maximum fluidity</term><term>Maximum mass loss rate</term><term>Maximum weight loss</term><term>Microgranular cellulose</term><term>Miscanthus</term><term>Miscanthus cellulose</term><term>Mobile hydrogen fraction</term><term>Mobile phase</term><term>Mobility</term><term>Mobility development</term><term>Molecular mobility</term><term>Native biomass network</term><term>Native miscanthus</term><term>Native network</term><term>Polym</term><term>Polymer</term><term>Proton</term><term>Protons</term><term>Pyrolysis</term><term>Pyrolysis products</term><term>Relaxation time</term><term>Snape</term><term>Synthetic blend</term><term>Temperature</term><term>Thermogravimetric analysis</term><term>Verlag</term><term>Verlag gmbh</term><term>Weinheim</term><term>Weinheim chemsuschem</term><term>Xylan</term><term>Xylan pyrolysis</term></keywords><keywords scheme="Wicri" type="topic" xml:lang="fr"><term>Biomasse</term><term>Biopolymères</term><term>Cellulose</term><term>Lignine</term><term>Minéraux</term><term>Poaceae</term><term>Polymère</term><term>Protons</term><term>Spectroscopie par résonance magnétique</term><term>Température</term><term>Xylanes</term></keywords><keywords scheme="mix" xml:lang="en"><term>CELL-WALL</term><term>CELLULOSE PYROLYSIS</term><term>CO-PYROLYSIS</term><term>KINETICS</term><term>MAGNETIC-RESONANCE</term><term>RADIANT FLASH PYROLYSIS</term><term>TEMPERATURE H-1-NMR</term><term>THERMAL-DECOMPOSITION</term><term>THERMOGRAVIMETRY MASS-SPECTROMETRY</term><term>WOOD PYROLYSIS</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">The thermochemical conversion of lignocellulosic biomass feedstocks offers an important potential route for the production of biofuels and value‐added green chemicals. Pyrolysis is the first phenomenon involved in all biomass thermochemical processes and it controls to a major extent the product composition. The composition of pyrolysis products can be affected markedly by the extent of softening that occurs. In spite of extensive work on biomass pyrolysis, the development of fluidity during the pyrolysis of biomass has not been quantified. This paper provides the first experimental investigation of proton mobility during biomass pyrolysis by in situ 1H NMR spectroscopy. The origin of mobility is discussed for cellulose, lignin and xylan. The effect of minerals on cellulose mobility is also investigated. Interactions between polymers in the native biomass network are revealed by in situ 1H NMR analysis.</div></front></TEI><affiliations><list><country><li>France</li><li>Royaume-Uni</li></country><region><li>Angleterre</li><li>Grand Est</li><li>Lorraine (région)</li><li>Nottinghamshire</li></region><settlement><li>Nancy</li><li>Nottingham</li></settlement><orgName><li>Centre national de la recherche scientifique</li><li>Laboratoire réactions et génie des procédés</li><li>Nancy-Université</li><li>Université de Lorraine</li><li>Université de Nottingham</li></orgName></list><tree><country name="France"><region name="Grand Est"><name sortKey="Dufour, Anthony" sort="Dufour, Anthony" uniqKey="Dufour A" first="Anthony" last="Dufour">Anthony Dufour (génie des procédés)</name></region><name sortKey="Bouroukba, Mohamed" sort="Bouroukba, Mohamed" uniqKey="Bouroukba M" first="Mohamed" last="Bouroukba">Mohamed Bouroukba</name><name sortKey="Brosse, Nicolas" sort="Brosse, Nicolas" uniqKey="Brosse N" first="Nicolas" last="Brosse">Nicolas Brosse</name><name sortKey="Dufour, Anthony" sort="Dufour, Anthony" uniqKey="Dufour A" first="Anthony" last="Dufour">Anthony Dufour (génie des procédés)</name></country><country name="Royaume-Uni"><region name="Angleterre"><name sortKey="Dufour, Anthony" sort="Dufour, Anthony" uniqKey="Dufour A" first="Anthony" last="Dufour">Anthony Dufour (génie des procédés)</name></region><name sortKey="Castro Iaz, Miguel" sort="Castro Iaz, Miguel" uniqKey="Castro Iaz M" first="Miguel" last="Castro-Diaz">Miguel Castro-Diaz</name><name sortKey="Snape, Colin" sort="Snape, Colin" uniqKey="Snape C" first="Colin" last="Snape">Colin Snape</name><name sortKey="Snape, Colin" sort="Snape, Colin" uniqKey="Snape C" first="Colin" last="Snape">Colin Snape</name><name sortKey="Snape, Colin" sort="Snape, Colin" uniqKey="Snape C" first="Colin" last="Snape">Colin Snape</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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