CobaltMaghrebV1, PubMed, Corpus, bibRecord, 000011

Crystal structure of bis-(2-amino-5-chloro-pyridinium) tetra-chlorido-cobaltate(II).

Identifieur interne : 000011 ( PubMed/Corpus ); précédent : 000010; suivant : 000012

Crystal structure of bis-(2-amino-5-chloro-pyridinium) tetra-chlorido-cobaltate(II).

Auteurs : Marwa Mghandef ; Habib Boughzala

Source :

Acta crystallographica. Section E, Crystallographic communications ; 2015.

RBID : pubmed:25995878

Abstract

The title salt, (C5H6ClN2)2[CoCl4], was synthesized by slow evaporation of an aqueous solution at room temperature. The asymmetric unit consists of two essentially planar (C5H6ClN2)(+) cations [maximum deviations = 0.010 (3) and 0.014 (3) Å] that are nearly perpendicular to each other [dihedral angle = 84.12 (7)°]. They are bonded through N-H⋯Cl hydrogen bonds to distorted [CoCl4](2-) tetra-hedra, leading to the formation of undulating layers parallel to (100). The structure is isotypic with the Zn analogue [Kefi et. al (2011). Acta Cryst. E67, m355-m356.].

DOI: 10.1107/S2056989015007707
PubMed: 25995878

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<author><name sortKey="Boughzala, Habib" sort="Boughzala, Habib" uniqKey="Boughzala H" first="Habib" last="Boughzala">Habib Boughzala</name>
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<front><div type="abstract" xml:lang="en">The title salt, (C5H6ClN2)2[CoCl4], was synthesized by slow evaporation of an aqueous solution at room temperature. The asymmetric unit consists of two essentially planar (C5H6ClN2)(+) cations [maximum deviations = 0.010 (3) and 0.014 (3) Å] that are nearly perpendicular to each other [dihedral angle = 84.12 (7)°]. They are bonded through N-H⋯Cl hydrogen bonds to distorted [CoCl4](2-) tetra-hedra, leading to the formation of undulating layers parallel to (100). The structure is isotypic with the Zn analogue [Kefi et. al (2011). Acta Cryst. E67, m355-m356.].</div>
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<Abstract><AbstractText>The title salt, (C5H6ClN2)2[CoCl4], was synthesized by slow evaporation of an aqueous solution at room temperature. The asymmetric unit consists of two essentially planar (C5H6ClN2)(+) cations [maximum deviations = 0.010 (3) and 0.014 (3) Å] that are nearly perpendicular to each other [dihedral angle = 84.12 (7)°]. They are bonded through N-H⋯Cl hydrogen bonds to distorted [CoCl4](2-) tetra-hedra, leading to the formation of undulating layers parallel to (100). The structure is isotypic with the Zn analogue [Kefi et. al (2011). Acta Cryst. E67, m355-m356.].</AbstractText>
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<KeywordList Owner="NOTNLM"><Keyword MajorTopicYN="N">2-amino-5-chloropyridine</Keyword>
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Crystal structure of bis-(2-amino-5-chloro-pyridinium) tetra-chlorido-cobaltate(II).

Crystal structure of bis-(2-amino-5-chloro-pyridinium) tetra-chlorido-cobaltate(II).

Source :

Abstract

Links to Exploration step

Le document en format XML

Pour manipuler ce document sous Unix (Dilib)

Pour mettre un lien sur cette page dans le réseau Wicri

Pour générer des pages wiki