The identification of faulted prismatic dislocation loops in single crystals of undoped InP
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Auteurs : RBID : ISTEX:10853_1981_Article_BF00552972.pdfAbstract
High-voltage transmission electron microscopy has shown that undoped single crystals of indium phosphide, grown by the liquid-encapsulated Czochralski technique, can contain linear arrays of faulted dislocation loops. The plane of the loops is (1 1 0), the fault vector is 1/n [1 1 0] and the Burgers vector of the dislocation loop is 1/n [1 1 0]. A direct correlation has been obtained between these loops and arrays of both ridge and prism features revealed by chemical etching. Sequential use of two etchants has also established a direct link between the faulted dislocation loops and the slip dislocations induced by thermal stresses during crystal growth. A study of a number of crystals grown from differently prepared starting materials suggests that the formation of the loops is associated with departures from stoichiometry and inhibited by the presence of dopant impurities.
DOI: 10.1007/BF00552972
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<front><div type="abstract" xml:lang="eng">High-voltage transmission electron microscopy has shown that undoped single crystals of indium phosphide, grown by the liquid-encapsulated Czochralski technique, can contain linear arrays of faulted dislocation loops. The plane of the loops is (1 1 0), the fault vector is 1/n [1 1 0] and the Burgers vector of the dislocation loop is 1/n [1 1 0]. A direct correlation has been obtained between these loops and arrays of both ridge and prism features revealed by chemical etching. Sequential use of two etchants has also established a direct link between the faulted dislocation loops and the slip dislocations induced by thermal stresses during crystal growth. A study of a number of crystals grown from differently prepared starting materials suggests that the formation of the loops is associated with departures from stoichiometry and inhibited by the presence of dopant impurities.</div>
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<abstract lang="eng">High-voltage transmission electron microscopy has shown that undoped single crystals of indium phosphide, grown by the liquid-encapsulated Czochralski technique, can contain linear arrays of faulted dislocation loops. The plane of the loops is (1 1 0), the fault vector is 1/n [1 1 0] and the Burgers vector of the dislocation loop is 1/n [1 1 0]. A direct correlation has been obtained between these loops and arrays of both ridge and prism features revealed by chemical etching. Sequential use of two etchants has also established a direct link between the faulted dislocation loops and the slip dislocations induced by thermal stresses during crystal growth. A study of a number of crystals grown from differently prepared starting materials suggests that the formation of the loops is associated with departures from stoichiometry and inhibited by the presence of dopant impurities.</abstract>
<relatedItem type="series"><titleInfo type="abbreviated"><title>J Mater Sci</title>
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<titleInfo><title>Journal of Materials Science</title>
<partNumber>Year: 1981</partNumber>
<partNumber>Volume: 16</partNumber>
<partNumber>Number: 10</partNumber>
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<subject usage="primary"><topic>Chemistry</topic>
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<identifier type="issn">0022-2461</identifier>
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