IndiumV3, Russie, Analysis, bibRecord, 000813

Metal sulfide synthesis by self-propagating combustion of sulfur-containing complexes

Identifieur interne : 000813 ( Russie/Analysis ); précédent : 000812; suivant : 000814

Metal sulfide synthesis by self-propagating combustion of sulfur-containing complexes

Auteurs : RBID : Pascal:03-0031514

Descripteurs français

Pascal (Inist)
- Métal transition Composé, Cadmium II Sulfure, Zinc II Sulfure, Bismuth III Sulfure, Indium III Sulfure, Préparation chimique, Combustion autopropagée, Synthèse combustion, Coordinat organique, Métal Complexe, Thiourée, Métal Nitrate, Poudre, Etude expérimentale, CdS, ZnS, Bi2S3, In2S3.

English descriptors

KwdEn :
- Bismuth III Sulfides, Cadmium II Sulfides, Chemical preparation, Combustion synthesis, Experimental study, Indium III Sulfides, Metal Complexes, Metal Nitrates, Organic ligand, Powder, Self propagating high temperature synthesis, Thiourea, Transition metal Compounds, Zinc II Sulfides.

Abstract

Coordination compounds of thiourea with cadmium(II), zinc(II), bismuth(III), and indium(III) nitrates were synthesized. The self-sustained combustion of these complexes, as well as that of thiosemicarbazide coordination compounds of nickel(II), cobalt(II), iron(II), copper(II), lead(II), and zinc(II) nitrates, was studied in an inert atmosphere. All these compounds burn to yield metal sulfides. The particle size and morphology of the product depend on the pressure at which the process is carried out. For cadmium(II) and zinc(II) sulfides, which are capable of subliming at the combustion temperatures of their precursors, these parameters can be varied in wide ranges.

Links toward previous steps (curation, corpus...)

to stream Main, to step Corpus: 00E058
to stream Main, to step Repository: 00EF24
to stream Russie, to step Extraction: 000813

Links to Exploration step

Pascal:03-0031514

Le document en format XML

<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en" level="a">Metal sulfide synthesis by self-propagating combustion of sulfur-containing complexes</title>
<author><name sortKey="Tukhtaev, R K" uniqKey="Tukhtaev R">R. K. Tukhtaev</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Institute of Solid-State Chemistry and Mechanochemistry, Siberian Division, Russian Academy of Sciences, ul. Kutateladze 18</s1>
<s2>Novosibirsk, 630128</s2>
<s3>RUS</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
</inist:fA14>
<country>Russie</country>
<wicri:noRegion>Novosibirsk, 630128</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Boldyrev, V V" uniqKey="Boldyrev V">V. V. Boldyrev</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Institute of Solid-State Chemistry and Mechanochemistry, Siberian Division, Russian Academy of Sciences, ul. Kutateladze 18</s1>
<s2>Novosibirsk, 630128</s2>
<s3>RUS</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
</inist:fA14>
<country>Russie</country>
<wicri:noRegion>Novosibirsk, 630128</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Gavrilov, A I" uniqKey="Gavrilov A">A. I. Gavrilov</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Institute of Solid-State Chemistry and Mechanochemistry, Siberian Division, Russian Academy of Sciences, ul. Kutateladze 18</s1>
<s2>Novosibirsk, 630128</s2>
<s3>RUS</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
</inist:fA14>
<country>Russie</country>
<wicri:noRegion>Novosibirsk, 630128</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Larionov, S V" uniqKey="Larionov S">S. V. Larionov</name>
<affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Institute of Inorganic Chemistry, Siberian Division, Russian Academy of Sciences, pr. Akademika Lavrent'eva 3</s1>
<s2>Novosibirsk, 630090</s2>
<s3>RUS</s3>
<sZ>4 aut.</sZ>
<sZ>5 aut.</sZ>
<sZ>6 aut.</sZ>
</inist:fA14>
<country>Russie</country>
<wicri:noRegion>Novosibirsk, 630090</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Myachina, L I" uniqKey="Myachina L">L. I. Myachina</name>
<affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Institute of Inorganic Chemistry, Siberian Division, Russian Academy of Sciences, pr. Akademika Lavrent'eva 3</s1>
<s2>Novosibirsk, 630090</s2>
<s3>RUS</s3>
<sZ>4 aut.</sZ>
<sZ>5 aut.</sZ>
<sZ>6 aut.</sZ>
</inist:fA14>
<country>Russie</country>
<wicri:noRegion>Novosibirsk, 630090</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Savel Eva, Z A" uniqKey="Savel Eva Z">Z. A. Savel Eva</name>
<affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Institute of Inorganic Chemistry, Siberian Division, Russian Academy of Sciences, pr. Akademika Lavrent'eva 3</s1>
<s2>Novosibirsk, 630090</s2>
<s3>RUS</s3>
<sZ>4 aut.</sZ>
<sZ>5 aut.</sZ>
<sZ>6 aut.</sZ>
</inist:fA14>
<country>Russie</country>
<wicri:noRegion>Novosibirsk, 630090</wicri:noRegion>
</affiliation>
</author>
</titleStmt>
<publicationStmt><idno type="inist">03-0031514</idno>
<date when="2002">2002</date>
<idno type="stanalyst">PASCAL 03-0031514 INIST</idno>
<idno type="RBID">Pascal:03-0031514</idno>
<idno type="wicri:Area/Main/Corpus">00E058</idno>
<idno type="wicri:Area/Main/Repository">00EF24</idno>
<idno type="wicri:Area/Russie/Extraction">000813</idno>
</publicationStmt>
<seriesStmt><idno type="ISSN">0020-1685</idno>
<title level="j" type="abbreviated">Inorg. mater.</title>
<title level="j" type="main">Inorganic materials</title>
</seriesStmt>
</fileDesc>
<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Bismuth III Sulfides</term>
<term>Cadmium II Sulfides</term>
<term>Chemical preparation</term>
<term>Combustion synthesis</term>
<term>Experimental study</term>
<term>Indium III Sulfides</term>
<term>Metal Complexes</term>
<term>Metal Nitrates</term>
<term>Organic ligand</term>
<term>Powder</term>
<term>Self propagating high temperature synthesis</term>
<term>Thiourea</term>
<term>Transition metal Compounds</term>
<term>Zinc II Sulfides</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Métal transition Composé</term>
<term>Cadmium II Sulfure</term>
<term>Zinc II Sulfure</term>
<term>Bismuth III Sulfure</term>
<term>Indium III Sulfure</term>
<term>Préparation chimique</term>
<term>Combustion autopropagée</term>
<term>Synthèse combustion</term>
<term>Coordinat organique</term>
<term>Métal Complexe</term>
<term>Thiourée</term>
<term>Métal Nitrate</term>
<term>Poudre</term>
<term>Etude expérimentale</term>
<term>CdS</term>
<term>ZnS</term>
<term>Bi2S3</term>
<term>In2S3</term>
</keywords>
</textClass>
</profileDesc>
</teiHeader>
<front><div type="abstract" xml:lang="en">Coordination compounds of thiourea with cadmium(II), zinc(II), bismuth(III), and indium(III) nitrates were synthesized. The self-sustained combustion of these complexes, as well as that of thiosemicarbazide coordination compounds of nickel(II), cobalt(II), iron(II), copper(II), lead(II), and zinc(II) nitrates, was studied in an inert atmosphere. All these compounds burn to yield metal sulfides. The particle size and morphology of the product depend on the pressure at which the process is carried out. For cadmium(II) and zinc(II) sulfides, which are capable of subliming at the combustion temperatures of their precursors, these parameters can be varied in wide ranges.</div>
</front>
</TEI>
<inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>0020-1685</s0>
</fA01>
<fA02 i1="01"><s0>INOMAF</s0>
</fA02>
<fA03 i2="1"><s0>Inorg. mater.</s0>
</fA03>
<fA05><s2>38</s2>
</fA05>
<fA06><s2>10</s2>
</fA06>
<fA08 i1="01" i2="1" l="ENG"><s1>Metal sulfide synthesis by self-propagating combustion of sulfur-containing complexes</s1>
</fA08>
<fA11 i1="01" i2="1"><s1>TUKHTAEV (R. K.)</s1>
</fA11>
<fA11 i1="02" i2="1"><s1>BOLDYREV (V. V.)</s1>
</fA11>
<fA11 i1="03" i2="1"><s1>GAVRILOV (A. I.)</s1>
</fA11>
<fA11 i1="04" i2="1"><s1>LARIONOV (S. V.)</s1>
</fA11>
<fA11 i1="05" i2="1"><s1>MYACHINA (L. I.)</s1>
</fA11>
<fA11 i1="06" i2="1"><s1>SAVEL'EVA (Z. A.)</s1>
</fA11>
<fA14 i1="01"><s1>Institute of Solid-State Chemistry and Mechanochemistry, Siberian Division, Russian Academy of Sciences, ul. Kutateladze 18</s1>
<s2>Novosibirsk, 630128</s2>
<s3>RUS</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
</fA14>
<fA14 i1="02"><s1>Institute of Inorganic Chemistry, Siberian Division, Russian Academy of Sciences, pr. Akademika Lavrent'eva 3</s1>
<s2>Novosibirsk, 630090</s2>
<s3>RUS</s3>
<sZ>4 aut.</sZ>
<sZ>5 aut.</sZ>
<sZ>6 aut.</sZ>
</fA14>
<fA20><s1>985-991</s1>
</fA20>
<fA21><s1>2002</s1>
</fA21>
<fA23 i1="01"><s0>ENG</s0>
</fA23>
<fA43 i1="01"><s1>INIST</s1>
<s2>12674</s2>
<s5>354000105431070020</s5>
</fA43>
<fA44><s0>0000</s0>
<s1>© 2003 INIST-CNRS. All rights reserved.</s1>
</fA44>
<fA45><s0>18 ref.</s0>
</fA45>
<fA47 i1="01" i2="1"><s0>03-0031514</s0>
</fA47>
<fA60><s1>P</s1>
<s3>V</s3>
</fA60>
<fA61><s0>A</s0>
</fA61>
<fA64 i1="01" i2="1"><s0>Inorganic materials</s0>
</fA64>
<fA66 i1="01"><s0>USA</s0>
</fA66>
<fA99><s0>Trad. de Neorganicheskie Materialy, RU, 2002, 38, 10,  1173-1180</s0>
</fA99>
<fC01 i1="01" l="ENG"><s0>Coordination compounds of thiourea with cadmium(II), zinc(II), bismuth(III), and indium(III) nitrates were synthesized. The self-sustained combustion of these complexes, as well as that of thiosemicarbazide coordination compounds of nickel(II), cobalt(II), iron(II), copper(II), lead(II), and zinc(II) nitrates, was studied in an inert atmosphere. All these compounds burn to yield metal sulfides. The particle size and morphology of the product depend on the pressure at which the process is carried out. For cadmium(II) and zinc(II) sulfides, which are capable of subliming at the combustion temperatures of their precursors, these parameters can be varied in wide ranges.</s0>
</fC01>
<fC02 i1="01" i2="X"><s0>001C02B01</s0>
</fC02>
<fC03 i1="01" i2="X" l="FRE"><s0>Métal transition Composé</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="X" l="ENG"><s0>Transition metal Compounds</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="X" l="SPA"><s0>Metal transición Compuesto</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>01</s5>
</fC03>
<fC03 i1="02" i2="X" l="FRE"><s0>Cadmium II Sulfure</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>02</s5>
<s6>Cadmium «II» Sulfure</s6>
</fC03>
<fC03 i1="02" i2="X" l="ENG"><s0>Cadmium II Sulfides</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>02</s5>
<s6>Cadmium «II» Sulfides</s6>
</fC03>
<fC03 i1="02" i2="X" l="SPA"><s0>Cadmio II Sulfuro</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>02</s5>
<s6>Cadmio «II» Sulfuro</s6>
</fC03>
<fC03 i1="03" i2="X" l="FRE"><s0>Zinc II Sulfure</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>03</s5>
<s6>Zinc «II» Sulfure</s6>
</fC03>
<fC03 i1="03" i2="X" l="ENG"><s0>Zinc II Sulfides</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>03</s5>
<s6>Zinc «II» Sulfides</s6>
</fC03>
<fC03 i1="03" i2="X" l="SPA"><s0>Zinc II Sulfuro</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>03</s5>
<s6>Zinc «II» Sulfuro</s6>
</fC03>
<fC03 i1="04" i2="X" l="FRE"><s0>Bismuth III Sulfure</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>04</s5>
<s6>Bismuth «III» Sulfure</s6>
</fC03>
<fC03 i1="04" i2="X" l="ENG"><s0>Bismuth III Sulfides</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>04</s5>
<s6>Bismuth «III» Sulfides</s6>
</fC03>
<fC03 i1="04" i2="X" l="SPA"><s0>Bismuto III Sulfuro</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>04</s5>
<s6>Bismuto «III» Sulfuro</s6>
</fC03>
<fC03 i1="05" i2="X" l="FRE"><s0>Indium III Sulfure</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>05</s5>
<s6>Indium «III» Sulfure</s6>
</fC03>
<fC03 i1="05" i2="X" l="ENG"><s0>Indium III Sulfides</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>05</s5>
<s6>Indium «III» Sulfides</s6>
</fC03>
<fC03 i1="05" i2="X" l="SPA"><s0>Indio III Sulfuro</s0>
<s1>FIN</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>05</s5>
<s6>Indio «III» Sulfuro</s6>
</fC03>
<fC03 i1="06" i2="3" l="FRE"><s0>Préparation chimique</s0>
<s5>06</s5>
<s6>Préparation chimique</s6>
</fC03>
<fC03 i1="06" i2="3" l="ENG"><s0>Chemical preparation</s0>
<s5>06</s5>
<s6>Chemical preparation</s6>
</fC03>
<fC03 i1="07" i2="3" l="FRE"><s0>Combustion autopropagée</s0>
<s5>07</s5>
<s6>Combustion autopropagée</s6>
</fC03>
<fC03 i1="07" i2="3" l="ENG"><s0>Self propagating high temperature synthesis</s0>
<s5>07</s5>
<s6>Self propagating high temperature synthesis</s6>
</fC03>
<fC03 i1="08" i2="3" l="FRE"><s0>Synthèse combustion</s0>
<s5>08</s5>
<s6>Synthèse combustion</s6>
</fC03>
<fC03 i1="08" i2="3" l="ENG"><s0>Combustion synthesis</s0>
<s5>08</s5>
<s6>Combustion synthesis</s6>
</fC03>
<fC03 i1="09" i2="X" l="FRE"><s0>Coordinat organique</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="ENG"><s0>Organic ligand</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="SPA"><s0>Ligando orgánico</s0>
<s5>09</s5>
</fC03>
<fC03 i1="10" i2="X" l="FRE"><s0>Métal Complexe</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="ENG"><s0>Metal Complexes</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="SPA"><s0>Metal Complejo</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>10</s5>
</fC03>
<fC03 i1="11" i2="X" l="FRE"><s0>Thiourée</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="ENG"><s0>Thiourea</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="SPA"><s0>Tiourea</s0>
<s5>11</s5>
</fC03>
<fC03 i1="12" i2="X" l="FRE"><s0>Métal Nitrate</s0>
<s2>NC</s2>
<s2>NA</s2>
<s2>FX</s2>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="ENG"><s0>Metal Nitrates</s0>
<s2>NC</s2>
<s2>NA</s2>
<s2>FX</s2>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="SPA"><s0>Metal Nitrato</s0>
<s2>NC</s2>
<s2>NA</s2>
<s2>FX</s2>
<s5>12</s5>
</fC03>
<fC03 i1="13" i2="X" l="FRE"><s0>Poudre</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="X" l="ENG"><s0>Powder</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="X" l="SPA"><s0>Polvo</s0>
<s5>13</s5>
</fC03>
<fC03 i1="14" i2="X" l="FRE"><s0>Etude expérimentale</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="X" l="ENG"><s0>Experimental study</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="X" l="SPA"><s0>Estudio experimental</s0>
<s5>14</s5>
</fC03>
<fC03 i1="15" i2="X" l="FRE"><s0>CdS</s0>
<s1>FIN</s1>
<s4>INC</s4>
<s5>32</s5>
</fC03>
<fC03 i1="16" i2="X" l="FRE"><s0>ZnS</s0>
<s1>FIN</s1>
<s4>INC</s4>
<s5>33</s5>
</fC03>
<fC03 i1="17" i2="X" l="FRE"><s0>Bi2S3</s0>
<s1>FIN</s1>
<s4>INC</s4>
<s5>34</s5>
</fC03>
<fC03 i1="18" i2="X" l="FRE"><s0>In2S3</s0>
<s1>FIN</s1>
<s4>INC</s4>
<s5>35</s5>
</fC03>
<fN21><s1>013</s1>
</fN21>
<fN82><s1>PSI</s1>
</fN82>
</pA>
</standard>
</inist>
</record>

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Metal sulfide synthesis by self-propagating combustion of sulfur-containing complexes

Metal sulfide synthesis by self-propagating combustion of sulfur-containing complexes

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