CobaltMaghrebV1, PascalFrancis, Curation, bibRecord, 000062

LiAlyCo1-yO2 (0.0 ≤ y ≤ 0.3) intercalation compounds synthesized from the citrate precursors

Identifieur interne : 000062 ( PascalFrancis/Curation ); précédent : 000061; suivant : 000063

LiAlyCo1-yO2 (0.0 ≤ y ≤ 0.3) intercalation compounds synthesized from the citrate precursors

Auteurs : N. Amdouni [Tunisie] ; H. Zarrouk [Tunisie] ; F. Soulette [France] ; C. Julien [France]

Source :

Materials chemistry and physics [ 0254-0584 ] ; 2003.

RBID : Pascal:03-0305472

Descripteurs français

Pascal (Inist)
- Composé insertion, Citrate, Synthèse chimique, Lithium oxyde, Aluminium oxyde, Cobalt oxyde, Composé quaternaire, Batterie lithium, ATD, Microscopie électronique balayage, Etude expérimentale, Structure cristalline, Diffraction RX, 8120K.

English descriptors

KwdEn :
- Aluminium oxides, Chemical synthesis, Citrates, Cobalt oxides, Crystal structure, DTA, Experimental study, Intercalation compounds, Lithium battery, Lithium oxides, Quaternary compounds, Scanning electron microscopy, XRD.

Abstract

We present the synthesis, characterization and electrode behaviour ofLiAl_yCo_1-yO₂(0.0 ≤ y ≤ 0.3) oxides prepared by the citrate route. The phase evolution was studied as a function of the aluminium substitution and the modification on the intercalation and deintercalation of Li ions. Characterization methods include X-ray powder diffraction (XRD), thermogravimetry analysis (TG-DTA), scanning electron microscopy (SEM), Raman scattering (RS) and Fourier transform infrared (FTIR) spectroscopy. Samples belong to the LiCoO₂-LiAlO₂ solid solution and have the layered α-NaFeO₂ structure (R3m space group). Raman scattering and FT-infrared vibrational spectroscopies indicate that the vibrational mode frequencies and relative intensities of the bands are sensitive to the covalency of the (Co, Al)O₂ slabs. SEM micrographs show that the particle size of the LiAl_yCo_1-yO₂powders ranges in the submicronic domain with a narrow grain-size distribution. The overall electrochemical capacity of the LiAl_yCo_1-yO₂ oxides have been reduced due to the sp metal substitution, however, a more stable charge-discharge cycling performances have been observed when electrodes are charged up to 4.3V as compared to the performance of the native oxide. For such a cut-off voltage, the charge capacity of the Li//LiAl_0.2Co_0.8O₂ cell is ca. 118 mAh g^-1. Kinetics were characterized by the galvanostatic intermittent titration technique (GITT). Aluminium substitution provides an increase of the chemical diffusion coefficients ofLi⁺ ions in the LiAl_y Co_1-yO₂ matrix. Differences and similarities between LiCoO₂ and Al-substituted oxides are discussed therefrom.

A01	`01`	`1`		`@0 0254-0584`
A02	`01`			`@0 MCHPDR`
A03		`1`		`@0 Mater. chem. phys.`
A05				`@2 80`
A06				`@2 1`
A08	`01`	`1`	`ENG`	`@1 LiAl_yCo₁-_yO₂ (0.0 ≤ y ≤ 0.3) intercalation compounds synthesized from the citrate precursors`
A11	`01`	`1`		`@1 AMDOUNI (N.)`
A11	`02`	`1`		`@1 ZARROUK (H.)`
A11	`03`	`1`		`@1 SOULETTE (F.)`
A11	`04`	`1`		`@1 JULIEN (C.)`
A14	`01`			`@1 Laboratoire de Chimie des Matériaux, Faculté des Sciences de Tunis Université de Tunis El Manar Campus Universitaire @2 2092 El Manar II @3 TUN @Z 1 aut. @Z 2 aut.`
A14	`02`			`@1 Laboratoire des Milieux Désordonnés et Hétérogènes, CNRS-UMR7603, Université Pierre et Marie Curie, 4 place Jussieu, case 86 @2 75252 Paris @3 FRA @Z 3 aut. @Z 4 aut.`
A20				`@1 205-214`
A21				`@1 2003`
A23	`01`			`@0 ENG`
A43	`01`			`@1 INIST @2 17552 @5 354000118040940340`
A44				`@0 0000 @1 © 2003 INIST-CNRS. All rights reserved.`
A45				`@0 44 ref.`
A47	`01`	`1`		`@0 03-0305472`
A60				`@1 P`
A61				`@0 A`
A64	`01`	`1`		`@0 Materials chemistry and physics`
A66	`01`			`@0 CHE`
C01	`01`		`ENG`	@0 We present the synthesis, characterization and electrode behaviour ofLiAl_yCo_1-yO₂(0.0 ≤ y ≤ 0.3) oxides prepared by the citrate route. The phase evolution was studied as a function of the aluminium substitution and the modification on the intercalation and deintercalation of Li ions. Characterization methods include X-ray powder diffraction (XRD), thermogravimetry analysis (TG-DTA), scanning electron microscopy (SEM), Raman scattering (RS) and Fourier transform infrared (FTIR) spectroscopy. Samples belong to the LiCoO₂-LiAlO₂ solid solution and have the layered α-NaFeO₂ structure (R3m space group). Raman scattering and FT-infrared vibrational spectroscopies indicate that the vibrational mode frequencies and relative intensities of the bands are sensitive to the covalency of the (Co, Al)O₂ slabs. SEM micrographs show that the particle size of the LiAl_yCo_1-yO₂powders ranges in the submicronic domain with a narrow grain-size distribution. The overall electrochemical capacity of the LiAl_yCo_1-yO₂ oxides have been reduced due to the sp metal substitution, however, a more stable charge-discharge cycling performances have been observed when electrodes are charged up to 4.3V as compared to the performance of the native oxide. For such a cut-off voltage, the charge capacity of the Li//LiAl_0.2Co_0.8O₂ cell is ca. 118 mAh g^-1. Kinetics were characterized by the galvanostatic intermittent titration technique (GITT). Aluminium substitution provides an increase of the chemical diffusion coefficients ofLi⁺ ions in the LiAl_y Co_1-yO₂ matrix. Differences and similarities between LiCoO₂ and Al-substituted oxides are discussed therefrom.
C02	`01`	`3`		`@0 001B80A20`
C03	`01`	`3`	`FRE`	`@0 Composé insertion @5 01`
C03	`01`	`3`	`ENG`	`@0 Intercalation compounds @5 01`
C03	`02`	`3`	`FRE`	`@0 Citrate @2 NK @5 02`
C03	`02`	`3`	`ENG`	`@0 Citrates @2 NK @5 02`
C03	`03`	`X`	`FRE`	`@0 Synthèse chimique @5 03`
C03	`03`	`X`	`ENG`	`@0 Chemical synthesis @5 03`
C03	`03`	`X`	`SPA`	`@0 Síntesis química @5 03`
C03	`04`	`3`	`FRE`	`@0 Lithium oxyde @2 NK @5 04`
C03	`04`	`3`	`ENG`	`@0 Lithium oxides @2 NK @5 04`
C03	`05`	`3`	`FRE`	`@0 Aluminium oxyde @2 NK @5 05`
C03	`05`	`3`	`ENG`	`@0 Aluminium oxides @2 NK @5 05`
C03	`06`	`3`	`FRE`	`@0 Cobalt oxyde @2 NK @5 06`
C03	`06`	`3`	`ENG`	`@0 Cobalt oxides @2 NK @5 06`
C03	`07`	`3`	`FRE`	`@0 Composé quaternaire @5 07`
C03	`07`	`3`	`ENG`	`@0 Quaternary compounds @5 07`
C03	`08`	`3`	`FRE`	`@0 Batterie lithium @5 08`
C03	`08`	`3`	`ENG`	`@0 Lithium battery @5 08`
C03	`09`	`3`	`FRE`	`@0 ATD @5 10`
C03	`09`	`3`	`ENG`	`@0 DTA @5 10`
C03	`10`	`3`	`FRE`	`@0 Microscopie électronique balayage @5 11`
C03	`10`	`3`	`ENG`	`@0 Scanning electron microscopy @5 11`
C03	`11`	`3`	`FRE`	`@0 Etude expérimentale @5 12`
C03	`11`	`3`	`ENG`	`@0 Experimental study @5 12`
C03	`12`	`3`	`FRE`	`@0 Structure cristalline @5 23`
C03	`12`	`3`	`ENG`	`@0 Crystal structure @5 23`
C03	`13`	`3`	`FRE`	`@0 Diffraction RX @5 24`
C03	`13`	`3`	`ENG`	`@0 XRD @5 24`
C03	`14`	`3`	`FRE`	`@0 8120K @2 PAC @4 INC @5 95`
N21				`@1 202`
N82				`@1 PSI`

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Le document en format XML

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Co<sub>1</sub>
-<sub>y</sub>
O<sub>2</sub>
 (0.0 ≤ y ≤ 0.3) intercalation compounds synthesized from the citrate precursors</title>
<author><name sortKey="Amdouni, N" sort="Amdouni, N" uniqKey="Amdouni N" first="N." last="Amdouni">N. Amdouni</name>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a">LiAl<sub>y</sub>
Co<sub>1</sub>
-<sub>y</sub>
O<sub>2</sub>
 (0.0 ≤ y ≤ 0.3) intercalation compounds synthesized from the citrate precursors</title>
<author><name sortKey="Amdouni, N" sort="Amdouni, N" uniqKey="Amdouni N" first="N." last="Amdouni">N. Amdouni</name>
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<author><name sortKey="Zarrouk, H" sort="Zarrouk, H" uniqKey="Zarrouk H" first="H." last="Zarrouk">H. Zarrouk</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Laboratoire de Chimie des Matériaux, Faculté des Sciences de Tunis Université de Tunis El Manar Campus Universitaire</s1>
<s2>2092 El Manar II</s2>
<s3>TUN</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
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<country>Tunisie</country>
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<author><name sortKey="Soulette, F" sort="Soulette, F" uniqKey="Soulette F" first="F." last="Soulette">F. Soulette</name>
<affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Laboratoire des Milieux Désordonnés et Hétérogènes, CNRS-UMR7603, Université Pierre et Marie Curie, 4 place Jussieu, case 86</s1>
<s2>75252 Paris</s2>
<s3>FRA</s3>
<sZ>3 aut.</sZ>
<sZ>4 aut.</sZ>
</inist:fA14>
<country>France</country>
</affiliation>
</author>
<author><name sortKey="Julien, C" sort="Julien, C" uniqKey="Julien C" first="C." last="Julien">C. Julien</name>
<affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Laboratoire des Milieux Désordonnés et Hétérogènes, CNRS-UMR7603, Université Pierre et Marie Curie, 4 place Jussieu, case 86</s1>
<s2>75252 Paris</s2>
<s3>FRA</s3>
<sZ>3 aut.</sZ>
<sZ>4 aut.</sZ>
</inist:fA14>
<country>France</country>
</affiliation>
</author>
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<series><title level="j" type="main">Materials chemistry and physics</title>
<title level="j" type="abbreviated">Mater. chem. phys.</title>
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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Aluminium oxides</term>
<term>Chemical synthesis</term>
<term>Citrates</term>
<term>Cobalt oxides</term>
<term>Crystal structure</term>
<term>DTA</term>
<term>Experimental study</term>
<term>Intercalation compounds</term>
<term>Lithium battery</term>
<term>Lithium oxides</term>
<term>Quaternary compounds</term>
<term>Scanning electron microscopy</term>
<term>XRD</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Composé insertion</term>
<term>Citrate</term>
<term>Synthèse chimique</term>
<term>Lithium oxyde</term>
<term>Aluminium oxyde</term>
<term>Cobalt oxyde</term>
<term>Composé quaternaire</term>
<term>Batterie lithium</term>
<term>ATD</term>
<term>Microscopie électronique balayage</term>
<term>Etude expérimentale</term>
<term>Structure cristalline</term>
<term>Diffraction RX</term>
<term>8120K</term>
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<front><div type="abstract" xml:lang="en">We present the synthesis, characterization and electrode behaviour ofLiAl<sub>y</sub>
Co<sub>1-y</sub>
O<sub>2</sub>
(0.0 ≤ y ≤ 0.3) oxides prepared by the citrate route. The phase evolution was studied as a function of the aluminium substitution and the modification on the intercalation and deintercalation of Li ions. Characterization methods include X-ray powder diffraction (XRD), thermogravimetry analysis (TG-DTA), scanning electron microscopy (SEM), Raman scattering (RS) and Fourier transform infrared (FTIR) spectroscopy. Samples belong to the LiCoO<sub>2</sub>
-LiAlO<sub>2</sub>
 solid solution and have the layered α-NaFeO<sub>2</sub>
 structure (R3m space group). Raman scattering and FT-infrared vibrational spectroscopies indicate that the vibrational mode frequencies and relative intensities of the bands are sensitive to the covalency of the (Co, Al)O<sub>2</sub>
 slabs. SEM micrographs show that the particle size of the LiAl<sub>y</sub>
Co<sub>1-y</sub>
O<sub>2</sub>
powders ranges in the submicronic domain with a narrow grain-size distribution. The overall electrochemical capacity of the LiAl<sub>y</sub>
Co<sub>1-y</sub>
O<sub>2</sub>
 oxides have been reduced due to the sp metal substitution, however, a more stable charge-discharge cycling performances have been observed when electrodes are charged up to 4.3V as compared to the performance of the native oxide. For such a cut-off voltage, the charge capacity of the Li//LiAl<sub>0.2</sub>
Co<sub>0.8</sub>
O<sub>2</sub>
 cell is ca. 118 mAh g<sup>-1</sup>
. Kinetics were characterized by the galvanostatic intermittent titration technique (GITT). Aluminium substitution provides an increase of the chemical diffusion coefficients ofLi<sup>+</sup>
 ions in the LiAl<sub>y</sub>
 Co<sub>1-y</sub>
O<sub>2</sub>
 matrix. Differences and similarities between LiCoO<sub>2</sub>
 and Al-substituted oxides are discussed therefrom.</div>
</front>
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<fA06><s2>1</s2>
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<fA08 i1="01" i2="1" l="ENG"><s1>LiAl<sub>y</sub>
Co<sub>1</sub>
-<sub>y</sub>
O<sub>2</sub>
 (0.0 ≤ y ≤ 0.3) intercalation compounds synthesized from the citrate precursors</s1>
</fA08>
<fA11 i1="01" i2="1"><s1>AMDOUNI (N.)</s1>
</fA11>
<fA11 i1="02" i2="1"><s1>ZARROUK (H.)</s1>
</fA11>
<fA11 i1="03" i2="1"><s1>SOULETTE (F.)</s1>
</fA11>
<fA11 i1="04" i2="1"><s1>JULIEN (C.)</s1>
</fA11>
<fA14 i1="01"><s1>Laboratoire de Chimie des Matériaux, Faculté des Sciences de Tunis Université de Tunis El Manar Campus Universitaire</s1>
<s2>2092 El Manar II</s2>
<s3>TUN</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
</fA14>
<fA14 i1="02"><s1>Laboratoire des Milieux Désordonnés et Hétérogènes, CNRS-UMR7603, Université Pierre et Marie Curie, 4 place Jussieu, case 86</s1>
<s2>75252 Paris</s2>
<s3>FRA</s3>
<sZ>3 aut.</sZ>
<sZ>4 aut.</sZ>
</fA14>
<fA20><s1>205-214</s1>
</fA20>
<fA21><s1>2003</s1>
</fA21>
<fA23 i1="01"><s0>ENG</s0>
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<fA43 i1="01"><s1>INIST</s1>
<s2>17552</s2>
<s5>354000118040940340</s5>
</fA43>
<fA44><s0>0000</s0>
<s1>© 2003 INIST-CNRS. All rights reserved.</s1>
</fA44>
<fA45><s0>44 ref.</s0>
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<fA47 i1="01" i2="1"><s0>03-0305472</s0>
</fA47>
<fA60><s1>P</s1>
</fA60>
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</fA64>
<fA66 i1="01"><s0>CHE</s0>
</fA66>
<fC01 i1="01" l="ENG"><s0>We present the synthesis, characterization and electrode behaviour ofLiAl<sub>y</sub>
Co<sub>1-y</sub>
O<sub>2</sub>
(0.0 ≤ y ≤ 0.3) oxides prepared by the citrate route. The phase evolution was studied as a function of the aluminium substitution and the modification on the intercalation and deintercalation of Li ions. Characterization methods include X-ray powder diffraction (XRD), thermogravimetry analysis (TG-DTA), scanning electron microscopy (SEM), Raman scattering (RS) and Fourier transform infrared (FTIR) spectroscopy. Samples belong to the LiCoO<sub>2</sub>
-LiAlO<sub>2</sub>
 solid solution and have the layered α-NaFeO<sub>2</sub>
 structure (R3m space group). Raman scattering and FT-infrared vibrational spectroscopies indicate that the vibrational mode frequencies and relative intensities of the bands are sensitive to the covalency of the (Co, Al)O<sub>2</sub>
 slabs. SEM micrographs show that the particle size of the LiAl<sub>y</sub>
Co<sub>1-y</sub>
O<sub>2</sub>
powders ranges in the submicronic domain with a narrow grain-size distribution. The overall electrochemical capacity of the LiAl<sub>y</sub>
Co<sub>1-y</sub>
O<sub>2</sub>
 oxides have been reduced due to the sp metal substitution, however, a more stable charge-discharge cycling performances have been observed when electrodes are charged up to 4.3V as compared to the performance of the native oxide. For such a cut-off voltage, the charge capacity of the Li//LiAl<sub>0.2</sub>
Co<sub>0.8</sub>
O<sub>2</sub>
 cell is ca. 118 mAh g<sup>-1</sup>
. Kinetics were characterized by the galvanostatic intermittent titration technique (GITT). Aluminium substitution provides an increase of the chemical diffusion coefficients ofLi<sup>+</sup>
 ions in the LiAl<sub>y</sub>
 Co<sub>1-y</sub>
O<sub>2</sub>
 matrix. Differences and similarities between LiCoO<sub>2</sub>
 and Al-substituted oxides are discussed therefrom.</s0>
</fC01>
<fC02 i1="01" i2="3"><s0>001B80A20</s0>
</fC02>
<fC03 i1="01" i2="3" l="FRE"><s0>Composé insertion</s0>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="3" l="ENG"><s0>Intercalation compounds</s0>
<s5>01</s5>
</fC03>
<fC03 i1="02" i2="3" l="FRE"><s0>Citrate</s0>
<s2>NK</s2>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="3" l="ENG"><s0>Citrates</s0>
<s2>NK</s2>
<s5>02</s5>
</fC03>
<fC03 i1="03" i2="X" l="FRE"><s0>Synthèse chimique</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="X" l="ENG"><s0>Chemical synthesis</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="X" l="SPA"><s0>Síntesis química</s0>
<s5>03</s5>
</fC03>
<fC03 i1="04" i2="3" l="FRE"><s0>Lithium oxyde</s0>
<s2>NK</s2>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="3" l="ENG"><s0>Lithium oxides</s0>
<s2>NK</s2>
<s5>04</s5>
</fC03>
<fC03 i1="05" i2="3" l="FRE"><s0>Aluminium oxyde</s0>
<s2>NK</s2>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="3" l="ENG"><s0>Aluminium oxides</s0>
<s2>NK</s2>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="3" l="FRE"><s0>Cobalt oxyde</s0>
<s2>NK</s2>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="3" l="ENG"><s0>Cobalt oxides</s0>
<s2>NK</s2>
<s5>06</s5>
</fC03>
<fC03 i1="07" i2="3" l="FRE"><s0>Composé quaternaire</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="3" l="ENG"><s0>Quaternary compounds</s0>
<s5>07</s5>
</fC03>
<fC03 i1="08" i2="3" l="FRE"><s0>Batterie lithium</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="3" l="ENG"><s0>Lithium battery</s0>
<s5>08</s5>
</fC03>
<fC03 i1="09" i2="3" l="FRE"><s0>ATD</s0>
<s5>10</s5>
</fC03>
<fC03 i1="09" i2="3" l="ENG"><s0>DTA</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="3" l="FRE"><s0>Microscopie électronique balayage</s0>
<s5>11</s5>
</fC03>
<fC03 i1="10" i2="3" l="ENG"><s0>Scanning electron microscopy</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="3" l="FRE"><s0>Etude expérimentale</s0>
<s5>12</s5>
</fC03>
<fC03 i1="11" i2="3" l="ENG"><s0>Experimental study</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="3" l="FRE"><s0>Structure cristalline</s0>
<s5>23</s5>
</fC03>
<fC03 i1="12" i2="3" l="ENG"><s0>Crystal structure</s0>
<s5>23</s5>
</fC03>
<fC03 i1="13" i2="3" l="FRE"><s0>Diffraction RX</s0>
<s5>24</s5>
</fC03>
<fC03 i1="13" i2="3" l="ENG"><s0>XRD</s0>
<s5>24</s5>
</fC03>
<fC03 i1="14" i2="3" l="FRE"><s0>8120K</s0>
<s2>PAC</s2>
<s4>INC</s4>
<s5>95</s5>
</fC03>
<fN21><s1>202</s1>
</fN21>
<fN82><s1>PSI</s1>
</fN82>
</pA>
</standard>
</inist>
</record>

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   |area=    CobaltMaghrebV1
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   |texte=   LiAlyCo1-yO2 (0.0 ≤ y ≤ 0.3) intercalation compounds synthesized from the citrate precursors
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	Serveur d'exploration sur le cobalt au Maghreb
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Serveur d'exploration sur le cobalt au Maghreb

LiAlyCo1-yO2 (0.0 ≤ y ≤ 0.3) intercalation compounds synthesized from the citrate precursors

LiAlyCo1-yO2 (0.0 ≤ y ≤ 0.3) intercalation compounds synthesized from the citrate precursors

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