CobaltMaghrebV1, PascalFrancis, Curation, bibRecord, 000147

Structure and properties of nanocrystalline Cu70Fe18Co12 obtained by mechanical alloying

Identifieur interne : 000147 ( PascalFrancis/Curation ); précédent : 000146; suivant : 000148

Structure and properties of nanocrystalline Cu70Fe18Co12 obtained by mechanical alloying

Auteurs : Warda Laslouni [Algérie] ; Kamel Taibi [Algérie] ; Djaffar Dahmoun [Algérie] ; Mohamed Azzaz [Algérie]

Source :

Journal of non-crystalline solids [ 0022-3093 ] ; 2007.

RBID : Pascal:07-0293665

Descripteurs français

Pascal (Inist)
- Alliage mécanique, Broyeur boulet, Microscopie électronique balayage, Diffraction RX, Effet Mössbauer, Analyse structurale, Microstructure, Nanocristal, Réseau cubique face centrée, Cuivre alliage, Métal transition alliage, 6146, 8107B.

English descriptors

KwdEn :
- Ball mill, Copper alloys, FCC lattices, Mechanical alloying, Microstructure, Moessbauer effect, Nanocrystal, Scanning electron microscopy, Structural analysis, Transition element alloys, XRD.

Abstract

Cu₇₀Fe₁₈Co₁₂ alloy is prepared by mechanical alloying of pure Cu, Fe, Co powder using a high energy ball mill, with increasing milling time ranging from 4 to 8, 24, 36 and 54 h. The variation of the morphology and the elemental distribution were measured at these different stages on various grains of the alloy using a scanning electron microscope with a dispersive energy analyzer. Atomic clusters of iron were observed on some grains after 8 h of milling, confirming the non-homogenisation of the powder at this stage. Beyond 12 h, the homogenisation is ensured over a volume of one cube micron. Microstructural changes during the mechanical alloying have been studied by X-ray diffractometry (XRD) and Mössbauer spectroscopy. X-ray diffraction measurements confirm the dissolution of iron and cobalt phases in the FCC matrix of copper after 24 h of milling with increase of the structural parameter. This same dissolution was also measured by Mössbauer spectroscopy, confirming that after 4 h of milling the CuFe phase begins to form and iron dissolution is incomplete with partial amount of alpha Fe phase surviving after 36 h of milling.

A01	`01`	`1`		`@0 0022-3093`
A02	`01`			`@0 JNCSBJ`
A03		`1`		`@0 J. non-cryst. solids`
A05				`@2 353`
A06				`@2 18-21`
A08	`01`	`1`	`ENG`	`@1 Structure and properties of nanocrystalline Cu₇₀Fe₁₈Co₁₂ obtained by mechanical alloying`
A09	`01`	`1`	`ENG`	`@1 Structure of non-crystalline materials 10: proceedings of the 10th International Conference on the Structure of Non-Crystalline Materials (NCM 10), Prague, September 18-22, 2006`
A11	`01`	`1`		`@1 LASLOUNI (Warda)`
A11	`02`	`1`		`@1 TAIBI (Kamel)`
A11	`03`	`1`		`@1 DAHMOUN (Djaffar)`
A11	`04`	`1`		`@1 AZZAZ (Mohamed)`
A12	`01`	`1`		`@1 CERVINKA (Ladislav) @9 ed.`
A14	`01`			`@1 Laboratoire de Science et Génie des Matériaux, U.S.T.H.B., BP 32 El-Alia @2 Babezzouar 16311, Alger @3 DZA @Z 1 aut. @Z 2 aut. @Z 3 aut. @Z 4 aut.`
A15	`01`			`@1 Institute of Physics, Academy of Sciences of the Czech Republic @2 Prague @3 CZE @Z 1 aut.`
A20				`@1 2090-2093`
A21				`@1 2007`
A23	`01`			`@0 ENG`
A43	`01`			`@1 INIST @2 14572 @5 354000162259070750`
A44				`@0 0000 @1 © 2007 INIST-CNRS. All rights reserved.`
A45				`@0 13 ref.`
A47	`01`	`1`		`@0 07-0293665`
A60				`@1 P @2 C`
A61				`@0 A`
A64	`01`	`1`		`@0 Journal of non-crystalline solids`
A66	`01`			`@0 NLD`
C01	`01`		`ENG`	@0 Cu₇₀Fe₁₈Co₁₂ alloy is prepared by mechanical alloying of pure Cu, Fe, Co powder using a high energy ball mill, with increasing milling time ranging from 4 to 8, 24, 36 and 54 h. The variation of the morphology and the elemental distribution were measured at these different stages on various grains of the alloy using a scanning electron microscope with a dispersive energy analyzer. Atomic clusters of iron were observed on some grains after 8 h of milling, confirming the non-homogenisation of the powder at this stage. Beyond 12 h, the homogenisation is ensured over a volume of one cube micron. Microstructural changes during the mechanical alloying have been studied by X-ray diffractometry (XRD) and Mössbauer spectroscopy. X-ray diffraction measurements confirm the dissolution of iron and cobalt phases in the FCC matrix of copper after 24 h of milling with increase of the structural parameter. This same dissolution was also measured by Mössbauer spectroscopy, confirming that after 4 h of milling the CuFe phase begins to form and iron dissolution is incomplete with partial amount of alpha Fe phase surviving after 36 h of milling.
C02	`01`	`3`		`@0 001B80A07B`
C02	`02`	`3`		`@0 001B60A46`
C03	`01`	`3`	`FRE`	`@0 Alliage mécanique @5 02`
C03	`01`	`3`	`ENG`	`@0 Mechanical alloying @5 02`
C03	`02`	`X`	`FRE`	`@0 Broyeur boulet @5 03`
C03	`02`	`X`	`ENG`	`@0 Ball mill @5 03`
C03	`02`	`X`	`SPA`	`@0 Molino bolas @5 03`
C03	`03`	`3`	`FRE`	`@0 Microscopie électronique balayage @5 04`
C03	`03`	`3`	`ENG`	`@0 Scanning electron microscopy @5 04`
C03	`04`	`3`	`FRE`	`@0 Diffraction RX @5 05`
C03	`04`	`3`	`ENG`	`@0 XRD @5 05`
C03	`05`	`3`	`FRE`	`@0 Effet Mössbauer @5 06`
C03	`05`	`3`	`ENG`	`@0 Moessbauer effect @5 06`
C03	`06`	`X`	`FRE`	`@0 Analyse structurale @5 07`
C03	`06`	`X`	`ENG`	`@0 Structural analysis @5 07`
C03	`06`	`X`	`SPA`	`@0 Análisis estructural @5 07`
C03	`07`	`3`	`FRE`	`@0 Microstructure @5 11`
C03	`07`	`3`	`ENG`	`@0 Microstructure @5 11`
C03	`08`	`X`	`FRE`	`@0 Nanocristal @5 15`
C03	`08`	`X`	`ENG`	`@0 Nanocrystal @5 15`
C03	`08`	`X`	`SPA`	`@0 Nanocristal @5 15`
C03	`09`	`3`	`FRE`	`@0 Réseau cubique face centrée @5 20`
C03	`09`	`3`	`ENG`	`@0 FCC lattices @5 20`
C03	`10`	`3`	`FRE`	`@0 Cuivre alliage @5 21`
C03	`10`	`3`	`ENG`	`@0 Copper alloys @5 21`
C03	`11`	`3`	`FRE`	`@0 Métal transition alliage @5 48`
C03	`11`	`3`	`ENG`	`@0 Transition element alloys @5 48`
C03	`12`	`3`	`FRE`	`@0 6146 @4 INC @5 60`
C03	`13`	`3`	`FRE`	`@0 8107B @4 INC @5 61`
N21				`@1 190`

A30	`01`	`1`	`ENG`	`@1 NCM 10 : International Conference on the Structure of Non-Crystalline Materials @2 10 @3 Prague CZE @4 2006-09-18`

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Fe<sub>18</sub>
Co<sub>12</sub>
 obtained by mechanical alloying</title>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a">Structure and properties of nanocrystalline Cu<sub>70</sub>
Fe<sub>18</sub>
Co<sub>12</sub>
 obtained by mechanical alloying</title>
<author><name sortKey="Laslouni, Warda" sort="Laslouni, Warda" uniqKey="Laslouni W" first="Warda" last="Laslouni">Warda Laslouni</name>
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<s3>DZA</s3>
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<author><name sortKey="Taibi, Kamel" sort="Taibi, Kamel" uniqKey="Taibi K" first="Kamel" last="Taibi">Kamel Taibi</name>
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<s2>Babezzouar 16311, Alger</s2>
<s3>DZA</s3>
<sZ>1 aut.</sZ>
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<sZ>4 aut.</sZ>
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<author><name sortKey="Dahmoun, Djaffar" sort="Dahmoun, Djaffar" uniqKey="Dahmoun D" first="Djaffar" last="Dahmoun">Djaffar Dahmoun</name>
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<s3>DZA</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>4 aut.</sZ>
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<country>Algérie</country>
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<author><name sortKey="Azzaz, Mohamed" sort="Azzaz, Mohamed" uniqKey="Azzaz M" first="Mohamed" last="Azzaz">Mohamed Azzaz</name>
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<sZ>1 aut.</sZ>
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<sZ>4 aut.</sZ>
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<series><title level="j" type="main">Journal of non-crystalline solids</title>
<title level="j" type="abbreviated">J. non-cryst. solids</title>
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<term>Moessbauer effect</term>
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<term>XRD</term>
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<keywords scheme="Pascal" xml:lang="fr"><term>Alliage mécanique</term>
<term>Broyeur boulet</term>
<term>Microscopie électronique balayage</term>
<term>Diffraction RX</term>
<term>Effet Mössbauer</term>
<term>Analyse structurale</term>
<term>Microstructure</term>
<term>Nanocristal</term>
<term>Réseau cubique face centrée</term>
<term>Cuivre alliage</term>
<term>Métal transition alliage</term>
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<front><div type="abstract" xml:lang="en">Cu<sub>70</sub>
Fe<sub>18</sub>
Co<sub>12</sub>
 alloy is prepared by mechanical alloying of pure Cu, Fe, Co powder using a high energy ball mill, with increasing milling time ranging from 4 to 8, 24, 36 and 54 h. The variation of the morphology and the elemental distribution were measured at these different stages on various grains of the alloy using a scanning electron microscope with a dispersive energy analyzer. Atomic clusters of iron were observed on some grains after 8 h of milling, confirming the non-homogenisation of the powder at this stage. Beyond 12 h, the homogenisation is ensured over a volume of one cube micron. Microstructural changes during the mechanical alloying have been studied by X-ray diffractometry (XRD) and Mössbauer spectroscopy. X-ray diffraction measurements confirm the dissolution of iron and cobalt phases in the FCC matrix of copper after 24 h of milling with increase of the structural parameter. This same dissolution was also measured by Mössbauer spectroscopy, confirming that after 4 h of milling the CuFe phase begins to form and iron dissolution is incomplete with partial amount of alpha Fe phase surviving after 36 h of milling.</div>
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<fA02 i1="01"><s0>JNCSBJ</s0>
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<fA05><s2>353</s2>
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<fA08 i1="01" i2="1" l="ENG"><s1>Structure and properties of nanocrystalline Cu<sub>70</sub>
Fe<sub>18</sub>
Co<sub>12</sub>
 obtained by mechanical alloying</s1>
</fA08>
<fA09 i1="01" i2="1" l="ENG"><s1>Structure of non-crystalline materials 10: proceedings of the 10th International Conference on the Structure of Non-Crystalline Materials (NCM 10), Prague, September 18-22, 2006</s1>
</fA09>
<fA11 i1="01" i2="1"><s1>LASLOUNI (Warda)</s1>
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<fA11 i1="02" i2="1"><s1>TAIBI (Kamel)</s1>
</fA11>
<fA11 i1="03" i2="1"><s1>DAHMOUN (Djaffar)</s1>
</fA11>
<fA11 i1="04" i2="1"><s1>AZZAZ (Mohamed)</s1>
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<fA12 i1="01" i2="1"><s1>CERVINKA (Ladislav)</s1>
<s9>ed.</s9>
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<fA14 i1="01"><s1>Laboratoire de Science et Génie des Matériaux, U.S.T.H.B., BP 32 El-Alia</s1>
<s2>Babezzouar 16311, Alger</s2>
<s3>DZA</s3>
<sZ>1 aut.</sZ>
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<sZ>3 aut.</sZ>
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<fA15 i1="01"><s1>Institute of Physics, Academy of Sciences of the Czech Republic</s1>
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<sZ>1 aut.</sZ>
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<fA20><s1>2090-2093</s1>
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<fC01 i1="01" l="ENG"><s0>Cu<sub>70</sub>
Fe<sub>18</sub>
Co<sub>12</sub>
 alloy is prepared by mechanical alloying of pure Cu, Fe, Co powder using a high energy ball mill, with increasing milling time ranging from 4 to 8, 24, 36 and 54 h. The variation of the morphology and the elemental distribution were measured at these different stages on various grains of the alloy using a scanning electron microscope with a dispersive energy analyzer. Atomic clusters of iron were observed on some grains after 8 h of milling, confirming the non-homogenisation of the powder at this stage. Beyond 12 h, the homogenisation is ensured over a volume of one cube micron. Microstructural changes during the mechanical alloying have been studied by X-ray diffractometry (XRD) and Mössbauer spectroscopy. X-ray diffraction measurements confirm the dissolution of iron and cobalt phases in the FCC matrix of copper after 24 h of milling with increase of the structural parameter. This same dissolution was also measured by Mössbauer spectroscopy, confirming that after 4 h of milling the CuFe phase begins to form and iron dissolution is incomplete with partial amount of alpha Fe phase surviving after 36 h of milling.</s0>
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<s5>02</s5>
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<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="FRE"><s0>Broyeur boulet</s0>
<s5>03</s5>
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<fC03 i1="02" i2="X" l="ENG"><s0>Ball mill</s0>
<s5>03</s5>
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<s5>03</s5>
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<s5>04</s5>
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<s5>06</s5>
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<s5>06</s5>
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<s5>07</s5>
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<s5>11</s5>
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<s5>15</s5>
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<s5>15</s5>
</fC03>
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<s5>15</s5>
</fC03>
<fC03 i1="09" i2="3" l="FRE"><s0>Réseau cubique face centrée</s0>
<s5>20</s5>
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<fC03 i1="09" i2="3" l="ENG"><s0>FCC lattices</s0>
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<s5>21</s5>
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<s5>21</s5>
</fC03>
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<s5>48</s5>
</fC03>
<fC03 i1="11" i2="3" l="ENG"><s0>Transition element alloys</s0>
<s5>48</s5>
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<fC03 i1="12" i2="3" l="FRE"><s0>6146</s0>
<s4>INC</s4>
<s5>60</s5>
</fC03>
<fC03 i1="13" i2="3" l="FRE"><s0>8107B</s0>
<s4>INC</s4>
<s5>61</s5>
</fC03>
<fN21><s1>190</s1>
</fN21>
</pA>
<pR><fA30 i1="01" i2="1" l="ENG"><s1>NCM 10 : International Conference on the Structure of Non-Crystalline Materials</s1>
<s2>10</s2>
<s3>Prague CZE</s3>
<s4>2006-09-18</s4>
</fA30>
</pR>
</standard>
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Structure and properties of nanocrystalline Cu70Fe18Co12 obtained by mechanical alloying

Structure and properties of nanocrystalline Cu70Fe18Co12 obtained by mechanical alloying

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