Serveur d'exploration sur le cobalt au Maghreb

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Amorphisation of Cr-10Co mixture by mechanical alloying

Identifieur interne : 000094 ( PascalFrancis/Corpus ); précédent : 000093; suivant : 000095

Amorphisation of Cr-10Co mixture by mechanical alloying

Auteurs : S. Louidi ; F. Z. Bentayeb ; W. Tebi ; J. J. Sunol ; A. M. Mercier ; J. M. Greneche

Source :

RBID : Pascal:10-0249219

Descripteurs français

English descriptors

Abstract

Mechanical alloying of blended chromium and cobalt powders is carried out in order to obtain a nano-structured Cr-10Co alloy. The alloy formation is studied by means of scanning electron microscopy with energy-dispersive X-ray analysis, X-ray diffraction and differential scanning calorimetry. The results show that an allotropic transformation of Co from fcc to hcp structure occurs within the first 3 h of milling. After 12 h of milling, nanostructured bcc-Cr(Co) solid solution is obtained. Contamination of the powder by the milling tools and atmosphere for 24 h of milling contributes to the formation of a high degree of structural disorder. In addition to Fe, Cr and Co oxides, Cr(Co) solid solutions with bcc and unusual hcp structures are formed. The differential scanning calorimetry analysis in the temperature range 50-700 °C gives evidence for the presence of both microstrain relaxation and crystallization of the amorphous-like structures. Heating the 24 h-milled powder at 600 °C leads to the formation of bcc-Cr, Fe oxide and tetragonal σ-CrCo phases.

Notice en format standard (ISO 2709)

Pour connaître la documentation sur le format Inist Standard.

pA  
A01 01  1    @0 0022-3093
A02 01      @0 JNCSBJ
A03   1    @0 J. non-cryst. solids
A05       @2 356
A06       @2 20-22
A08 01  1  ENG  @1 Amorphisation of Cr-10Co mixture by mechanical alloying
A11 01  1    @1 LOUIDI (S.)
A11 02  1    @1 BENTAYEB (F. Z.)
A11 03  1    @1 TEBI (W.)
A11 04  1    @1 SUNOL (J. J.)
A11 05  1    @1 MERCIER (A. M.)
A11 06  1    @1 GRENECHE (J. M.)
A14 01      @1 Laboratoire de Magnétisme et de Spectroscopie des Solides (LM2S), Département de Physique, Faculté des Sciences, Université de Annaba, B.P. 12 @2 23000 Annaba @3 DZA @Z 1 aut. @Z 2 aut. @Z 3 aut.
A14 02      @1 Dep. Fisica, Universitat Girona, Campus Montilivi @2 17071 Girona @3 ESP @Z 3 aut. @Z 4 aut.
A14 03      @1 Laboratoire des Fluorures, UMR CNRS 6010, Université du Maine @2 72085 Le Mans @3 FRA @Z 5 aut.
A14 04      @1 Laboratoire de Physique de l'Etat Condensé, UMR CNRS 6087, Université du Maine @2 72085 Le Mans @3 FRA @Z 6 aut.
A20       @1 1052-1056
A21       @1 2010
A23 01      @0 ENG
A43 01      @1 INIST @2 14572 @5 354000181735500190
A44       @0 0000 @1 © 2010 INIST-CNRS. All rights reserved.
A45       @0 30 ref.
A47 01  1    @0 10-0249219
A60       @1 P
A61       @0 A
A64 01  1    @0 Journal of non-crystalline solids
A66 01      @0 GBR
C01 01    ENG  @0 Mechanical alloying of blended chromium and cobalt powders is carried out in order to obtain a nano-structured Cr-10Co alloy. The alloy formation is studied by means of scanning electron microscopy with energy-dispersive X-ray analysis, X-ray diffraction and differential scanning calorimetry. The results show that an allotropic transformation of Co from fcc to hcp structure occurs within the first 3 h of milling. After 12 h of milling, nanostructured bcc-Cr(Co) solid solution is obtained. Contamination of the powder by the milling tools and atmosphere for 24 h of milling contributes to the formation of a high degree of structural disorder. In addition to Fe, Cr and Co oxides, Cr(Co) solid solutions with bcc and unusual hcp structures are formed. The differential scanning calorimetry analysis in the temperature range 50-700 °C gives evidence for the presence of both microstrain relaxation and crystallization of the amorphous-like structures. Heating the 24 h-milled powder at 600 °C leads to the formation of bcc-Cr, Fe oxide and tetragonal σ-CrCo phases.
C02 01  3    @0 001B60D70P
C03 01  3  FRE  @0 Amorphisation @5 02
C03 01  3  ENG  @0 Amorphization @5 02
C03 02  3  FRE  @0 Alliage mécanique @5 03
C03 02  3  ENG  @0 Mechanical alloying @5 03
C03 03  3  FRE  @0 Microscopie électronique balayage @5 04
C03 03  3  ENG  @0 Scanning electron microscopy @5 04
C03 04  X  FRE  @0 Spectrométrie dispersive @5 05
C03 04  X  ENG  @0 Dispersive spectrometry @5 05
C03 04  X  SPA  @0 Espectrometría dispersiva @5 05
C03 05  3  FRE  @0 Diffraction RX @5 06
C03 05  3  ENG  @0 XRD @5 06
C03 06  3  FRE  @0 Calorimétrie différentielle balayage @5 07
C03 06  3  ENG  @0 Differential scanning calorimetry @5 07
C03 07  X  FRE  @0 Transformation allotropique @5 08
C03 07  X  ENG  @0 Allotropic transformation @5 08
C03 07  X  SPA  @0 Transformación alotrópica @5 08
C03 08  3  FRE  @0 Relaxation contrainte @5 09
C03 08  3  ENG  @0 Stress relaxation @5 09
C03 09  3  FRE  @0 Addition fer @5 10
C03 09  3  ENG  @0 Iron additions @5 10
C03 10  3  FRE  @0 Cristallisation @5 12
C03 10  3  ENG  @0 Crystallization @5 12
C03 11  X  FRE  @0 Méthode Rietveld @5 13
C03 11  X  ENG  @0 Rietveld method @5 13
C03 11  X  SPA  @0 Método Rietveld @5 13
C03 12  3  FRE  @0 Traitement thermique @5 14
C03 12  3  ENG  @0 Heat treatments @5 14
C03 13  3  FRE  @0 Alliage base chrome @2 NK @5 15
C03 13  3  ENG  @0 Chromium base alloys @2 NK @5 15
C03 14  3  FRE  @0 Cobalt alliage @5 16
C03 14  3  ENG  @0 Cobalt alloys @5 16
C03 15  3  FRE  @0 Nanostructure @5 17
C03 15  3  ENG  @0 Nanostructures @5 17
C03 16  3  FRE  @0 Réseau cubique face centrée @5 18
C03 16  3  ENG  @0 FCC lattices @5 18
C03 17  3  FRE  @0 Réseau hexagonal compact @5 19
C03 17  3  ENG  @0 HCP lattices @5 19
C03 18  3  FRE  @0 Métal transition alliage @5 48
C03 18  3  ENG  @0 Transition element alloys @5 48
N21       @1 165

Format Inist (serveur)

NO : PASCAL 10-0249219 INIST
ET : Amorphisation of Cr-10Co mixture by mechanical alloying
AU : LOUIDI (S.); BENTAYEB (F. Z.); TEBI (W.); SUNOL (J. J.); MERCIER (A. M.); GRENECHE (J. M.)
AF : Laboratoire de Magnétisme et de Spectroscopie des Solides (LM2S), Département de Physique, Faculté des Sciences, Université de Annaba, B.P. 12/23000 Annaba/Algérie (1 aut., 2 aut., 3 aut.); Dep. Fisica, Universitat Girona, Campus Montilivi/17071 Girona/Espagne (3 aut., 4 aut.); Laboratoire des Fluorures, UMR CNRS 6010, Université du Maine/72085 Le Mans/France (5 aut.); Laboratoire de Physique de l'Etat Condensé, UMR CNRS 6087, Université du Maine/72085 Le Mans/France (6 aut.)
DT : Publication en série; Niveau analytique
SO : Journal of non-crystalline solids; ISSN 0022-3093; Coden JNCSBJ; Royaume-Uni; Da. 2010; Vol. 356; No. 20-22; Pp. 1052-1056; Bibl. 30 ref.
LA : Anglais
EA : Mechanical alloying of blended chromium and cobalt powders is carried out in order to obtain a nano-structured Cr-10Co alloy. The alloy formation is studied by means of scanning electron microscopy with energy-dispersive X-ray analysis, X-ray diffraction and differential scanning calorimetry. The results show that an allotropic transformation of Co from fcc to hcp structure occurs within the first 3 h of milling. After 12 h of milling, nanostructured bcc-Cr(Co) solid solution is obtained. Contamination of the powder by the milling tools and atmosphere for 24 h of milling contributes to the formation of a high degree of structural disorder. In addition to Fe, Cr and Co oxides, Cr(Co) solid solutions with bcc and unusual hcp structures are formed. The differential scanning calorimetry analysis in the temperature range 50-700 °C gives evidence for the presence of both microstrain relaxation and crystallization of the amorphous-like structures. Heating the 24 h-milled powder at 600 °C leads to the formation of bcc-Cr, Fe oxide and tetragonal σ-CrCo phases.
CC : 001B60D70P
FD : Amorphisation; Alliage mécanique; Microscopie électronique balayage; Spectrométrie dispersive; Diffraction RX; Calorimétrie différentielle balayage; Transformation allotropique; Relaxation contrainte; Addition fer; Cristallisation; Méthode Rietveld; Traitement thermique; Alliage base chrome; Cobalt alliage; Nanostructure; Réseau cubique face centrée; Réseau hexagonal compact; Métal transition alliage
ED : Amorphization; Mechanical alloying; Scanning electron microscopy; Dispersive spectrometry; XRD; Differential scanning calorimetry; Allotropic transformation; Stress relaxation; Iron additions; Crystallization; Rietveld method; Heat treatments; Chromium base alloys; Cobalt alloys; Nanostructures; FCC lattices; HCP lattices; Transition element alloys
SD : Espectrometría dispersiva; Transformación alotrópica; Método Rietveld
LO : INIST-14572.354000181735500190
ID : 10-0249219

Links to Exploration step

Pascal:10-0249219

Le document en format XML

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<term>Amorphisation</term>
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<term>Relaxation contrainte</term>
<term>Addition fer</term>
<term>Cristallisation</term>
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<term>Cobalt alliage</term>
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<div type="abstract" xml:lang="en">Mechanical alloying of blended chromium and cobalt powders is carried out in order to obtain a nano-structured Cr-10Co alloy. The alloy formation is studied by means of scanning electron microscopy with energy-dispersive X-ray analysis, X-ray diffraction and differential scanning calorimetry. The results show that an allotropic transformation of Co from fcc to hcp structure occurs within the first 3 h of milling. After 12 h of milling, nanostructured bcc-Cr(Co) solid solution is obtained. Contamination of the powder by the milling tools and atmosphere for 24 h of milling contributes to the formation of a high degree of structural disorder. In addition to Fe, Cr and Co oxides, Cr(Co) solid solutions with bcc and unusual hcp structures are formed. The differential scanning calorimetry analysis in the temperature range 50-700 °C gives evidence for the presence of both microstrain relaxation and crystallization of the amorphous-like structures. Heating the 24 h-milled powder at 600 °C leads to the formation of bcc-Cr, Fe oxide and tetragonal σ-CrCo phases.</div>
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</fA66>
<fC01 i1="01" l="ENG">
<s0>Mechanical alloying of blended chromium and cobalt powders is carried out in order to obtain a nano-structured Cr-10Co alloy. The alloy formation is studied by means of scanning electron microscopy with energy-dispersive X-ray analysis, X-ray diffraction and differential scanning calorimetry. The results show that an allotropic transformation of Co from fcc to hcp structure occurs within the first 3 h of milling. After 12 h of milling, nanostructured bcc-Cr(Co) solid solution is obtained. Contamination of the powder by the milling tools and atmosphere for 24 h of milling contributes to the formation of a high degree of structural disorder. In addition to Fe, Cr and Co oxides, Cr(Co) solid solutions with bcc and unusual hcp structures are formed. The differential scanning calorimetry analysis in the temperature range 50-700 °C gives evidence for the presence of both microstrain relaxation and crystallization of the amorphous-like structures. Heating the 24 h-milled powder at 600 °C leads to the formation of bcc-Cr, Fe oxide and tetragonal σ-CrCo phases.</s0>
</fC01>
<fC02 i1="01" i2="3">
<s0>001B60D70P</s0>
</fC02>
<fC03 i1="01" i2="3" l="FRE">
<s0>Amorphisation</s0>
<s5>02</s5>
</fC03>
<fC03 i1="01" i2="3" l="ENG">
<s0>Amorphization</s0>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="3" l="FRE">
<s0>Alliage mécanique</s0>
<s5>03</s5>
</fC03>
<fC03 i1="02" i2="3" l="ENG">
<s0>Mechanical alloying</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="3" l="FRE">
<s0>Microscopie électronique balayage</s0>
<s5>04</s5>
</fC03>
<fC03 i1="03" i2="3" l="ENG">
<s0>Scanning electron microscopy</s0>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="X" l="FRE">
<s0>Spectrométrie dispersive</s0>
<s5>05</s5>
</fC03>
<fC03 i1="04" i2="X" l="ENG">
<s0>Dispersive spectrometry</s0>
<s5>05</s5>
</fC03>
<fC03 i1="04" i2="X" l="SPA">
<s0>Espectrometría dispersiva</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="3" l="FRE">
<s0>Diffraction RX</s0>
<s5>06</s5>
</fC03>
<fC03 i1="05" i2="3" l="ENG">
<s0>XRD</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="3" l="FRE">
<s0>Calorimétrie différentielle balayage</s0>
<s5>07</s5>
</fC03>
<fC03 i1="06" i2="3" l="ENG">
<s0>Differential scanning calorimetry</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="FRE">
<s0>Transformation allotropique</s0>
<s5>08</s5>
</fC03>
<fC03 i1="07" i2="X" l="ENG">
<s0>Allotropic transformation</s0>
<s5>08</s5>
</fC03>
<fC03 i1="07" i2="X" l="SPA">
<s0>Transformación alotrópica</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="3" l="FRE">
<s0>Relaxation contrainte</s0>
<s5>09</s5>
</fC03>
<fC03 i1="08" i2="3" l="ENG">
<s0>Stress relaxation</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="3" l="FRE">
<s0>Addition fer</s0>
<s5>10</s5>
</fC03>
<fC03 i1="09" i2="3" l="ENG">
<s0>Iron additions</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="3" l="FRE">
<s0>Cristallisation</s0>
<s5>12</s5>
</fC03>
<fC03 i1="10" i2="3" l="ENG">
<s0>Crystallization</s0>
<s5>12</s5>
</fC03>
<fC03 i1="11" i2="X" l="FRE">
<s0>Méthode Rietveld</s0>
<s5>13</s5>
</fC03>
<fC03 i1="11" i2="X" l="ENG">
<s0>Rietveld method</s0>
<s5>13</s5>
</fC03>
<fC03 i1="11" i2="X" l="SPA">
<s0>Método Rietveld</s0>
<s5>13</s5>
</fC03>
<fC03 i1="12" i2="3" l="FRE">
<s0>Traitement thermique</s0>
<s5>14</s5>
</fC03>
<fC03 i1="12" i2="3" l="ENG">
<s0>Heat treatments</s0>
<s5>14</s5>
</fC03>
<fC03 i1="13" i2="3" l="FRE">
<s0>Alliage base chrome</s0>
<s2>NK</s2>
<s5>15</s5>
</fC03>
<fC03 i1="13" i2="3" l="ENG">
<s0>Chromium base alloys</s0>
<s2>NK</s2>
<s5>15</s5>
</fC03>
<fC03 i1="14" i2="3" l="FRE">
<s0>Cobalt alliage</s0>
<s5>16</s5>
</fC03>
<fC03 i1="14" i2="3" l="ENG">
<s0>Cobalt alloys</s0>
<s5>16</s5>
</fC03>
<fC03 i1="15" i2="3" l="FRE">
<s0>Nanostructure</s0>
<s5>17</s5>
</fC03>
<fC03 i1="15" i2="3" l="ENG">
<s0>Nanostructures</s0>
<s5>17</s5>
</fC03>
<fC03 i1="16" i2="3" l="FRE">
<s0>Réseau cubique face centrée</s0>
<s5>18</s5>
</fC03>
<fC03 i1="16" i2="3" l="ENG">
<s0>FCC lattices</s0>
<s5>18</s5>
</fC03>
<fC03 i1="17" i2="3" l="FRE">
<s0>Réseau hexagonal compact</s0>
<s5>19</s5>
</fC03>
<fC03 i1="17" i2="3" l="ENG">
<s0>HCP lattices</s0>
<s5>19</s5>
</fC03>
<fC03 i1="18" i2="3" l="FRE">
<s0>Métal transition alliage</s0>
<s5>48</s5>
</fC03>
<fC03 i1="18" i2="3" l="ENG">
<s0>Transition element alloys</s0>
<s5>48</s5>
</fC03>
<fN21>
<s1>165</s1>
</fN21>
</pA>
</standard>
<server>
<NO>PASCAL 10-0249219 INIST</NO>
<ET>Amorphisation of Cr-10Co mixture by mechanical alloying</ET>
<AU>LOUIDI (S.); BENTAYEB (F. Z.); TEBI (W.); SUNOL (J. J.); MERCIER (A. M.); GRENECHE (J. M.)</AU>
<AF>Laboratoire de Magnétisme et de Spectroscopie des Solides (LM2S), Département de Physique, Faculté des Sciences, Université de Annaba, B.P. 12/23000 Annaba/Algérie (1 aut., 2 aut., 3 aut.); Dep. Fisica, Universitat Girona, Campus Montilivi/17071 Girona/Espagne (3 aut., 4 aut.); Laboratoire des Fluorures, UMR CNRS 6010, Université du Maine/72085 Le Mans/France (5 aut.); Laboratoire de Physique de l'Etat Condensé, UMR CNRS 6087, Université du Maine/72085 Le Mans/France (6 aut.)</AF>
<DT>Publication en série; Niveau analytique</DT>
<SO>Journal of non-crystalline solids; ISSN 0022-3093; Coden JNCSBJ; Royaume-Uni; Da. 2010; Vol. 356; No. 20-22; Pp. 1052-1056; Bibl. 30 ref.</SO>
<LA>Anglais</LA>
<EA>Mechanical alloying of blended chromium and cobalt powders is carried out in order to obtain a nano-structured Cr-10Co alloy. The alloy formation is studied by means of scanning electron microscopy with energy-dispersive X-ray analysis, X-ray diffraction and differential scanning calorimetry. The results show that an allotropic transformation of Co from fcc to hcp structure occurs within the first 3 h of milling. After 12 h of milling, nanostructured bcc-Cr(Co) solid solution is obtained. Contamination of the powder by the milling tools and atmosphere for 24 h of milling contributes to the formation of a high degree of structural disorder. In addition to Fe, Cr and Co oxides, Cr(Co) solid solutions with bcc and unusual hcp structures are formed. The differential scanning calorimetry analysis in the temperature range 50-700 °C gives evidence for the presence of both microstrain relaxation and crystallization of the amorphous-like structures. Heating the 24 h-milled powder at 600 °C leads to the formation of bcc-Cr, Fe oxide and tetragonal σ-CrCo phases.</EA>
<CC>001B60D70P</CC>
<FD>Amorphisation; Alliage mécanique; Microscopie électronique balayage; Spectrométrie dispersive; Diffraction RX; Calorimétrie différentielle balayage; Transformation allotropique; Relaxation contrainte; Addition fer; Cristallisation; Méthode Rietveld; Traitement thermique; Alliage base chrome; Cobalt alliage; Nanostructure; Réseau cubique face centrée; Réseau hexagonal compact; Métal transition alliage</FD>
<ED>Amorphization; Mechanical alloying; Scanning electron microscopy; Dispersive spectrometry; XRD; Differential scanning calorimetry; Allotropic transformation; Stress relaxation; Iron additions; Crystallization; Rietveld method; Heat treatments; Chromium base alloys; Cobalt alloys; Nanostructures; FCC lattices; HCP lattices; Transition element alloys</ED>
<SD>Espectrometría dispersiva; Transformación alotrópica; Método Rietveld</SD>
<LO>INIST-14572.354000181735500190</LO>
<ID>10-0249219</ID>
</server>
</inist>
</record>

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