CobaltMaghrebV1, PascalFrancis, Corpus, bibRecord, 000348

Influence of preparation method on catalytic properties of mixed calcium-cobalt orthophosphates

Identifieur interne : 000348 ( PascalFrancis/Corpus ); précédent : 000347; suivant : 000349

Influence of preparation method on catalytic properties of mixed calcium-cobalt orthophosphates

Auteurs : A. Legrouri ; S. S. Romdhane ; J. Lenzi ; M. Lenzi ; G. Bonel

Source :

Journal of materials science [ 0022-2461 ] ; 1996.

RBID : Pascal:96-0276914

Descripteurs français

Pascal (Inist)
- Activité catalytique, Préparation, Coprécipitation, Cobalt Phosphate, Calcium Phosphate, Ca3-xCox(PO4)2, C Ca O P.

English descriptors

KwdEn :
- Calcium Phosphates, Catalyst activity, Cobalt Phosphates, Coprecipitation, Preparation.

Abstract

Mixed calcium-cobalt orthophosphates of the formula Ca_3-xCO_x(PO₄)₂, with 0 ≤ x ≤ 1.1, were prepared by coprecipitation and solid-state reaction. Structural characterization showed that, in both cases, the solids obtained resulted from substitution of some Ca²⁺ ions by Co²⁺ ions in the β-Ca₃(PO₄)₂ structure. The solubility limit of cobalt in this structure corresponded to x = 0.31. The morphology of these compounds was investigated by surface-area measurements and scanning electron microscopy. When tested in the 2-propanol decomposition reaction, the maximum activity in dehydrogenation was obtained with the compound corresponding to cobalt maximum solubility in β-Ca₃(PO₄)₂ structure. Higher activities were obtained for samples prepared by coprecipitation.

Notice en format standard (ISO 2709)

Pour connaître la documentation sur le format Inist Standard.

A01	`01`	`1`		`@0 0022-2461`
A02	`01`			`@0 JMTSAS`
A03		`1`		`@0 J. mater. sci.`
A05				`@2 31`
A06				`@2 9`
A08	`01`	`1`	`ENG`	`@1 Influence of preparation method on catalytic properties of mixed calcium-cobalt orthophosphates`
A11	`01`	`1`		`@1 LEGROURI (A.)`
A11	`02`	`1`		`@1 ROMDHANE (S. S.)`
A11	`03`	`1`		`@1 LENZI (J.)`
A11	`04`	`1`		`@1 LENZI (M.)`
A11	`05`	`1`		`@1 BONEL (G.)`
A14	`01`			`@1 School of Science and Engineering, Al Akhawayn University, P.O. Box 104 @2 5300 Ifrane @3 MAR @Z 1 aut.`
A14	`02`			`@1 Centre de Génie Photochimique, Ecole Nationale Supérieure de Chimie, 118, Route de Narbornne @2 31077 Toulouse @3 FRA @Z 3 aut. @Z 4 aut.`
A14	`03`			`@1 Laboratoire de Physicochimie des Solides, 38, Rue dees 36-Ponts @2 31400 Toulouse @3 FRA @Z 5 aut.`
A20				`@1 2469-2473`
A21				`@1 1996`
A23	`01`			`@0 ENG`
A43	`01`			`@1 INIST @2 12733 @5 354000043597590330`
A44				`@0 0000`
A45				`@0 30 ref.`
A47	`01`	`1`		`@0 96-0276914`
A60				`@1 P`
A61				`@0 A`
A64	`01`	`1`		`@0 Journal of materials science`
A66	`01`			`@0 GBR`
C01	`01`		`ENG`	@0 Mixed calcium-cobalt orthophosphates of the formula Ca_3-xCO_x(PO₄)₂, with 0 ≤ x ≤ 1.1, were prepared by coprecipitation and solid-state reaction. Structural characterization showed that, in both cases, the solids obtained resulted from substitution of some Ca²⁺ ions by Co²⁺ ions in the β-Ca₃(PO₄)₂ structure. The solubility limit of cobalt in this structure corresponded to x = 0.31. The morphology of these compounds was investigated by surface-area measurements and scanning electron microscopy. When tested in the 2-propanol decomposition reaction, the maximum activity in dehydrogenation was obtained with the compound corresponding to cobalt maximum solubility in β-Ca₃(PO₄)₂ structure. Higher activities were obtained for samples prepared by coprecipitation.
C02	`01`	`X`		`@0 001C01A03A`
C03	`01`	`X`	`FRE`	`@0 Activité catalytique @5 01`
C03	`01`	`X`	`ENG`	`@0 Catalyst activity @5 01`
C03	`01`	`X`	`SPA`	`@0 Actividad catalítica @5 01`
C03	`02`	`X`	`FRE`	`@0 Préparation @5 02`
C03	`02`	`X`	`ENG`	`@0 Preparation @5 02`
C03	`02`	`X`	`GER`	`@0 Vorbereitung @5 02`
C03	`02`	`X`	`SPA`	`@0 Preparación @5 02`
C03	`03`	`X`	`FRE`	`@0 Coprécipitation @5 04`
C03	`03`	`X`	`ENG`	`@0 Coprecipitation @5 04`
C03	`03`	`X`	`SPA`	`@0 Coprecipitación @5 04`
C03	`04`	`X`	`FRE`	`@0 Cobalt Phosphate @1 ACT @2 NC @2 NA @5 13`
C03	`04`	`X`	`ENG`	`@0 Cobalt Phosphates @1 ACT @2 NC @2 NA @5 13`
C03	`04`	`X`	`SPA`	`@0 Cobalto Fosfato @1 ACT @2 NC @2 NA @5 13`
C03	`05`	`X`	`FRE`	`@0 Calcium Phosphate @1 ACT @2 NC @2 FR @2 NA @5 14`
C03	`05`	`X`	`ENG`	`@0 Calcium Phosphates @1 ACT @2 NC @2 FR @2 NA @5 14`
C03	`05`	`X`	`SPA`	`@0 Calcio Fosfato @1 ACT @2 NC @2 FR @2 NA @5 14`
C03	`06`	`X`	`FRE`	`@0 Ca3-xCox(PO4)2 @4 INC @5 75`
C03	`07`	`X`	`FRE`	`@0 C Ca O P @4 INC @5 76`
N21				`@1 190`

Format Inist (serveur)

NO :	PASCAL 96-0276914 INIST
ET :	Influence of preparation method on catalytic properties of mixed calcium-cobalt orthophosphates
AU :	LEGROURI (A.); ROMDHANE (S. S.); LENZI (J.); LENZI (M.); BONEL (G.)
AF :	School of Science and Engineering, Al Akhawayn University, P.O. Box 104/5300 Ifrane/Maroc (1 aut.); Centre de Génie Photochimique, Ecole Nationale Supérieure de Chimie, 118, Route de Narbornne/31077 Toulouse/France (3 aut., 4 aut.); Laboratoire de Physicochimie des Solides, 38, Rue dees 36-Ponts/31400 Toulouse/France (5 aut.)
DT :	Publication en série; Niveau analytique
SO :	Journal of materials science; ISSN 0022-2461; Coden JMTSAS; Royaume-Uni; Da. 1996; Vol. 31; No. 9; Pp. 2469-2473; Bibl. 30 ref.
LA :	Anglais
EA :	Mixed calcium-cobalt orthophosphates of the formula Ca_3-xCO_x(PO₄)₂, with 0 ≤ x ≤ 1.1, were prepared by coprecipitation and solid-state reaction. Structural characterization showed that, in both cases, the solids obtained resulted from substitution of some Ca²⁺ ions by Co²⁺ ions in the β-Ca₃(PO₄)₂ structure. The solubility limit of cobalt in this structure corresponded to x = 0.31. The morphology of these compounds was investigated by surface-area measurements and scanning electron microscopy. When tested in the 2-propanol decomposition reaction, the maximum activity in dehydrogenation was obtained with the compound corresponding to cobalt maximum solubility in β-Ca₃(PO₄)₂ structure. Higher activities were obtained for samples prepared by coprecipitation.
CC :	001C01A03A
FD :	Activité catalytique; Préparation; Coprécipitation; Cobalt Phosphate; Calcium Phosphate; Ca3-xCox(PO4)2; C Ca O P
ED :	Catalyst activity; Preparation; Coprecipitation; Cobalt Phosphates; Calcium Phosphates
GD :	Vorbereitung
SD :	Actividad catalítica; Preparación; Coprecipitación; Cobalto Fosfato; Calcio Fosfato
LO :	INIST-12733.354000043597590330
ID :	96-0276914

Links to Exploration step

Pascal:96-0276914

Le document en format XML

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<author><name sortKey="Bonel, G" sort="Bonel, G" uniqKey="Bonel G" first="G." last="Bonel">G. Bonel</name>
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<author><name sortKey="Bonel, G" sort="Bonel, G" uniqKey="Bonel G" first="G." last="Bonel">G. Bonel</name>
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<series><title level="j" type="main">Journal of materials science</title>
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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Calcium Phosphates</term>
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<keywords scheme="Pascal" xml:lang="fr"><term>Activité catalytique</term>
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<front><div type="abstract" xml:lang="en">Mixed calcium-cobalt orthophosphates of the formula Ca<sub>3-x</sub>
CO<sub>x</sub>
(PO<sub>4</sub>
)<sub>2</sub>
, with 0 ≤ x ≤ 1.1, were prepared by coprecipitation and solid-state reaction. Structural characterization showed that, in both cases, the solids obtained resulted from substitution of some Ca<sup>2+</sup>
 ions by Co<sup>2+</sup>
 ions in the β-Ca<sub>3</sub>
(PO<sub>4</sub>
)<sub>2</sub>
 structure. The solubility limit of cobalt in this structure corresponded to x = 0.31. The morphology of these compounds was investigated by surface-area measurements and scanning electron microscopy. When tested in the 2-propanol decomposition reaction, the maximum activity in dehydrogenation was obtained with the compound corresponding to cobalt maximum solubility in β-Ca<sub>3</sub>
(PO<sub>4</sub>
)<sub>2</sub>
 structure. Higher activities were obtained for samples prepared by coprecipitation.</div>
</front>
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<inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>0022-2461</s0>
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<fA11 i1="01" i2="1"><s1>LEGROURI (A.)</s1>
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<fA11 i1="05" i2="1"><s1>BONEL (G.)</s1>
</fA11>
<fA14 i1="01"><s1>School of Science and Engineering, Al Akhawayn University, P.O. Box 104</s1>
<s2>5300 Ifrane</s2>
<s3>MAR</s3>
<sZ>1 aut.</sZ>
</fA14>
<fA14 i1="02"><s1>Centre de Génie Photochimique, Ecole Nationale Supérieure de Chimie, 118, Route de Narbornne</s1>
<s2>31077 Toulouse</s2>
<s3>FRA</s3>
<sZ>3 aut.</sZ>
<sZ>4 aut.</sZ>
</fA14>
<fA14 i1="03"><s1>Laboratoire de Physicochimie des Solides, 38, Rue dees 36-Ponts</s1>
<s2>31400 Toulouse</s2>
<s3>FRA</s3>
<sZ>5 aut.</sZ>
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<fA20><s1>2469-2473</s1>
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<fA60><s1>P</s1>
</fA60>
<fA61><s0>A</s0>
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</fA64>
<fA66 i1="01"><s0>GBR</s0>
</fA66>
<fC01 i1="01" l="ENG"><s0>Mixed calcium-cobalt orthophosphates of the formula Ca<sub>3-x</sub>
CO<sub>x</sub>
(PO<sub>4</sub>
)<sub>2</sub>
, with 0 ≤ x ≤ 1.1, were prepared by coprecipitation and solid-state reaction. Structural characterization showed that, in both cases, the solids obtained resulted from substitution of some Ca<sup>2+</sup>
 ions by Co<sup>2+</sup>
 ions in the β-Ca<sub>3</sub>
(PO<sub>4</sub>
)<sub>2</sub>
 structure. The solubility limit of cobalt in this structure corresponded to x = 0.31. The morphology of these compounds was investigated by surface-area measurements and scanning electron microscopy. When tested in the 2-propanol decomposition reaction, the maximum activity in dehydrogenation was obtained with the compound corresponding to cobalt maximum solubility in β-Ca<sub>3</sub>
(PO<sub>4</sub>
)<sub>2</sub>
 structure. Higher activities were obtained for samples prepared by coprecipitation.</s0>
</fC01>
<fC02 i1="01" i2="X"><s0>001C01A03A</s0>
</fC02>
<fC03 i1="01" i2="X" l="FRE"><s0>Activité catalytique</s0>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="X" l="ENG"><s0>Catalyst activity</s0>
<s5>01</s5>
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<s5>01</s5>
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<fC03 i1="02" i2="X" l="FRE"><s0>Préparation</s0>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="ENG"><s0>Preparation</s0>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="GER"><s0>Vorbereitung</s0>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="SPA"><s0>Preparación</s0>
<s5>02</s5>
</fC03>
<fC03 i1="03" i2="X" l="FRE"><s0>Coprécipitation</s0>
<s5>04</s5>
</fC03>
<fC03 i1="03" i2="X" l="ENG"><s0>Coprecipitation</s0>
<s5>04</s5>
</fC03>
<fC03 i1="03" i2="X" l="SPA"><s0>Coprecipitación</s0>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="X" l="FRE"><s0>Cobalt Phosphate</s0>
<s1>ACT</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>13</s5>
</fC03>
<fC03 i1="04" i2="X" l="ENG"><s0>Cobalt Phosphates</s0>
<s1>ACT</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>13</s5>
</fC03>
<fC03 i1="04" i2="X" l="SPA"><s0>Cobalto Fosfato</s0>
<s1>ACT</s1>
<s2>NC</s2>
<s2>NA</s2>
<s5>13</s5>
</fC03>
<fC03 i1="05" i2="X" l="FRE"><s0>Calcium Phosphate</s0>
<s1>ACT</s1>
<s2>NC</s2>
<s2>FR</s2>
<s2>NA</s2>
<s5>14</s5>
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<fC03 i1="05" i2="X" l="ENG"><s0>Calcium Phosphates</s0>
<s1>ACT</s1>
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<s2>FR</s2>
<s2>NA</s2>
<s5>14</s5>
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<fC03 i1="05" i2="X" l="SPA"><s0>Calcio Fosfato</s0>
<s1>ACT</s1>
<s2>NC</s2>
<s2>FR</s2>
<s2>NA</s2>
<s5>14</s5>
</fC03>
<fC03 i1="06" i2="X" l="FRE"><s0>Ca3-xCox(PO4)2</s0>
<s4>INC</s4>
<s5>75</s5>
</fC03>
<fC03 i1="07" i2="X" l="FRE"><s0>C Ca O P</s0>
<s4>INC</s4>
<s5>76</s5>
</fC03>
<fN21><s1>190</s1>
</fN21>
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</standard>
<server><NO>PASCAL 96-0276914 INIST</NO>
<ET>Influence of preparation method on catalytic properties of mixed calcium-cobalt orthophosphates</ET>
<AU>LEGROURI (A.); ROMDHANE (S. S.); LENZI (J.); LENZI (M.); BONEL (G.)</AU>
<AF>School of Science and Engineering, Al Akhawayn University, P.O. Box 104/5300 Ifrane/Maroc (1 aut.); Centre de Génie Photochimique, Ecole Nationale Supérieure de Chimie, 118, Route de Narbornne/31077 Toulouse/France (3 aut., 4 aut.); Laboratoire de Physicochimie des Solides, 38, Rue dees 36-Ponts/31400 Toulouse/France (5 aut.)</AF>
<DT>Publication en série; Niveau analytique</DT>
<SO>Journal of materials science; ISSN 0022-2461; Coden JMTSAS; Royaume-Uni; Da. 1996; Vol. 31; No. 9; Pp. 2469-2473; Bibl. 30 ref.</SO>
<LA>Anglais</LA>
<EA>Mixed calcium-cobalt orthophosphates of the formula Ca<sub>3-x</sub>
CO<sub>x</sub>
(PO<sub>4</sub>
)<sub>2</sub>
, with 0 ≤ x ≤ 1.1, were prepared by coprecipitation and solid-state reaction. Structural characterization showed that, in both cases, the solids obtained resulted from substitution of some Ca<sup>2+</sup>
 ions by Co<sup>2+</sup>
 ions in the β-Ca<sub>3</sub>
(PO<sub>4</sub>
)<sub>2</sub>
 structure. The solubility limit of cobalt in this structure corresponded to x = 0.31. The morphology of these compounds was investigated by surface-area measurements and scanning electron microscopy. When tested in the 2-propanol decomposition reaction, the maximum activity in dehydrogenation was obtained with the compound corresponding to cobalt maximum solubility in β-Ca<sub>3</sub>
(PO<sub>4</sub>
)<sub>2</sub>
 structure. Higher activities were obtained for samples prepared by coprecipitation.</EA>
<CC>001C01A03A</CC>
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<ED>Catalyst activity; Preparation; Coprecipitation; Cobalt Phosphates; Calcium Phosphates</ED>
<GD>Vorbereitung</GD>
<SD>Actividad catalítica; Preparación; Coprecipitación; Cobalto Fosfato; Calcio Fosfato</SD>
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Influence of preparation method on catalytic properties of mixed calcium-cobalt orthophosphates

Influence of preparation method on catalytic properties of mixed calcium-cobalt orthophosphates

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