CobaltMaghrebV1, PascalFrancis, Curation, bibRecord, 000003

Structural characterization of a series of cyclohexaphosphates : M0.5((C6H5CH2)2NH2)5P6O18-H2O (M = Co, Cu, Cd)

Identifieur interne : 000003 ( PascalFrancis/Curation ); précédent : 000002; suivant : 000004

Structural characterization of a series of cyclohexaphosphates : M0.5((C6H5CH2)2NH2)5P6O18-H2O (M = Co, Cu, Cd)

Auteurs : S. Abid [Tunisie] ; M. Rzaigui [Tunisie] ; M. Bagieu-Beucher [France]

Source :

Journal of chemical crystallography [ 1074-1542 ] ; 1999.

RBID : Pascal:00-0210809

Descripteurs français

Pascal (Inist)
- Etude expérimentale, Préparation chimique, Diffraction RX, Structure cristalline, Structure moléculaire, Phosphate cyclique, Cation organique, Cuivre composé, Cadmium composé, Cobalt composé, Spectre IR, Analyse thermique, 6166F, Cyclohexaphosphate, Ammonium(dibenzyl).

English descriptors

KwdEn :
- Cadmium compounds, Chemical preparation, Cobalt compounds, Copper compounds, Crystal structure, Cyclophosphate, Experimental study, Infrared spectra, Molecular structure, Organic cation, Thermal analysis, XRD.

Abstract

Three new cyclohexaphosphates with general formula M_0.5((C₆H₅CH₂)₂NH₂)₅P₆O₁₈-H₂O (M=Co, Cu, Cd) are reported. They crystallize with monoclinic unit-cells and are isotropic. We have determined their structure from the salt M = Co. This later exhibits the following unit-cell parameters: a = 22.739(5), b = 17.682(3), c = 18.342(3) Å, β = 91.22(1)°, Z = 4 P2₁/n, V = 7373 Å³, and Dx = 1.373 g cm^-3. The atomic arrangement can be described as layers containing P₆O₁₈ ring anions and CoO₆ octahedra spreading in the (101) planes and intercalated by the dibenzylammonium groups and the water molecules. Synthesis and charac terization by X-ray diffraction, IR absorption, and TA are described.

A01	`01`	`1`		`@0 1074-1542`
A03		`1`		`@0 J. chem. crystallogr.`
A05				`@2 29`
A06				`@2 8`
A08	`01`	`1`	`ENG`	`@1 Structural characterization of a series of cyclohexaphosphates : M_0.5((C₆H₅CH₂)₂NH₂)₅P₆O₁₈-H₂O (M = Co, Cu, Cd)`
A11	`01`	`1`		`@1 ABID (S.)`
A11	`02`	`1`		`@1 RZAIGUI (M.)`
A11	`03`	`1`		`@1 BAGIEU-BEUCHER (M.)`
A14	`01`			`@1 Laboratoire de Chimie des Matériaux, Faculté des Sciences de Bizerte @2 7021-Zarzouna @3 TUN @Z 1 aut. @Z 2 aut.`
A14	`02`			`@1 Laboratoire de Cristallographie associé à l'Université J. Fourier, C.N.R.S., BP. 166 @2 38042 Grenoble @3 FRA @Z 3 aut.`
A20				`@1 891-899`
A21				`@1 1999`
A23	`01`			`@0 ENG`
A43	`01`			`@1 INIST @2 15151 @5 354000082355420050`
A44				`@0 0000 @1 © 2000 INIST-CNRS. All rights reserved.`
A45				`@0 15 ref.`
A47	`01`	`1`		`@0 00-0210809`
A60				`@1 P`
A61				`@0 A`
A64	`01`	`1`		`@0 Journal of chemical crystallography`
A66	`01`			`@0 USA`
C01	`01`		`ENG`	@0 Three new cyclohexaphosphates with general formula M_0.5((C₆H₅CH₂)₂NH₂)₅P₆O₁₈-H₂O (M=Co, Cu, Cd) are reported. They crystallize with monoclinic unit-cells and are isotropic. We have determined their structure from the salt M = Co. This later exhibits the following unit-cell parameters: a = 22.739(5), b = 17.682(3), c = 18.342(3) Å, β = 91.22(1)°, Z = 4 P2₁/n, V = 7373 Å³, and Dx = 1.373 g cm^-3. The atomic arrangement can be described as layers containing P₆O₁₈ ring anions and CoO₆ octahedra spreading in the (101) planes and intercalated by the dibenzylammonium groups and the water molecules. Synthesis and charac terization by X-ray diffraction, IR absorption, and TA are described.
C02	`01`	`3`		`@0 001B60A66F4`
C02	`02`	`3`		`@0 001B60A66F5`
C03	`01`	`3`	`FRE`	`@0 Etude expérimentale @5 01`
C03	`01`	`3`	`ENG`	`@0 Experimental study @5 01`
C03	`02`	`3`	`FRE`	`@0 Préparation chimique @5 02`
C03	`02`	`3`	`ENG`	`@0 Chemical preparation @5 02`
C03	`03`	`3`	`FRE`	`@0 Diffraction RX @5 03`
C03	`03`	`3`	`ENG`	`@0 XRD @5 03`
C03	`04`	`3`	`FRE`	`@0 Structure cristalline @5 04`
C03	`04`	`3`	`ENG`	`@0 Crystal structure @5 04`
C03	`05`	`3`	`FRE`	`@0 Structure moléculaire @5 05`
C03	`05`	`3`	`ENG`	`@0 Molecular structure @5 05`
C03	`06`	`X`	`FRE`	`@0 Phosphate cyclique @5 07`
C03	`06`	`X`	`ENG`	`@0 Cyclophosphate @5 07`
C03	`06`	`X`	`SPA`	`@0 Ciclofosfato @5 07`
C03	`07`	`X`	`FRE`	`@0 Cation organique @5 09`
C03	`07`	`X`	`ENG`	`@0 Organic cation @5 09`
C03	`07`	`X`	`SPA`	`@0 Catión orgánico @5 09`
C03	`08`	`3`	`FRE`	`@0 Cuivre composé @5 11`
C03	`08`	`3`	`ENG`	`@0 Copper compounds @5 11`
C03	`09`	`3`	`FRE`	`@0 Cadmium composé @5 12`
C03	`09`	`3`	`ENG`	`@0 Cadmium compounds @5 12`
C03	`10`	`3`	`FRE`	`@0 Cobalt composé @5 13`
C03	`10`	`3`	`ENG`	`@0 Cobalt compounds @5 13`
C03	`11`	`3`	`FRE`	`@0 Spectre IR @5 14`
C03	`11`	`3`	`ENG`	`@0 Infrared spectra @5 14`
C03	`12`	`3`	`FRE`	`@0 Analyse thermique @5 15`
C03	`12`	`3`	`ENG`	`@0 Thermal analysis @5 15`
C03	`13`	`3`	`FRE`	`@0 6166F @2 PAC @4 INC @5 56`
C03	`14`	`3`	`FRE`	`@0 Cyclohexaphosphate @2 NK @4 INC @5 92`
C03	`15`	`3`	`FRE`	`@0 Ammonium(dibenzyl) @2 NK @4 INC @5 93`
C07	`01`	`3`	`FRE`	`@0 Composé minéral @5 06`
C07	`01`	`3`	`ENG`	`@0 Inorganic compounds @5 06`
C07	`02`	`3`	`FRE`	`@0 Composé organique @5 08`
C07	`02`	`3`	`ENG`	`@0 Organic compounds @5 08`
C07	`03`	`X`	`FRE`	`@0 Ammonium Composé organique @2 NC @2 NA @5 10`
C07	`03`	`X`	`ENG`	`@0 Ammonium Organic compounds @2 NC @2 NA @5 10`
C07	`03`	`X`	`SPA`	`@0 Amonio Compuesto orgánico @2 NC @2 NA @5 10`
N21				`@1 150`

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Le document en format XML

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((C<sub>6</sub>
H<sub>5</sub>
CH<sub>2</sub>
)<sub>2</sub>
NH<sub>2</sub>
)<sub>5</sub>
P<sub>6</sub>
O<sub>18</sub>
-H<sub>2</sub>
O (M = Co, Cu, Cd)</title>
<author><name sortKey="Abid, S" sort="Abid, S" uniqKey="Abid S" first="S." last="Abid">S. Abid</name>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a">Structural characterization of a series of cyclohexaphosphates : M<sub>0.5</sub>
((C<sub>6</sub>
H<sub>5</sub>
CH<sub>2</sub>
)<sub>2</sub>
NH<sub>2</sub>
)<sub>5</sub>
P<sub>6</sub>
O<sub>18</sub>
-H<sub>2</sub>
O (M = Co, Cu, Cd)</title>
<author><name sortKey="Abid, S" sort="Abid, S" uniqKey="Abid S" first="S." last="Abid">S. Abid</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Laboratoire de Chimie des Matériaux, Faculté des Sciences de Bizerte</s1>
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<sZ>2 aut.</sZ>
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<author><name sortKey="Bagieu Beucher, M" sort="Bagieu Beucher, M" uniqKey="Bagieu Beucher M" first="M." last="Bagieu-Beucher">M. Bagieu-Beucher</name>
<affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Laboratoire de Cristallographie associé à l'Université J. Fourier, C.N.R.S., BP. 166</s1>
<s2>38042 Grenoble</s2>
<s3>FRA</s3>
<sZ>3 aut.</sZ>
</inist:fA14>
<country>France</country>
</affiliation>
</author>
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<series><title level="j" type="main">Journal of chemical crystallography</title>
<title level="j" type="abbreviated">J. chem. crystallogr.</title>
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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Cadmium compounds</term>
<term>Chemical preparation</term>
<term>Cobalt compounds</term>
<term>Copper compounds</term>
<term>Crystal structure</term>
<term>Cyclophosphate</term>
<term>Experimental study</term>
<term>Infrared spectra</term>
<term>Molecular structure</term>
<term>Organic cation</term>
<term>Thermal analysis</term>
<term>XRD</term>
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<keywords scheme="Pascal" xml:lang="fr"><term>Etude expérimentale</term>
<term>Préparation chimique</term>
<term>Diffraction RX</term>
<term>Structure cristalline</term>
<term>Structure moléculaire</term>
<term>Phosphate cyclique</term>
<term>Cation organique</term>
<term>Cuivre composé</term>
<term>Cadmium composé</term>
<term>Cobalt composé</term>
<term>Spectre IR</term>
<term>Analyse thermique</term>
<term>6166F</term>
<term>Cyclohexaphosphate</term>
<term>Ammonium(dibenzyl)</term>
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<front><div type="abstract" xml:lang="en">Three new cyclohexaphosphates with general formula M<sub>0.5</sub>
((C<sub>6</sub>
H<sub>5</sub>
CH<sub>2</sub>
)<sub>2</sub>
NH<sub>2</sub>
)<sub>5</sub>
P<sub>6</sub>
O<sub>18</sub>
-H<sub>2</sub>
O (M=Co, Cu, Cd) are reported. They crystallize with monoclinic unit-cells and are isotropic. We have determined their structure from the salt M = Co. This later exhibits the following unit-cell parameters: a = 22.739(5), b = 17.682(3), c = 18.342(3) Å, β = 91.22(1)°, Z = 4 P2<sub>1</sub>
/n, V = 7373 Å<sup>3</sup>
, and Dx = 1.373 g cm<sup>-3</sup>
. The atomic arrangement can be described as layers containing P<sub>6</sub>
O<sub>18</sub>
 ring anions and CoO<sub>6</sub>
 octahedra spreading in the (101) planes and intercalated by the dibenzylammonium groups and the water molecules. Synthesis and charac terization by X-ray diffraction, IR absorption, and TA are described.</div>
</front>
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<fA06><s2>8</s2>
</fA06>
<fA08 i1="01" i2="1" l="ENG"><s1>Structural characterization of a series of cyclohexaphosphates : M<sub>0.5</sub>
((C<sub>6</sub>
H<sub>5</sub>
CH<sub>2</sub>
)<sub>2</sub>
NH<sub>2</sub>
)<sub>5</sub>
P<sub>6</sub>
O<sub>18</sub>
-H<sub>2</sub>
O (M = Co, Cu, Cd)</s1>
</fA08>
<fA11 i1="01" i2="1"><s1>ABID (S.)</s1>
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<fA11 i1="02" i2="1"><s1>RZAIGUI (M.)</s1>
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<fA11 i1="03" i2="1"><s1>BAGIEU-BEUCHER (M.)</s1>
</fA11>
<fA14 i1="01"><s1>Laboratoire de Chimie des Matériaux, Faculté des Sciences de Bizerte</s1>
<s2>7021-Zarzouna</s2>
<s3>TUN</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
</fA14>
<fA14 i1="02"><s1>Laboratoire de Cristallographie associé à l'Université J. Fourier, C.N.R.S., BP. 166</s1>
<s2>38042 Grenoble</s2>
<s3>FRA</s3>
<sZ>3 aut.</sZ>
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<fA20><s1>891-899</s1>
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<fA60><s1>P</s1>
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<fA66 i1="01"><s0>USA</s0>
</fA66>
<fC01 i1="01" l="ENG"><s0>Three new cyclohexaphosphates with general formula M<sub>0.5</sub>
((C<sub>6</sub>
H<sub>5</sub>
CH<sub>2</sub>
)<sub>2</sub>
NH<sub>2</sub>
)<sub>5</sub>
P<sub>6</sub>
O<sub>18</sub>
-H<sub>2</sub>
O (M=Co, Cu, Cd) are reported. They crystallize with monoclinic unit-cells and are isotropic. We have determined their structure from the salt M = Co. This later exhibits the following unit-cell parameters: a = 22.739(5), b = 17.682(3), c = 18.342(3) Å, β = 91.22(1)°, Z = 4 P2<sub>1</sub>
/n, V = 7373 Å<sup>3</sup>
, and Dx = 1.373 g cm<sup>-3</sup>
. The atomic arrangement can be described as layers containing P<sub>6</sub>
O<sub>18</sub>
 ring anions and CoO<sub>6</sub>
 octahedra spreading in the (101) planes and intercalated by the dibenzylammonium groups and the water molecules. Synthesis and charac terization by X-ray diffraction, IR absorption, and TA are described.</s0>
</fC01>
<fC02 i1="01" i2="3"><s0>001B60A66F4</s0>
</fC02>
<fC02 i1="02" i2="3"><s0>001B60A66F5</s0>
</fC02>
<fC03 i1="01" i2="3" l="FRE"><s0>Etude expérimentale</s0>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="3" l="ENG"><s0>Experimental study</s0>
<s5>01</s5>
</fC03>
<fC03 i1="02" i2="3" l="FRE"><s0>Préparation chimique</s0>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="3" l="ENG"><s0>Chemical preparation</s0>
<s5>02</s5>
</fC03>
<fC03 i1="03" i2="3" l="FRE"><s0>Diffraction RX</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="3" l="ENG"><s0>XRD</s0>
<s5>03</s5>
</fC03>
<fC03 i1="04" i2="3" l="FRE"><s0>Structure cristalline</s0>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="3" l="ENG"><s0>Crystal structure</s0>
<s5>04</s5>
</fC03>
<fC03 i1="05" i2="3" l="FRE"><s0>Structure moléculaire</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="3" l="ENG"><s0>Molecular structure</s0>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="X" l="FRE"><s0>Phosphate cyclique</s0>
<s5>07</s5>
</fC03>
<fC03 i1="06" i2="X" l="ENG"><s0>Cyclophosphate</s0>
<s5>07</s5>
</fC03>
<fC03 i1="06" i2="X" l="SPA"><s0>Ciclofosfato</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="FRE"><s0>Cation organique</s0>
<s5>09</s5>
</fC03>
<fC03 i1="07" i2="X" l="ENG"><s0>Organic cation</s0>
<s5>09</s5>
</fC03>
<fC03 i1="07" i2="X" l="SPA"><s0>Catión orgánico</s0>
<s5>09</s5>
</fC03>
<fC03 i1="08" i2="3" l="FRE"><s0>Cuivre composé</s0>
<s5>11</s5>
</fC03>
<fC03 i1="08" i2="3" l="ENG"><s0>Copper compounds</s0>
<s5>11</s5>
</fC03>
<fC03 i1="09" i2="3" l="FRE"><s0>Cadmium composé</s0>
<s5>12</s5>
</fC03>
<fC03 i1="09" i2="3" l="ENG"><s0>Cadmium compounds</s0>
<s5>12</s5>
</fC03>
<fC03 i1="10" i2="3" l="FRE"><s0>Cobalt composé</s0>
<s5>13</s5>
</fC03>
<fC03 i1="10" i2="3" l="ENG"><s0>Cobalt compounds</s0>
<s5>13</s5>
</fC03>
<fC03 i1="11" i2="3" l="FRE"><s0>Spectre IR</s0>
<s5>14</s5>
</fC03>
<fC03 i1="11" i2="3" l="ENG"><s0>Infrared spectra</s0>
<s5>14</s5>
</fC03>
<fC03 i1="12" i2="3" l="FRE"><s0>Analyse thermique</s0>
<s5>15</s5>
</fC03>
<fC03 i1="12" i2="3" l="ENG"><s0>Thermal analysis</s0>
<s5>15</s5>
</fC03>
<fC03 i1="13" i2="3" l="FRE"><s0>6166F</s0>
<s2>PAC</s2>
<s4>INC</s4>
<s5>56</s5>
</fC03>
<fC03 i1="14" i2="3" l="FRE"><s0>Cyclohexaphosphate</s0>
<s2>NK</s2>
<s4>INC</s4>
<s5>92</s5>
</fC03>
<fC03 i1="15" i2="3" l="FRE"><s0>Ammonium(dibenzyl)</s0>
<s2>NK</s2>
<s4>INC</s4>
<s5>93</s5>
</fC03>
<fC07 i1="01" i2="3" l="FRE"><s0>Composé minéral</s0>
<s5>06</s5>
</fC07>
<fC07 i1="01" i2="3" l="ENG"><s0>Inorganic compounds</s0>
<s5>06</s5>
</fC07>
<fC07 i1="02" i2="3" l="FRE"><s0>Composé organique</s0>
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<fC07 i1="02" i2="3" l="ENG"><s0>Organic compounds</s0>
<s5>08</s5>
</fC07>
<fC07 i1="03" i2="X" l="FRE"><s0>Ammonium Composé organique</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>10</s5>
</fC07>
<fC07 i1="03" i2="X" l="ENG"><s0>Ammonium Organic compounds</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>10</s5>
</fC07>
<fC07 i1="03" i2="X" l="SPA"><s0>Amonio Compuesto orgánico</s0>
<s2>NC</s2>
<s2>NA</s2>
<s5>10</s5>
</fC07>
<fN21><s1>150</s1>
</fN21>
</pA>
</standard>
</inist>
</record>

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   |texte=   Structural characterization of a series of cyclohexaphosphates : M0.5((C6H5CH2)2NH2)5P6O18-H2O (M = Co, Cu, Cd)
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	Serveur d'exploration sur le cobalt au Maghreb
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Serveur d'exploration sur le cobalt au Maghreb

Structural characterization of a series of cyclohexaphosphates : M0.5((C6H5CH2)2NH2)5P6O18-H2O (M = Co, Cu, Cd)

Structural characterization of a series of cyclohexaphosphates : M0.5((C6H5CH2)2NH2)5P6O18-H2O (M = Co, Cu, Cd)

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