Intensification principle of a new three-phase catalytic slurry reactor. Part I: Performance characterisation
Identifieur interne : 000542 ( Main/Curation ); précédent : 000541; suivant : 000543Intensification principle of a new three-phase catalytic slurry reactor. Part I: Performance characterisation
Auteurs : Stephan Machefer ; Laurent Falk [France] ; Fabrice PanthouSource :
- Chemical Engineering and Processing: Process Intensification [ 0255-2701 ] ; 2013-08.
Abstract
This paper presents the concept and the performances of a mini horizontal stirred tank reactor, used for hydrogenation reaction. A simple analytical model based on characteristic times of heat and mass transfer illustrates the intensification principle and shows that the relevant intensification parameter is the mass to heat transfer characteristics times ratio. The proof of concept is made through a small scale reactor named RAPTOR (R) (French acronym for Reactor with Polyvalent Rectilinear Stirred Reactor with Optimised Transfer). The mass transfer performances are measured and compared to conventional stirred tank reactor and other multiple impeller continuous reactors. In a following second paper, a comparative study is proposed to evaluate the eco-efficiency and the techno-economic advantages of a continuous process involving a RAPTOR (R) versus a classical batch process based on a stirred reactor.
Url:
DOI: 10.1016/j.cep.2013.04.014
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<sourceDesc><biblStruct><analytic><title xml:lang="en">Intensification principle of a new three-phase catalytic slurry reactor. Part II: Eco-efficiency and techno-economic performances</title>
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<author><name sortKey="Falk, Laurent" sort="Falk, Laurent" uniqKey="Falk L" first="Laurent" last="Falk">Laurent Falk</name>
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<front><div type="abstract" xml:lang="en">In two papers, the concept and the performances of a new continuous intensified reactor named RAPTOR (R) (French acronym for Reactor with Polyvalent Rectilinear Stirred Reactor with Optimised Transfer) are presented. Based on flow, heat and mass transfer characterisations and real hydrogenation experiments, Paper I presented a simple analytical model based on characteristic times that enables to explain the intensified performances compared with a semi-batch stirred reactor and to generalise the operability, rapidity and the flexibility of this minireactor. In Paper II (this article), the model is used to evaluate in a comparative study the eco-efficiency and the techno-economical advantages of a continuous process involving a RAPTOR (R) versus a classical batch process equipped with a stirred reactor. Economical, environmental aspects are considered as well as productivity, safety and process control.</div>
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