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Structure, sintering and electrical properties of new ionic conductor Ag4Co7(AsO4)6

Identifieur interne : 000286 ( PascalFrancis/Curation ); précédent : 000285; suivant : 000287

Structure, sintering and electrical properties of new ionic conductor Ag4Co7(AsO4)6

Auteurs : R. Marzouki [Tunisie] ; A. Guesmi [Tunisie] ; S. Georges [France] ; M. F. Zid [Tunisie] ; A. Driss [Tunisie]

Source :

RBID : Pascal:14-0159434

Descripteurs français

English descriptors

Abstract

A new silver-cobalt arsenate, Ag4Co7(AsO4)6, is synthesized by solid state reaction method and characterized by X-ray diffraction and impedance spectroscopy. The phase crystallizes in the monoclinic space group C2/m with a = 10.755(2) Å, b = 14.937(2) Å, c = 6.731(2) Å, and β = 106.17(3)°. The structure is described as a three-dimensional anionic framework having interconnecting tunnels running along [100] and [010]. The former contains the silver cations. Ball milling is used as mechanical means to reduce the particles sizes of the as synthesized powder. At the optimal sintering temperature of 1173 K, dense ceramics (96% of the relative density) are obtained. Their microstructure is characterized by scanning electron microscopy. The conductivity of the ceramics is studied at different relative densities over a temperature interval from 437 to 773 K. The high conductivity at 210 °C (3.3 × 10-5 S cm-1) and the activation energy (Ea = 0.45 eV) show that Ag4Co7(AsO4)6 is a fast ionic conductor.
pA  
A01 01  1    @0 0925-8388
A03   1    @0 J. alloys compd.
A05       @2 586
A08 01  1  ENG  @1 Structure, sintering and electrical properties of new ionic conductor Ag4Co7(AsO4)6
A11 01  1    @1 MARZOUKI (R.)
A11 02  1    @1 GUESMI (A.)
A11 03  1    @1 GEORGES (S.)
A11 04  1    @1 ZID (M. F.)
A11 05  1    @1 DRISS (A.)
A14 01      @1 Département de Chimie, Faculté des Sciences, Université Tunis El Manar @2 Tunis @3 TUN @Z 1 aut. @Z 2 aut. @Z 4 aut. @Z 5 aut.
A14 02      @1 Institut Préparatoire aux Etudes d'Ingénieur, Université Tunis El Manar @2 Tunis @3 TUN @Z 2 aut.
A14 03      @1 Laboratoire d'Electrochimie et de Physicochimie des Matériaux et des Interfaces LEPMI, UMR 5279, CNRS: Grenoble INP, Université de Savoie, Université Joseph Fourier, BP75 @2 38402 Saint Martin d'Hères @3 FRA @Z 3 aut.
A20       @1 74-79
A21       @1 2014
A23 01      @0 ENG
A43 01      @1 INIST @2 1151 @5 354000505794820130
A44       @0 0000 @1 © 2014 INIST-CNRS. All rights reserved.
A45       @0 43 ref.
A47 01  1    @0 14-0159434
A60       @1 P
A61       @0 A
A64 01  1    @0 Journal of alloys and compounds
A66 01      @0 GBR
C01 01    ENG  @0 A new silver-cobalt arsenate, Ag4Co7(AsO4)6, is synthesized by solid state reaction method and characterized by X-ray diffraction and impedance spectroscopy. The phase crystallizes in the monoclinic space group C2/m with a = 10.755(2) Å, b = 14.937(2) Å, c = 6.731(2) Å, and β = 106.17(3)°. The structure is described as a three-dimensional anionic framework having interconnecting tunnels running along [100] and [010]. The former contains the silver cations. Ball milling is used as mechanical means to reduce the particles sizes of the as synthesized powder. At the optimal sintering temperature of 1173 K, dense ceramics (96% of the relative density) are obtained. Their microstructure is characterized by scanning electron microscopy. The conductivity of the ceramics is studied at different relative densities over a temperature interval from 437 to 773 K. The high conductivity at 210 °C (3.3 × 10-5 S cm-1) and the activation energy (Ea = 0.45 eV) show that Ag4Co7(AsO4)6 is a fast ionic conductor.
C02 01  3    @0 001B60F30H
C03 01  3  FRE  @0 Frittage @5 02
C03 01  3  ENG  @0 Sintering @5 02
C03 02  3  FRE  @0 Conductivité ionique @5 03
C03 02  3  ENG  @0 Ionic conductivity @5 03
C03 03  X  FRE  @0 Réaction état solide @5 04
C03 03  X  ENG  @0 Solid state reaction @5 04
C03 03  X  SPA  @0 Reacción estado sólido @5 04
C03 04  3  FRE  @0 Diffraction RX @5 05
C03 04  3  ENG  @0 XRD @5 05
C03 05  3  FRE  @0 Effet tunnel @5 07
C03 05  3  ENG  @0 Tunnel effect @5 07
C03 06  X  FRE  @0 Broyeur boulet @5 08
C03 06  X  ENG  @0 Ball mill @5 08
C03 06  X  SPA  @0 Molino bolas @5 08
C03 07  3  FRE  @0 Dimension particule @5 09
C03 07  3  ENG  @0 Particle size @5 09
C03 08  3  FRE  @0 Microstructure @5 10
C03 08  3  ENG  @0 Microstructure @5 10
C03 09  3  FRE  @0 Energie activation @5 12
C03 09  3  ENG  @0 Activation energy @5 12
C03 10  X  FRE  @0 Argent Cobalt Arséniate Mixte @2 NC @2 NA @5 13
C03 10  X  ENG  @0 Silver Cobalt Arsenates Mixed @2 NC @2 NA @5 13
C03 10  X  SPA  @0 Mixto @2 NC @2 NA @5 13
C03 11  3  FRE  @0 Conducteur ionique @5 15
C03 11  3  ENG  @0 Ionic conductors @5 15
N21       @1 202

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Pascal:14-0159434

Le document en format XML

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<div type="abstract" xml:lang="en">A new silver-cobalt arsenate, Ag
<sub>4</sub>
Co
<sub>7</sub>
(AsO
<sub>4</sub>
)
<sub>6</sub>
, is synthesized by solid state reaction method and characterized by X-ray diffraction and impedance spectroscopy. The phase crystallizes in the monoclinic space group C2/m with a = 10.755(2) Å, b = 14.937(2) Å, c = 6.731(2) Å, and β = 106.17(3)°. The structure is described as a three-dimensional anionic framework having interconnecting tunnels running along [100] and [010]. The former contains the silver cations. Ball milling is used as mechanical means to reduce the particles sizes of the as synthesized powder. At the optimal sintering temperature of 1173 K, dense ceramics (96% of the relative density) are obtained. Their microstructure is characterized by scanning electron microscopy. The conductivity of the ceramics is studied at different relative densities over a temperature interval from 437 to 773 K. The high conductivity at 210 °C (3.3 × 10
<sup>-5</sup>
S cm
<sup>-1</sup>
) and the activation energy (Ea = 0.45 eV) show that Ag
<sub>4</sub>
Co
<sub>7</sub>
(AsO
<sub>4</sub>
)
<sub>6</sub>
is a fast ionic conductor.</div>
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<s0>A new silver-cobalt arsenate, Ag
<sub>4</sub>
Co
<sub>7</sub>
(AsO
<sub>4</sub>
)
<sub>6</sub>
, is synthesized by solid state reaction method and characterized by X-ray diffraction and impedance spectroscopy. The phase crystallizes in the monoclinic space group C2/m with a = 10.755(2) Å, b = 14.937(2) Å, c = 6.731(2) Å, and β = 106.17(3)°. The structure is described as a three-dimensional anionic framework having interconnecting tunnels running along [100] and [010]. The former contains the silver cations. Ball milling is used as mechanical means to reduce the particles sizes of the as synthesized powder. At the optimal sintering temperature of 1173 K, dense ceramics (96% of the relative density) are obtained. Their microstructure is characterized by scanning electron microscopy. The conductivity of the ceramics is studied at different relative densities over a temperature interval from 437 to 773 K. The high conductivity at 210 °C (3.3 × 10
<sup>-5</sup>
S cm
<sup>-1</sup>
) and the activation energy (Ea = 0.45 eV) show that Ag
<sub>4</sub>
Co
<sub>7</sub>
(AsO
<sub>4</sub>
)
<sub>6</sub>
is a fast ionic conductor.</s0>
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<s5>07</s5>
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<s5>09</s5>
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<s5>10</s5>
</fC03>
<fC03 i1="08" i2="3" l="ENG">
<s0>Microstructure</s0>
<s5>10</s5>
</fC03>
<fC03 i1="09" i2="3" l="FRE">
<s0>Energie activation</s0>
<s5>12</s5>
</fC03>
<fC03 i1="09" i2="3" l="ENG">
<s0>Activation energy</s0>
<s5>12</s5>
</fC03>
<fC03 i1="10" i2="X" l="FRE">
<s0>Argent Cobalt Arséniate Mixte</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>13</s5>
</fC03>
<fC03 i1="10" i2="X" l="ENG">
<s0>Silver Cobalt Arsenates Mixed</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>13</s5>
</fC03>
<fC03 i1="10" i2="X" l="SPA">
<s0>Mixto</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>13</s5>
</fC03>
<fC03 i1="11" i2="3" l="FRE">
<s0>Conducteur ionique</s0>
<s5>15</s5>
</fC03>
<fC03 i1="11" i2="3" l="ENG">
<s0>Ionic conductors</s0>
<s5>15</s5>
</fC03>
<fN21>
<s1>202</s1>
</fN21>
</pA>
</standard>
</inist>
</record>

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