Facile synthesis of AgInS₂ hierarchical flowerlike nanoarchitectures composed of ultrathin nanowires.
Identifieur interne : 000697 ( Main/Exploration ); précédent : 000696; suivant : 000698Facile synthesis of AgInS₂ hierarchical flowerlike nanoarchitectures composed of ultrathin nanowires.
Auteurs : RBID : pubmed:23329060English descriptors
- KwdEn :
- MESH :
- chemical , chemical synthesis : Silver Compounds.
- chemical , chemistry : Macromolecular Substances.
- chemical : Indium.
- chemistry : Nanostructures.
- methods : Crystallization.
- ultrastructure : Nanostructures.
- Materials Testing, Molecular Conformation, Particle Size, Surface Properties.
Abstract
In this work, AgInS(2) hierarchical flowerlike nanoarchitectures, which are composed of ultrathin nanowires, were synthesized by thermolysis of a mixed solution of AgNO(3), InCl(3)·4H(2)O and n-dodecanethiol at elevated temperature. The average diameter and length of the nanowires composing the nanoarchitectures can reach 5 nm and ∼300 nm, respectively. We investigated the growth process of the nanoarchitectures and the effects of reaction parameters by XRD, SEM and TEM. In particular, the use of InCl(3)·4H(2)O played a decisive role in the synthesis of the nanoarchitectures. Moreover, it was found that polyhedra formed in the initial reaction time, and then the nanowires grew on the facets of these polyhedra, which resulted in the nanoarchitectures. The reaction temperature and the concentration of metal salts could influence the size of the nanowires.
DOI: 10.1039/c2nr33219a
PubMed: 23329060
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Facile synthesis of AgInS₂ hierarchical flowerlike nanoarchitectures composed of ultrathin nanowires.</title><author><name sortKey="Liu, Zhongping" uniqKey="Liu Z">Zhongping Liu</name><affiliation wicri:level="1"><nlm:affiliation>Division of Nanomaterials and Chemistry, Hefei National Laboratory for Physical Sciences at Microscale, Department of Chemistry, University of Science and Technology of China, Hefei, 230026, PR China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>Division of Nanomaterials and Chemistry, Hefei National Laboratory for Physical Sciences at Microscale, Department of Chemistry, University of Science and Technology of China, Hefei, 230026</wicri:regionArea></affiliation></author><author><name sortKey="Tang, Kaibin" uniqKey="Tang K">Kaibin Tang</name></author><author><name sortKey="Wang, Dake" uniqKey="Wang D">Dake Wang</name></author><author><name sortKey="Wang, Linlin" uniqKey="Wang L">Linlin Wang</name></author><author><name sortKey="Hao, Qiaoyan" uniqKey="Hao Q">Qiaoyan Hao</name></author></titleStmt><publicationStmt><date when="2013">2013</date><idno type="doi">10.1039/c2nr33219a</idno><idno type="RBID">pubmed:23329060</idno><idno type="pmid">23329060</idno><idno type="wicri:Area/Main/Corpus">000845</idno><idno type="wicri:Area/Main/Curation">000845</idno><idno type="wicri:Area/Main/Exploration">000697</idno></publicationStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Crystallization (methods)</term><term>Indium</term><term>Macromolecular Substances (chemistry)</term><term>Materials Testing</term><term>Molecular Conformation</term><term>Nanostructures (chemistry)</term><term>Nanostructures (ultrastructure)</term><term>Particle Size</term><term>Silver Compounds (chemical synthesis)</term><term>Surface Properties</term></keywords><keywords scheme="MESH" type="chemical" qualifier="chemical synthesis" xml:lang="en"><term>Silver Compounds</term></keywords><keywords scheme="MESH" type="chemical" qualifier="chemistry" xml:lang="en"><term>Macromolecular Substances</term></keywords><keywords scheme="MESH" type="chemical" xml:lang="en"><term>Indium</term></keywords><keywords scheme="MESH" qualifier="chemistry" xml:lang="en"><term>Nanostructures</term></keywords><keywords scheme="MESH" qualifier="methods" xml:lang="en"><term>Crystallization</term></keywords><keywords scheme="MESH" qualifier="ultrastructure" xml:lang="en"><term>Nanostructures</term></keywords><keywords scheme="MESH" xml:lang="en"><term>Materials Testing</term><term>Molecular Conformation</term><term>Particle Size</term><term>Surface Properties</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">In this work, AgInS(2) hierarchical flowerlike nanoarchitectures, which are composed of ultrathin nanowires, were synthesized by thermolysis of a mixed solution of AgNO(3), InCl(3)·4H(2)O and n-dodecanethiol at elevated temperature. The average diameter and length of the nanowires composing the nanoarchitectures can reach 5 nm and ∼300 nm, respectively. We investigated the growth process of the nanoarchitectures and the effects of reaction parameters by XRD, SEM and TEM. In particular, the use of InCl(3)·4H(2)O played a decisive role in the synthesis of the nanoarchitectures. Moreover, it was found that polyhedra formed in the initial reaction time, and then the nanowires grew on the facets of these polyhedra, which resulted in the nanoarchitectures. The reaction temperature and the concentration of metal salts could influence the size of the nanowires.</div></front></TEI><pubmed><MedlineCitation Owner="NLM" Status="MEDLINE"><PMID Version="1">23329060</PMID><DateCreated><Year>2013</Year><Month>02</Month><Day>04</Day></DateCreated><DateCompleted><Year>2013</Year><Month>07</Month><Day>16</Day></DateCompleted><DateRevised><Year>2013</Year><Month>11</Month><Day>21</Day></DateRevised><Article PubModel="Print"><Journal><ISSN IssnType="Electronic">2040-3372</ISSN><JournalIssue CitedMedium="Internet"><Volume>5</Volume><Issue>4</Issue><PubDate><Year>2013</Year><Month>Feb</Month><Day>21</Day></PubDate></JournalIssue><Title>Nanoscale</Title><ISOAbbreviation>Nanoscale</ISOAbbreviation></Journal><ArticleTitle>Facile synthesis of AgInS₂ hierarchical flowerlike nanoarchitectures composed of ultrathin nanowires.</ArticleTitle><Pagination><MedlinePgn>1570-5</MedlinePgn></Pagination><ELocationID EIdType="doi" ValidYN="Y">10.1039/c2nr33219a</ELocationID><Abstract><AbstractText>In this work, AgInS(2) hierarchical flowerlike nanoarchitectures, which are composed of ultrathin nanowires, were synthesized by thermolysis of a mixed solution of AgNO(3), InCl(3)·4H(2)O and n-dodecanethiol at elevated temperature. The average diameter and length of the nanowires composing the nanoarchitectures can reach 5 nm and ∼300 nm, respectively. We investigated the growth process of the nanoarchitectures and the effects of reaction parameters by XRD, SEM and TEM. In particular, the use of InCl(3)·4H(2)O played a decisive role in the synthesis of the nanoarchitectures. Moreover, it was found that polyhedra formed in the initial reaction time, and then the nanowires grew on the facets of these polyhedra, which resulted in the nanoarchitectures. The reaction temperature and the concentration of metal salts could influence the size of the nanowires.</AbstractText></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Liu</LastName><ForeName>Zhongping</ForeName><Initials>Z</Initials><Affiliation>Division of Nanomaterials and Chemistry, Hefei National Laboratory for Physical Sciences at Microscale, Department of Chemistry, University of Science and Technology of China, Hefei, 230026, PR China.</Affiliation></Author><Author ValidYN="Y"><LastName>Tang</LastName><ForeName>Kaibin</ForeName><Initials>K</Initials></Author><Author ValidYN="Y"><LastName>Wang</LastName><ForeName>Dake</ForeName><Initials>D</Initials></Author><Author ValidYN="Y"><LastName>Wang</LastName><ForeName>Linlin</ForeName><Initials>L</Initials></Author><Author ValidYN="Y"><LastName>Hao</LastName><ForeName>Qiaoyan</ForeName><Initials>Q</Initials></Author></AuthorList><Language>eng</Language><PublicationTypeList><PublicationType>Journal Article</PublicationType><PublicationType>Research Support, Non-U.S. Gov't</PublicationType></PublicationTypeList></Article><MedlineJournalInfo><Country>England</Country><MedlineTA>Nanoscale</MedlineTA><NlmUniqueID>101525249</NlmUniqueID><ISSNLinking>2040-3364</ISSNLinking></MedlineJournalInfo><ChemicalList><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance>Macromolecular Substances</NameOfSubstance></Chemical><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance>Silver Compounds</NameOfSubstance></Chemical><Chemical><RegistryNumber>045A6V3VFX</RegistryNumber><NameOfSubstance>Indium</NameOfSubstance></Chemical><Chemical><RegistryNumber>9ZB10YHC1C</RegistryNumber><NameOfSubstance>silver sulfide</NameOfSubstance></Chemical></ChemicalList><CitationSubset>IM</CitationSubset><MeshHeadingList><MeshHeading><DescriptorName MajorTopicYN="N">Crystallization</DescriptorName><QualifierName MajorTopicYN="Y">methods</QualifierName></MeshHeading><MeshHeading><DescriptorName MajorTopicYN="N">Indium</DescriptorName></MeshHeading><MeshHeading><DescriptorName MajorTopicYN="N">Macromolecular Substances</DescriptorName><QualifierName MajorTopicYN="N">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName MajorTopicYN="N">Materials Testing</DescriptorName></MeshHeading><MeshHeading><DescriptorName MajorTopicYN="N">Molecular Conformation</DescriptorName></MeshHeading><MeshHeading><DescriptorName MajorTopicYN="N">Nanostructures</DescriptorName><QualifierName MajorTopicYN="Y">chemistry</QualifierName><QualifierName MajorTopicYN="Y">ultrastructure</QualifierName></MeshHeading><MeshHeading><DescriptorName MajorTopicYN="N">Particle Size</DescriptorName></MeshHeading><MeshHeading><DescriptorName MajorTopicYN="N">Silver Compounds</DescriptorName><QualifierName MajorTopicYN="Y">chemical synthesis</QualifierName></MeshHeading><MeshHeading><DescriptorName MajorTopicYN="N">Surface Properties</DescriptorName></MeshHeading></MeshHeadingList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="entrez"><Year>2013</Year><Month>1</Month><Day>19</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="pubmed"><Year>2013</Year><Month>1</Month><Day>19</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="medline"><Year>2013</Year><Month>7</Month><Day>17</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate></History><PublicationStatus>ppublish</PublicationStatus><ArticleIdList><ArticleId IdType="doi">10.1039/c2nr33219a</ArticleId><ArticleId IdType="pubmed">23329060</ArticleId></ArticleIdList></PubmedData></pubmed></record>Pour manipuler ce document sous Unix (Dilib)
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