CobaltMaghrebV1, PascalFrancis, Checkpoint, bibRecord, 000262

On the metastable O2-type LiCoO2

Identifieur interne : 000262 ( PascalFrancis/Checkpoint ); précédent : 000261; suivant : 000263

On the metastable O2-type LiCoO2

Auteurs : D. Carlier [France] ; I. Saadoune [France, Maroc] ; L. Croguennec [France] ; M. Menetrier [France] ; E. Suard [France] ; C. Delmas [France]

Source :

Solid state ionics [ 0167-2738 ] ; 2001.

RBID : Pascal:02-0021500

Descripteurs français

Pascal (Inist)
- Structure cristalline, Phase métastable, Affinement, Diffraction neutron, Stoechiométrie, Angle magique, RMN, Traitement thermique, Microstructure, Echange ion, Microscopie électronique balayage, Mode empilement, Propriété électrochimique, Désinsertion, Cristal lamellaire, Lithium oxyde, Cobalt oxyde, Composé ternaire, Etude expérimentale, LiCoO2, Co Li O, 6166F, 7660.

English descriptors

KwdEn :
- Cobalt oxides, Crystal structure, Desinsertion, Electrochemical properties, Experimental study, Heat treatments, Ion exchange, Layered crystals, Lithium oxides, Magic angle, Metastable phases, Microstructure, NMR, Neutron diffraction, Refinement, Scanning electron microscopy, Stacking sequence, Stoichiometry, Ternary compounds.

Abstract

The exchange of sodium for lithium in P2-Na_0.70CoO₂ leads to an unusual O2-LiCoO₂ variety. Rietveld refinement of the neutron diffraction pattern of the O2-LiCoO₂ phase confirms the stoichiometry and the structural parameters previously reported and shows that the strong Li +-Co3^-+ electrostatic repulsion occurring through the common face of the CoO₆ and LiO₆ octahedra leads to small displacements of the lithium and cobalt ions from the center of their octahedra. Magnetic measurements and ⁷Li MAS NMR confirm a composition very close to the ideal one for the 02 phase. The O2-LiCoO₂ phase is metastable and transforms to well-crystallized O3-LiCoO₂ upon heating. Even at intermediate temperatures, the formation of LT-LiCoO₂ phase is never observed. Various morphologies are obtained for the O3-LiCoO₂ phases, depending on the thermal treatment used. A preliminary electrochemical study shows that almost all the lithium ions can be reversibly deintercalated from the O2-LiCoO₂ phase.

Affiliations:

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Le document en format XML

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<term>Experimental study</term>
<term>Heat treatments</term>
<term>Ion exchange</term>
<term>Layered crystals</term>
<term>Lithium oxides</term>
<term>Magic angle</term>
<term>Metastable phases</term>
<term>Microstructure</term>
<term>NMR</term>
<term>Neutron diffraction</term>
<term>Refinement</term>
<term>Scanning electron microscopy</term>
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<term>Ternary compounds</term>
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<term>Phase métastable</term>
<term>Affinement</term>
<term>Diffraction neutron</term>
<term>Stoechiométrie</term>
<term>Angle magique</term>
<term>RMN</term>
<term>Traitement thermique</term>
<term>Microstructure</term>
<term>Echange ion</term>
<term>Microscopie électronique balayage</term>
<term>Mode empilement</term>
<term>Propriété électrochimique</term>
<term>Désinsertion</term>
<term>Cristal lamellaire</term>
<term>Lithium oxyde</term>
<term>Cobalt oxyde</term>
<term>Composé ternaire</term>
<term>Etude expérimentale</term>
<term>LiCoO2</term>
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<front><div type="abstract" xml:lang="en">The exchange of sodium for lithium in P2-Na<sub>0.70</sub>
CoO<sub>2</sub>
 leads to an unusual O2-LiCoO<sub>2</sub>
 variety. Rietveld refinement of the neutron diffraction pattern of the O2-LiCoO<sub>2</sub>
 phase confirms the stoichiometry and the structural parameters previously reported and shows that the strong Li +-Co3<sup>-+</sup>
 electrostatic repulsion occurring through the common face of the CoO<sub>6</sub>
 and LiO<sub>6</sub>
 octahedra leads to small displacements of the lithium and cobalt ions from the center of their octahedra. Magnetic measurements and <sup>7</sup>
Li MAS NMR confirm a composition very close to the ideal one for the 02 phase. The O2-LiCoO<sub>2</sub>
 phase is metastable and transforms to well-crystallized O3-LiCoO<sub>2</sub>
 upon heating. Even at intermediate temperatures, the formation of LT-LiCoO<sub>2</sub>
 phase is never observed. Various morphologies are obtained for the O3-LiCoO<sub>2</sub>
 phases, depending on the thermal treatment used. A preliminary electrochemical study shows that almost all the lithium ions can be reversibly deintercalated from the O2-LiCoO<sub>2</sub>
 phase.</div>
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<fC01 i1="01" l="ENG"><s0>The exchange of sodium for lithium in P2-Na<sub>0.70</sub>
CoO<sub>2</sub>
 leads to an unusual O2-LiCoO<sub>2</sub>
 variety. Rietveld refinement of the neutron diffraction pattern of the O2-LiCoO<sub>2</sub>
 phase confirms the stoichiometry and the structural parameters previously reported and shows that the strong Li +-Co3<sup>-+</sup>
 electrostatic repulsion occurring through the common face of the CoO<sub>6</sub>
 and LiO<sub>6</sub>
 octahedra leads to small displacements of the lithium and cobalt ions from the center of their octahedra. Magnetic measurements and <sup>7</sup>
Li MAS NMR confirm a composition very close to the ideal one for the 02 phase. The O2-LiCoO<sub>2</sub>
 phase is metastable and transforms to well-crystallized O3-LiCoO<sub>2</sub>
 upon heating. Even at intermediate temperatures, the formation of LT-LiCoO<sub>2</sub>
 phase is never observed. Various morphologies are obtained for the O3-LiCoO<sub>2</sub>
 phases, depending on the thermal treatment used. A preliminary electrochemical study shows that almost all the lithium ions can be reversibly deintercalated from the O2-LiCoO<sub>2</sub>
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<s5>05</s5>
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<fC03 i1="05" i2="3" l="ENG"><s0>Stoichiometry</s0>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="X" l="FRE"><s0>Angle magique</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="ENG"><s0>Magic angle</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="SPA"><s0>Angulo mágico</s0>
<s5>06</s5>
</fC03>
<fC03 i1="07" i2="3" l="FRE"><s0>RMN</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="3" l="ENG"><s0>NMR</s0>
<s5>07</s5>
</fC03>
<fC03 i1="08" i2="3" l="FRE"><s0>Traitement thermique</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="3" l="ENG"><s0>Heat treatments</s0>
<s5>08</s5>
</fC03>
<fC03 i1="09" i2="3" l="FRE"><s0>Microstructure</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="3" l="ENG"><s0>Microstructure</s0>
<s5>09</s5>
</fC03>
<fC03 i1="10" i2="3" l="FRE"><s0>Echange ion</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="3" l="ENG"><s0>Ion exchange</s0>
<s5>10</s5>
</fC03>
<fC03 i1="11" i2="3" l="FRE"><s0>Microscopie électronique balayage</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="3" l="ENG"><s0>Scanning electron microscopy</s0>
<s5>11</s5>
</fC03>
<fC03 i1="12" i2="X" l="FRE"><s0>Mode empilement</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="ENG"><s0>Stacking sequence</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="SPA"><s0>Modo apilamiento</s0>
<s5>12</s5>
</fC03>
<fC03 i1="13" i2="X" l="FRE"><s0>Propriété électrochimique</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="X" l="ENG"><s0>Electrochemical properties</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="X" l="SPA"><s0>Propiedad electroquímica</s0>
<s5>13</s5>
</fC03>
<fC03 i1="14" i2="X" l="FRE"><s0>Désinsertion</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="X" l="ENG"><s0>Desinsertion</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="X" l="SPA"><s0>Desinserción</s0>
<s5>14</s5>
</fC03>
<fC03 i1="15" i2="3" l="FRE"><s0>Cristal lamellaire</s0>
<s5>15</s5>
</fC03>
<fC03 i1="15" i2="3" l="ENG"><s0>Layered crystals</s0>
<s5>15</s5>
</fC03>
<fC03 i1="16" i2="3" l="FRE"><s0>Lithium oxyde</s0>
<s2>NK</s2>
<s5>16</s5>
</fC03>
<fC03 i1="16" i2="3" l="ENG"><s0>Lithium oxides</s0>
<s2>NK</s2>
<s5>16</s5>
</fC03>
<fC03 i1="17" i2="3" l="FRE"><s0>Cobalt oxyde</s0>
<s2>NK</s2>
<s5>17</s5>
</fC03>
<fC03 i1="17" i2="3" l="ENG"><s0>Cobalt oxides</s0>
<s2>NK</s2>
<s5>17</s5>
</fC03>
<fC03 i1="18" i2="3" l="FRE"><s0>Composé ternaire</s0>
<s5>18</s5>
</fC03>
<fC03 i1="18" i2="3" l="ENG"><s0>Ternary compounds</s0>
<s5>18</s5>
</fC03>
<fC03 i1="19" i2="3" l="FRE"><s0>Etude expérimentale</s0>
<s5>19</s5>
</fC03>
<fC03 i1="19" i2="3" l="ENG"><s0>Experimental study</s0>
<s5>19</s5>
</fC03>
<fC03 i1="20" i2="3" l="FRE"><s0>LiCoO2</s0>
<s4>INC</s4>
<s5>53</s5>
</fC03>
<fC03 i1="21" i2="3" l="FRE"><s0>Co Li O</s0>
<s4>INC</s4>
<s5>54</s5>
</fC03>
<fC03 i1="22" i2="3" l="FRE"><s0>6166F</s0>
<s2>PAC</s2>
<s4>INC</s4>
<s5>56</s5>
</fC03>
<fC03 i1="23" i2="3" l="FRE"><s0>7660</s0>
<s2>PAC</s2>
<s4>INC</s4>
<s5>57</s5>
</fC03>
<fC07 i1="01" i2="3" l="FRE"><s0>Métal transition composé</s0>
<s5>48</s5>
</fC07>
<fC07 i1="01" i2="3" l="ENG"><s0>Transition element compounds</s0>
<s5>48</s5>
</fC07>
<fC07 i1="02" i2="3" l="FRE"><s0>Composé minéral</s0>
<s5>49</s5>
</fC07>
<fC07 i1="02" i2="3" l="ENG"><s0>Inorganic compounds</s0>
<s5>49</s5>
</fC07>
<fN21><s1>007</s1>
</fN21>
</pA>
</standard>
</inist>
<affiliations><list><country><li>France</li>
<li>Maroc</li>
</country>
<region><li>Aquitaine</li>
<li>Auvergne-Rhône-Alpes</li>
<li>Nouvelle-Aquitaine</li>
<li>Rhône-Alpes</li>
</region>
<settlement><li>Grenoble</li>
<li>Pessac</li>
</settlement>
</list>
<tree><country name="France"><region name="Nouvelle-Aquitaine"><name sortKey="Carlier, D" sort="Carlier, D" uniqKey="Carlier D" first="D." last="Carlier">D. Carlier</name>
</region>
<name sortKey="Croguennec, L" sort="Croguennec, L" uniqKey="Croguennec L" first="L." last="Croguennec">L. Croguennec</name>
<name sortKey="Delmas, C" sort="Delmas, C" uniqKey="Delmas C" first="C." last="Delmas">C. Delmas</name>
<name sortKey="Menetrier, M" sort="Menetrier, M" uniqKey="Menetrier M" first="M." last="Menetrier">M. Menetrier</name>
<name sortKey="Saadoune, I" sort="Saadoune, I" uniqKey="Saadoune I" first="I." last="Saadoune">I. Saadoune</name>
<name sortKey="Suard, E" sort="Suard, E" uniqKey="Suard E" first="E." last="Suard">E. Suard</name>
</country>
<country name="Maroc"><noRegion><name sortKey="Saadoune, I" sort="Saadoune, I" uniqKey="Saadoune I" first="I." last="Saadoune">I. Saadoune</name>
</noRegion>
</country>
</tree>
</affiliations>
</record>

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	Serveur d'exploration sur le cobalt au Maghreb
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Serveur d'exploration sur le cobalt au Maghreb

On the metastable O2-type LiCoO2

On the metastable O2-type LiCoO2

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English descriptors

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