CobaltMaghrebV1, Pmc, Checkpoint, bibRecord, 000300

Tris(1,10-phenanthroline)cobalt(II) bis(perrhenate) monohydrate

Identifieur interne : 000300 ( Pmc/Checkpoint ); précédent : 000299; suivant : 000301

Tris(1,10-phenanthroline)cobalt(II) bis(perrhenate) monohydrate

Auteurs : Samah Toumi Akriche [Tunisie] ; Zeid Abdellah Al Othman [Arabie saoudite] ; Mohamed Rzaigui [Tunisie] ; Refaat Mohamed Mahfouz [Arabie saoudite]

Source :

Acta Crystallographica Section E: Structure Reports Online [ 1600-5368 ] ; 2010.

RBID : PMC:3006859

Abstract

In the title compound, [Co(C₁₂H₈N₂)₃][ReO₄]₂·H₂O, the Co^II atom is coordinated by three 1,10-phenanthroline ligands in a distorted octahedral arrangement. In the crystal, the components are linked by O—H⋯O, C—H⋯O and aromatic π–π stacking [shortest centroid–centroid separation = 3.659 (5) Å] interactions.

Url:

http://www.ncbi.nlm.nih.gov/pmc/articles/PMC3006859

DOI: 10.1107/S1600536810022750
PubMed: 21587733
PubMed Central: 3006859

Affiliations:

Arabie saoudite, Tunisie

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Le document en format XML

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<author><name sortKey="Toumi Akriche, Samah" sort="Toumi Akriche, Samah" uniqKey="Toumi Akriche S" first="Samah" last="Toumi Akriche">Samah Toumi Akriche</name>
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<country xml:lang="fr">Tunisie</country>
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<author><name sortKey="Al Othman, Zeid Abdellah" sort="Al Othman, Zeid Abdellah" uniqKey="Al Othman Z" first="Zeid Abdellah" last="Al Othman">Zeid Abdellah Al Othman</name>
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</nlm:aff>
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<author><name sortKey="Rzaigui, Mohamed" sort="Rzaigui, Mohamed" uniqKey="Rzaigui M" first="Mohamed" last="Rzaigui">Mohamed Rzaigui</name>
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<author><name sortKey="Mahfouz, Refaat Mohamed" sort="Mahfouz, Refaat Mohamed" uniqKey="Mahfouz R" first="Refaat Mohamed" last="Mahfouz">Refaat Mohamed Mahfouz</name>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Tris(1,10-phenanthroline)cobalt(II) bis(perrhenate) monohydrate</title>
<author><name sortKey="Toumi Akriche, Samah" sort="Toumi Akriche, Samah" uniqKey="Toumi Akriche S" first="Samah" last="Toumi Akriche">Samah Toumi Akriche</name>
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<author><name sortKey="Al Othman, Zeid Abdellah" sort="Al Othman, Zeid Abdellah" uniqKey="Al Othman Z" first="Zeid Abdellah" last="Al Othman">Zeid Abdellah Al Othman</name>
<affiliation wicri:level="1"><nlm:aff id="b">Chemistry Department, Faculty of Science, King Saud University, PO Box 2455, Riyadh 11451,<country>Saudi Arabia</country>
</nlm:aff>
<country xml:lang="fr">Arabie saoudite</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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<author><name sortKey="Rzaigui, Mohamed" sort="Rzaigui, Mohamed" uniqKey="Rzaigui M" first="Mohamed" last="Rzaigui">Mohamed Rzaigui</name>
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</nlm:aff>
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<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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<author><name sortKey="Mahfouz, Refaat Mohamed" sort="Mahfouz, Refaat Mohamed" uniqKey="Mahfouz R" first="Refaat Mohamed" last="Mahfouz">Refaat Mohamed Mahfouz</name>
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<series><title level="j">Acta Crystallographica Section E: Structure Reports Online</title>
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<front><div type="abstract" xml:lang="en"><p>In the title compound, [Co(C<sub>12</sub>
H<sub>8</sub>
N<sub>2</sub>
)<sub>3</sub>
][ReO<sub>4</sub>
]<sub>2</sub>
·H<sub>2</sub>
O, the Co<sup>II</sup>
 atom is coordinated by three 1,10-phenanthroline ligands in a distorted octahedral arrangement. In the crystal, the components are linked by O—H⋯O, C—H⋯O and aromatic π–π stacking [shortest centroid–centroid separation = 3.659 (5) Å] interactions.</p>
</div>
</front>
<back><div1 type="bibliography"><listBibl><biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
<biblStruct></biblStruct>
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<pmc article-type="research-article"><pmc-dir>properties open_access</pmc-dir>
  <front><journal-meta><journal-id journal-id-type="nlm-ta">Acta Crystallogr Sect E Struct Rep Online</journal-id>
<journal-id journal-id-type="publisher-id">Acta Cryst. E</journal-id>
<journal-title-group><journal-title>Acta Crystallographica Section E: Structure Reports Online</journal-title>
</journal-title-group>
<issn pub-type="epub">1600-5368</issn>
<publisher><publisher-name>International Union of Crystallography</publisher-name>
</publisher>
</journal-meta>
<article-meta><article-id pub-id-type="pmid">21587733</article-id>
<article-id pub-id-type="pmc">3006859</article-id>
<article-id pub-id-type="publisher-id">hb5497</article-id>
<article-id pub-id-type="doi">10.1107/S1600536810022750</article-id>
<article-id pub-id-type="coden">ACSEBH</article-id>
<article-id pub-id-type="pii">S1600536810022750</article-id>
<article-categories><subj-group subj-group-type="heading"><subject>Metal-Organic Papers</subject>
</subj-group>
</article-categories>
<title-group><article-title>Tris(1,10-phenanthroline)cobalt(II) bis(perrhenate) monohydrate</article-title>
<alt-title><italic>[Co(C<sub>12</sub>
H<sub>8</sub>
N<sub>2</sub>
)<sub>3</sub>
][ReO<sub>4</sub>
]<sub>2</sub>
·H<sub>2</sub>
O</italic>
</alt-title>
</title-group>
<contrib-group><contrib contrib-type="author"><name><surname>Toumi Akriche</surname>
<given-names>Samah</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
<xref ref-type="corresp" rid="cor">*</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Al Othman</surname>
<given-names>Zeid Abdellah</given-names>
</name>
<xref ref-type="aff" rid="b">b</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Rzaigui</surname>
<given-names>Mohamed</given-names>
</name>
<xref ref-type="aff" rid="a">a</xref>
</contrib>
<contrib contrib-type="author"><name><surname>Mahfouz</surname>
<given-names>Refaat Mohamed</given-names>
</name>
<xref ref-type="aff" rid="b">b</xref>
</contrib>
<aff id="a"><label>a</label>
Laboratoire de Chimie des Matériaux, Faculté des Sciences de Bizerte, 7021 Zarzouna Bizerte,<country>Tunisia</country>
</aff>
<aff id="b"><label>b</label>
Chemistry Department, Faculty of Science, King Saud University, PO Box 2455, Riyadh 11451,<country>Saudi Arabia</country>
</aff>
</contrib-group>
<author-notes><corresp id="cor">Correspondence e-mail: <email>toumiakriche@yahoo.fr</email>
</corresp>
</author-notes>
<pub-date pub-type="collection"><day>01</day>
<month>7</month>
<year>2010</year>
</pub-date>
<pub-date pub-type="epub"><day>18</day>
<month>6</month>
<year>2010</year>
</pub-date>
<pub-date pub-type="pmc-release"><day>18</day>
<month>6</month>
<year>2010</year>
</pub-date>
<pmc-comment> PMC Release delay is 0 months and 0 days and was based on the 
 							. </pmc-comment>
      <volume>66</volume>
<issue>Pt 7</issue>
<issue-id pub-id-type="publisher-id">e100700</issue-id>
<fpage>m816</fpage>
<lpage>m816</lpage>
<history><date date-type="received"><day>11</day>
<month>6</month>
<year>2010</year>
</date>
<date date-type="accepted"><day>13</day>
<month>6</month>
<year>2010</year>
</date>
</history>
<permissions><copyright-statement>© Toumi Akriche et al. 2010</copyright-statement>
<copyright-year>2010</copyright-year>
<license license-type="open-access" xlink:href="http://creativecommons.org/licenses/by/2.0/uk/"><license-p>This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.</license-p>
</license>
</permissions>
<self-uri xlink:type="simple" xlink:href="http://dx.doi.org/10.1107/S1600536810022750">A full version of this article is available from Crystallography Journals Online.</self-uri>
<abstract><p>In the title compound, [Co(C<sub>12</sub>
H<sub>8</sub>
N<sub>2</sub>
)<sub>3</sub>
][ReO<sub>4</sub>
]<sub>2</sub>
·H<sub>2</sub>
O, the Co<sup>II</sup>
 atom is coordinated by three 1,10-phenanthroline ligands in a distorted octahedral arrangement. In the crystal, the components are linked by O—H⋯O, C—H⋯O and aromatic π–π stacking [shortest centroid–centroid separation = 3.659 (5) Å] interactions.</p>
</abstract>
</article-meta>
</front>
<floats-group><table-wrap id="table1" position="float"><label>Table 1</label>
<caption><title>Selected bond lengths (Å)</title>
</caption>
<table frame="hsides" rules="groups"><tbody valign="top"><tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Re2—O7</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">1.549 (15)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Re2—O5</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">1.685 (8)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Re2—O6</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">1.708 (8)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Re2—O8</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">1.728 (8)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Re1—O3</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">1.688 (9)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Re1—O2</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">1.691 (9)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Re1—O1</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">1.700 (7)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Re1—O4</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">1.724 (10)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Co1—N6</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.122 (5)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Co1—N2</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.122 (5)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Co1—N1</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.136 (5)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Co1—N4</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.147 (5)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Co1—N3</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.148 (6)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">Co1—N5</td>
<td style="" rowspan="1" colspan="1" align="char" valign="top">2.151 (6)</td>
</tr>
</tbody>
</table>
</table-wrap>
<table-wrap id="table2" position="float"><label>Table 2</label>
<caption><title>Hydrogen-bond geometry (Å, °)</title>
</caption>
<table frame="hsides" rules="groups"><thead valign="bottom"><tr><th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom">H⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
⋯<italic>A</italic>
</th>
<th style="border-bottom:1px solid black;" rowspan="1" colspan="1" align="left" valign="bottom"><italic>D</italic>
—H⋯<italic>A</italic>
</th>
</tr>
</thead>
<tbody valign="top"><tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O9—H209⋯O1<sup>i</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.85 (10)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">1.99 (8)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.802 (13)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">157 (19)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">O9—H109⋯O8</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.86 (14)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.26 (17)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.953 (17)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">139 (23)</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">C15—H15⋯O9<sup>ii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.93</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.56</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">3.271 (14)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">134</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">C33—H33⋯O5<sup>iii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.93</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.51</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">3.116 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">123</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">C5—H5⋯O4<sup>iv</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.93</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.45</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">3.309 (13)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">154</td>
</tr>
<tr><td style="" rowspan="1" colspan="1" align="left" valign="top">C33—H33⋯O5<sup>iii</sup>
</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">0.93</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">2.51</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">3.116 (12)</td>
<td style="" rowspan="1" colspan="1" align="left" valign="top">123</td>
</tr>
</tbody>
</table>
<table-wrap-foot><p>Symmetry codes: (i) <inline-formula><inline-graphic xlink:href="e-66-0m816-efi2.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (ii) <inline-formula><inline-graphic xlink:href="e-66-0m816-efi3.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (iii) <inline-formula><inline-graphic xlink:href="e-66-0m816-efi4.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
; (iv) <inline-formula><inline-graphic xlink:href="e-66-0m816-efi5.jpg" mimetype="image" mime-subtype="gif"></inline-graphic>
</inline-formula>
.</p>
</table-wrap-foot>
</table-wrap>
</floats-group>
</pmc>
<affiliations><list><country><li>Arabie saoudite</li>
<li>Tunisie</li>
</country>
</list>
<tree><country name="Tunisie"><noRegion><name sortKey="Toumi Akriche, Samah" sort="Toumi Akriche, Samah" uniqKey="Toumi Akriche S" first="Samah" last="Toumi Akriche">Samah Toumi Akriche</name>
</noRegion>
<name sortKey="Rzaigui, Mohamed" sort="Rzaigui, Mohamed" uniqKey="Rzaigui M" first="Mohamed" last="Rzaigui">Mohamed Rzaigui</name>
</country>
<country name="Arabie saoudite"><noRegion><name sortKey="Al Othman, Zeid Abdellah" sort="Al Othman, Zeid Abdellah" uniqKey="Al Othman Z" first="Zeid Abdellah" last="Al Othman">Zeid Abdellah Al Othman</name>
</noRegion>
<name sortKey="Mahfouz, Refaat Mohamed" sort="Mahfouz, Refaat Mohamed" uniqKey="Mahfouz R" first="Refaat Mohamed" last="Mahfouz">Refaat Mohamed Mahfouz</name>
</country>
</tree>
</affiliations>
</record>

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Tris(1,10-phenanthroline)cobalt(II) bis­(perrhenate) monohydrate

Tris(1,10-phenanthroline)cobalt(II) bis­(perrhenate) monohydrate

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Tris(1,10-phenanthroline)cobalt(II) bis(perrhenate) monohydrate

Tris(1,10-phenanthroline)cobalt(II) bis(perrhenate) monohydrate