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Solid state amorphisation of mechanically alloyed Fe-Co-Nb-B alloys : NANOTECHNOLOGY AND ADVANCED MATERIALS - PART II

Identifieur interne : 000223 ( PascalFrancis/Curation ); précédent : 000222; suivant : 000224

Solid state amorphisation of mechanically alloyed Fe-Co-Nb-B alloys : NANOTECHNOLOGY AND ADVANCED MATERIALS - PART II

Auteurs : R. Bensalem [Algérie] ; A. Younes [Algérie] ; S. Alleg [Algérie] ; S. Souilah [Algérie] ; S. Azzaza [Algérie] ; J. J. Sunol [Espagne] ; J. M. Greneche [France]

Source :

RBID : Pascal:11-0308869

Descripteurs français

English descriptors

Abstract

Fe61Co21Nb3B15 powder mixture was prepared by mechanical alloying process in a high energy planetary ball mill. Structural and thermal changes of the milled powders were followed by X-ray diffraction (XRD), Mössbauer spectrometry and differential scanning calorimetry (DSC). Both XRD and Mössbauer spectrometry results reveal the formation, after 48 h of milling, of a highly disordered amorphous-like structure where nanometer-sized iron borides were embedded. A mechanical recrystallisation process gives rise to the formation of α-Fe and α-FeCo nanograins on further milling. The occurrence of structural disorder in the milled powders might be confirmed by broad exothermic reaction in the DSC scans which consists of several overlapping exothermic peaks. Such behaviour originates from recovery, strain relaxation, grain growth and crystallisation.
pA  
A01 01  1    @0 1753-2507
A03   1    @0 Int. j. nanopart. : (Print)
A05       @2 4
A06       @2 1
A08 01  1  ENG  @1 Solid state amorphisation of mechanically alloyed Fe-Co-Nb-B alloys : NANOTECHNOLOGY AND ADVANCED MATERIALS - PART II
A11 01  1    @1 BENSALEM (R.)
A11 02  1    @1 YOUNES (A.)
A11 03  1    @1 ALLEG (S.)
A11 04  1    @1 SOUILAH (S.)
A11 05  1    @1 AZZAZA (S.)
A11 06  1    @1 SUNOL (J. J.)
A11 07  1    @1 GRENECHE (J. M.)
A14 01      @1 Laboratoire de Magnétisme et spectroscopie des Solides, Department de Physique Université de Annaba, B.P. 12 @2 23000, Annaba @3 DZA @Z 1 aut. @Z 2 aut. @Z 3 aut. @Z 4 aut. @Z 5 aut.
A14 02      @1 Department de Fisica, Universitat de Girona, Campus Montilivi @2 Girona 17071 @3 ESP @Z 6 aut.
A14 03      @1 Laboratoire de Physique de L'Etat Condensé, UMR CNRS 6087, Institut de Recherche en Ingénierie Moléculaire et Matériaux Fonctionnels, IRIM2F, FR CNRS 2575, Université du Maine @2 72085, Le Mans @3 FRA @Z 7 aut.
A20       @1 45-52
A21       @1 2011
A23 01      @0 ENG
A43 01      @1 INIST @2 27946 @5 354000192022590060
A44       @0 0000 @1 © 2011 INIST-CNRS. All rights reserved.
A45       @0 3/4 p.
A47 01  1    @0 11-0308869
A60       @1 P
A61       @0 A
A64 01  1    @0 International journal of nanoparticles : (Print)
A66 01      @0 CHE
C01 01    ENG  @0 Fe61Co21Nb3B15 powder mixture was prepared by mechanical alloying process in a high energy planetary ball mill. Structural and thermal changes of the milled powders were followed by X-ray diffraction (XRD), Mössbauer spectrometry and differential scanning calorimetry (DSC). Both XRD and Mössbauer spectrometry results reveal the formation, after 48 h of milling, of a highly disordered amorphous-like structure where nanometer-sized iron borides were embedded. A mechanical recrystallisation process gives rise to the formation of α-Fe and α-FeCo nanograins on further milling. The occurrence of structural disorder in the milled powders might be confirmed by broad exothermic reaction in the DSC scans which consists of several overlapping exothermic peaks. Such behaviour originates from recovery, strain relaxation, grain growth and crystallisation.
C02 01  3    @0 001B80A07B
C02 02  3    @0 001B80A20
C03 01  3  FRE  @0 Déformation mécanique @5 03
C03 01  3  ENG  @0 Strains @5 03
C03 02  3  FRE  @0 Diffraction RX @5 30
C03 02  3  ENG  @0 XRD @5 30
C03 03  3  FRE  @0 Poudre @5 47
C03 03  3  ENG  @0 Powders @5 47
C03 04  3  FRE  @0 Nanostructure @5 48
C03 04  3  ENG  @0 Nanostructures @5 48
C03 05  3  FRE  @0 Calorimétrie @5 61
C03 05  3  ENG  @0 Calorimetry @5 61
C03 06  3  FRE  @0 Fer @2 NC @5 62
C03 06  3  ENG  @0 Iron @2 NC @5 62
C03 07  3  FRE  @0 Fer alliage @5 63
C03 07  3  ENG  @0 Iron alloys @5 63
C03 08  3  FRE  @0 Cobalt alliage @5 64
C03 08  3  ENG  @0 Cobalt alloys @5 64
C03 09  3  FRE  @0 Niobium alliage @5 65
C03 09  3  ENG  @0 Niobium alloys @5 65
C03 10  3  FRE  @0 Bore alliage @5 66
C03 10  3  ENG  @0 Boron alloys @5 66
C03 11  X  FRE  @0 Spectre Mössbauer @5 67
C03 11  X  ENG  @0 Moessbauer spectrum @5 67
C03 11  X  SPA  @0 Espectro Mossbauer @5 67
C03 12  3  FRE  @0 Alliage mécanique @5 68
C03 12  3  ENG  @0 Mechanical alloying @5 68
C03 13  3  FRE  @0 Amorphisation @5 69
C03 13  3  ENG  @0 Amorphization @5 69
C03 14  3  FRE  @0 8107B @4 INC @5 83
C03 15  3  FRE  @0 8120E @4 INC @5 84
N21       @1 213

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Pascal:11-0308869

Le document en format XML

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<term>Amorphization</term>
<term>Boron alloys</term>
<term>Calorimetry</term>
<term>Cobalt alloys</term>
<term>Iron</term>
<term>Iron alloys</term>
<term>Mechanical alloying</term>
<term>Moessbauer spectrum</term>
<term>Nanostructures</term>
<term>Niobium alloys</term>
<term>Powders</term>
<term>Strains</term>
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</keywords>
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<term>Déformation mécanique</term>
<term>Diffraction RX</term>
<term>Poudre</term>
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<term>Calorimétrie</term>
<term>Fer</term>
<term>Fer alliage</term>
<term>Cobalt alliage</term>
<term>Niobium alliage</term>
<term>Bore alliage</term>
<term>Spectre Mössbauer</term>
<term>Alliage mécanique</term>
<term>Amorphisation</term>
<term>8107B</term>
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<div type="abstract" xml:lang="en">Fe
<sub>61</sub>
Co
<sub>21</sub>
Nb
<sub>3</sub>
B
<sub>15</sub>
powder mixture was prepared by mechanical alloying process in a high energy planetary ball mill. Structural and thermal changes of the milled powders were followed by X-ray diffraction (XRD), Mössbauer spectrometry and differential scanning calorimetry (DSC). Both XRD and Mössbauer spectrometry results reveal the formation, after 48 h of milling, of a highly disordered amorphous-like structure where nanometer-sized iron borides were embedded. A mechanical recrystallisation process gives rise to the formation of α-Fe and α-FeCo nanograins on further milling. The occurrence of structural disorder in the milled powders might be confirmed by broad exothermic reaction in the DSC scans which consists of several overlapping exothermic peaks. Such behaviour originates from recovery, strain relaxation, grain growth and crystallisation.</div>
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<s0>Fe
<sub>61</sub>
Co
<sub>21</sub>
Nb
<sub>3</sub>
B
<sub>15</sub>
powder mixture was prepared by mechanical alloying process in a high energy planetary ball mill. Structural and thermal changes of the milled powders were followed by X-ray diffraction (XRD), Mössbauer spectrometry and differential scanning calorimetry (DSC). Both XRD and Mössbauer spectrometry results reveal the formation, after 48 h of milling, of a highly disordered amorphous-like structure where nanometer-sized iron borides were embedded. A mechanical recrystallisation process gives rise to the formation of α-Fe and α-FeCo nanograins on further milling. The occurrence of structural disorder in the milled powders might be confirmed by broad exothermic reaction in the DSC scans which consists of several overlapping exothermic peaks. Such behaviour originates from recovery, strain relaxation, grain growth and crystallisation.</s0>
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<fC03 i1="02" i2="3" l="ENG">
<s0>XRD</s0>
<s5>30</s5>
</fC03>
<fC03 i1="03" i2="3" l="FRE">
<s0>Poudre</s0>
<s5>47</s5>
</fC03>
<fC03 i1="03" i2="3" l="ENG">
<s0>Powders</s0>
<s5>47</s5>
</fC03>
<fC03 i1="04" i2="3" l="FRE">
<s0>Nanostructure</s0>
<s5>48</s5>
</fC03>
<fC03 i1="04" i2="3" l="ENG">
<s0>Nanostructures</s0>
<s5>48</s5>
</fC03>
<fC03 i1="05" i2="3" l="FRE">
<s0>Calorimétrie</s0>
<s5>61</s5>
</fC03>
<fC03 i1="05" i2="3" l="ENG">
<s0>Calorimetry</s0>
<s5>61</s5>
</fC03>
<fC03 i1="06" i2="3" l="FRE">
<s0>Fer</s0>
<s2>NC</s2>
<s5>62</s5>
</fC03>
<fC03 i1="06" i2="3" l="ENG">
<s0>Iron</s0>
<s2>NC</s2>
<s5>62</s5>
</fC03>
<fC03 i1="07" i2="3" l="FRE">
<s0>Fer alliage</s0>
<s5>63</s5>
</fC03>
<fC03 i1="07" i2="3" l="ENG">
<s0>Iron alloys</s0>
<s5>63</s5>
</fC03>
<fC03 i1="08" i2="3" l="FRE">
<s0>Cobalt alliage</s0>
<s5>64</s5>
</fC03>
<fC03 i1="08" i2="3" l="ENG">
<s0>Cobalt alloys</s0>
<s5>64</s5>
</fC03>
<fC03 i1="09" i2="3" l="FRE">
<s0>Niobium alliage</s0>
<s5>65</s5>
</fC03>
<fC03 i1="09" i2="3" l="ENG">
<s0>Niobium alloys</s0>
<s5>65</s5>
</fC03>
<fC03 i1="10" i2="3" l="FRE">
<s0>Bore alliage</s0>
<s5>66</s5>
</fC03>
<fC03 i1="10" i2="3" l="ENG">
<s0>Boron alloys</s0>
<s5>66</s5>
</fC03>
<fC03 i1="11" i2="X" l="FRE">
<s0>Spectre Mössbauer</s0>
<s5>67</s5>
</fC03>
<fC03 i1="11" i2="X" l="ENG">
<s0>Moessbauer spectrum</s0>
<s5>67</s5>
</fC03>
<fC03 i1="11" i2="X" l="SPA">
<s0>Espectro Mossbauer</s0>
<s5>67</s5>
</fC03>
<fC03 i1="12" i2="3" l="FRE">
<s0>Alliage mécanique</s0>
<s5>68</s5>
</fC03>
<fC03 i1="12" i2="3" l="ENG">
<s0>Mechanical alloying</s0>
<s5>68</s5>
</fC03>
<fC03 i1="13" i2="3" l="FRE">
<s0>Amorphisation</s0>
<s5>69</s5>
</fC03>
<fC03 i1="13" i2="3" l="ENG">
<s0>Amorphization</s0>
<s5>69</s5>
</fC03>
<fC03 i1="14" i2="3" l="FRE">
<s0>8107B</s0>
<s4>INC</s4>
<s5>83</s5>
</fC03>
<fC03 i1="15" i2="3" l="FRE">
<s0>8120E</s0>
<s4>INC</s4>
<s5>84</s5>
</fC03>
<fN21>
<s1>213</s1>
</fN21>
</pA>
</standard>
</inist>
</record>

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