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A systematic study of zone refining of single crystal indium antimonide

Identifieur interne : 000C62 ( Main/Exploration ); précédent : 000C61; suivant : 000C63

A systematic study of zone refining of single crystal indium antimonide

Auteurs : RBID : ISTEX:10853_1966_Article_BF00549717.pdf

Abstract

The experimental conditions have been determined whereby it is possible, in a closed system, to distil off volatile impurities from an ingot of InSb, and subsequently pass at least 10 to 15 zones through the ingot, whilst constantly maintaining a single crystal structure of a chosen crystallographic orientation. It has been found that preservation of singularity and control of dislocation density can be achieved by selection of: seed orientation and polarity; provision of a containing boat which is not wetted by InSb; careful purification of gas ambient; and the establishment of the correct conditions of temperature gradient at the crystal growing interface. A minimum concentration of ∼3×1013 extrinsic electrons/cm3 was found in uniform specimens substantially uncompensated by volatile impurities. The work provides good evidence that this carrier concentration is not due to Te. The maximum electron mobility at 77° K that could be reproducibly obtained in uniform specimens was 7.5×105 cm2/V sec.

DOI: 10.1007/BF00549717

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Le document en format XML

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