CobaltMaghrebV1, PascalFrancis, Checkpoint, bibRecord, 000155

Total oxidation of propene and propane over gold-copper oxide on alumina catalysts Comparison with Pt/Al2O3

Identifieur interne : 000155 ( PascalFrancis/Checkpoint ); précédent : 000154; suivant : 000156

Total oxidation of propene and propane over gold-copper oxide on alumina catalysts Comparison with Pt/Al2O3

Auteurs : Andreea C. Gluhoi [Pays-Bas] ; Nina Bogdanchikova [Mexique] ; Bernard E. Nieuwenhuys [Pays-Bas]

Source :

Catalysis today [ 0920-5861 ] ; 2006.

RBID : Pascal:06-0371423

Descripteurs français

Pascal (Inist)
- Oxydation, Propène, Propane, Or, Cuivre oxyde, Alumine, Catalyseur sur support, Platine, Additif, Cobalt oxyde, Catalyse hétérogène.
Wicri :
- topic : Propane, Or, Platine.

English descriptors

KwdEn :
- Additive, Alumina, Cobalt oxide, Copper oxide, Gold, Heterogeneous catalysis, Oxidation, Platinum, Propane, Propene, Supported catalyst.

Abstract

Oxidation of propene and propane to CO₂ and H₂O has been studied over Au/Al₂O₃ and two different Au/CuO/Al₂O₃ (4 wt.% Au and 7.4 wt.% Au) catalysts and compared with the catalytic behaviour of Au/Co₃O₄/Al₂O₃ (4.1 wt.% Au) and Pt/Al₂O₃ (4.8 wt.% Pt) catalysts. The various characterization techniques employed (XRD, HRTEM, TPR and DR-UV-vis) revealed the presence of metallic gold, along with a highly dispersed CuO (6 wt.% CuO), or more crystalline CuO phase (12 wt.% CuO). A higher CuO loading does not significantly influence the catalytic performance of the catalyst in propene oxidation, the gold loading appears to be more important. Moreover, it was found that 7.4Au/CuO/Al₂O₃ is almost as active as Pt/Al₂O₃, whereas Au/Co₃O₄/Al₂O₃ performs less than any of the CuO-containing gold-based catalysts. The light-off temperature for C₃H₈ oxidation is significantly higher than for C₃H₆. For this reaction the particle size effect appears to prevail over the effect of gold loading. The most active catalysts are 4Au/CuO/Al₂O₃ (gold particles less than 3 nm) and 4Au/Co₃O₄/Al₂O₃ (gold particles less than 5 nm).

Affiliations:

Mexique, Pays-Bas

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Le document en format XML

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O<sub>3</sub>
</title>
<author><name sortKey="Gluhoi, Andreea C" sort="Gluhoi, Andreea C" uniqKey="Gluhoi A" first="Andreea C." last="Gluhoi">Andreea C. Gluhoi</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Department of Heterogeneous Catalysis and Surface Chemistry, Leiden Institute of Chemistry, Leiden University, P.O. Box 9502</s1>
<s2>2300 RA Leiden</s2>
<s3>NLD</s3>
<sZ>1 aut.</sZ>
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<author><name sortKey="Bogdanchikova, Nina" sort="Bogdanchikova, Nina" uniqKey="Bogdanchikova N" first="Nina" last="Bogdanchikova">Nina Bogdanchikova</name>
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<s3>MEX</s3>
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<author><name sortKey="Nieuwenhuys, Bernard E" sort="Nieuwenhuys, Bernard E" uniqKey="Nieuwenhuys B" first="Bernard E." last="Nieuwenhuys">Bernard E. Nieuwenhuys</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Department of Heterogeneous Catalysis and Surface Chemistry, Leiden Institute of Chemistry, Leiden University, P.O. Box 9502</s1>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a">Total oxidation of propene and propane over gold-copper oxide on alumina catalysts Comparison with Pt/Al<sub>2</sub>
O<sub>3</sub>
</title>
<author><name sortKey="Gluhoi, Andreea C" sort="Gluhoi, Andreea C" uniqKey="Gluhoi A" first="Andreea C." last="Gluhoi">Andreea C. Gluhoi</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Department of Heterogeneous Catalysis and Surface Chemistry, Leiden Institute of Chemistry, Leiden University, P.O. Box 9502</s1>
<s2>2300 RA Leiden</s2>
<s3>NLD</s3>
<sZ>1 aut.</sZ>
<sZ>3 aut.</sZ>
</inist:fA14>
<country>Pays-Bas</country>
<wicri:noRegion>2300 RA Leiden</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Bogdanchikova, Nina" sort="Bogdanchikova, Nina" uniqKey="Bogdanchikova N" first="Nina" last="Bogdanchikova">Nina Bogdanchikova</name>
<affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Centro de Ciencias de la Materia Condensada, UNAM, Km. 107, Carretera Tijuana-Ensenada</s1>
<s2>22800 Ensenada, Baja California</s2>
<s3>MEX</s3>
<sZ>2 aut.</sZ>
</inist:fA14>
<country>Mexique</country>
<wicri:noRegion>22800 Ensenada, Baja California</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Nieuwenhuys, Bernard E" sort="Nieuwenhuys, Bernard E" uniqKey="Nieuwenhuys B" first="Bernard E." last="Nieuwenhuys">Bernard E. Nieuwenhuys</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Department of Heterogeneous Catalysis and Surface Chemistry, Leiden Institute of Chemistry, Leiden University, P.O. Box 9502</s1>
<s2>2300 RA Leiden</s2>
<s3>NLD</s3>
<sZ>1 aut.</sZ>
<sZ>3 aut.</sZ>
</inist:fA14>
<country>Pays-Bas</country>
<wicri:noRegion>2300 RA Leiden</wicri:noRegion>
</affiliation>
</author>
</analytic>
<series><title level="j" type="main">Catalysis today</title>
<title level="j" type="abbreviated">Catal. today</title>
<idno type="ISSN">0920-5861</idno>
<imprint><date when="2006">2006</date>
</imprint>
</series>
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<seriesStmt><title level="j" type="main">Catalysis today</title>
<title level="j" type="abbreviated">Catal. today</title>
<idno type="ISSN">0920-5861</idno>
</seriesStmt>
</fileDesc>
<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Additive</term>
<term>Alumina</term>
<term>Cobalt oxide</term>
<term>Copper oxide</term>
<term>Gold</term>
<term>Heterogeneous catalysis</term>
<term>Oxidation</term>
<term>Platinum</term>
<term>Propane</term>
<term>Propene</term>
<term>Supported catalyst</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Oxydation</term>
<term>Propène</term>
<term>Propane</term>
<term>Or</term>
<term>Cuivre oxyde</term>
<term>Alumine</term>
<term>Catalyseur sur support</term>
<term>Platine</term>
<term>Additif</term>
<term>Cobalt oxyde</term>
<term>Catalyse hétérogène</term>
</keywords>
<keywords scheme="Wicri" type="topic" xml:lang="fr"><term>Propane</term>
<term>Or</term>
<term>Platine</term>
</keywords>
</textClass>
</profileDesc>
</teiHeader>
<front><div type="abstract" xml:lang="en">Oxidation of propene and propane to CO<sub>2</sub>
 and H<sub>2</sub>
O has been studied over Au/Al<sub>2</sub>
O<sub>3</sub>
 and two different Au/CuO/Al<sub>2</sub>
O<sub>3</sub>
 (4 wt.% Au and 7.4 wt.% Au) catalysts and compared with the catalytic behaviour of Au/Co<sub>3</sub>
O<sub>4</sub>
/Al<sub>2</sub>
O<sub>3</sub>
 (4.1 wt.% Au) and Pt/Al<sub>2</sub>
O<sub>3</sub>
 (4.8 wt.% Pt) catalysts. The various characterization techniques employed (XRD, HRTEM, TPR and DR-UV-vis) revealed the presence of metallic gold, along with a highly dispersed CuO (6 wt.% CuO), or more crystalline CuO phase (12 wt.% CuO). A higher CuO loading does not significantly influence the catalytic performance of the catalyst in propene oxidation, the gold loading appears to be more important. Moreover, it was found that 7.4Au/CuO/Al<sub>2</sub>
O<sub>3</sub>
 is almost as active as Pt/Al<sub>2</sub>
O<sub>3</sub>
, whereas Au/Co<sub>3</sub>
O<sub>4</sub>
/Al<sub>2</sub>
O<sub>3</sub>
 performs less than any of the CuO-containing gold-based catalysts. The light-off temperature for C<sub>3</sub>
H<sub>8</sub>
 oxidation is significantly higher than for C<sub>3</sub>
H<sub>6</sub>
. For this reaction the particle size effect appears to prevail over the effect of gold loading. The most active catalysts are 4Au/CuO/Al<sub>2</sub>
O<sub>3</sub>
 (gold particles less than 3 nm) and 4Au/Co<sub>3</sub>
O<sub>4</sub>
/Al<sub>2</sub>
O<sub>3</sub>
 (gold particles less than 5 nm).</div>
</front>
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<fA08 i1="01" i2="1" l="ENG"><s1>Total oxidation of propene and propane over gold-copper oxide on alumina catalysts Comparison with Pt/Al<sub>2</sub>
O<sub>3</sub>
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<fA11 i1="01" i2="1"><s1>GLUHOI (Andreea C.)</s1>
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<fA12 i1="01" i2="1"><s1>GARIN (François)</s1>
<s9>ed.</s9>
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<fA12 i1="02" i2="1"><s1>MAAMACHE (Mustapha)</s1>
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<fA12 i1="04" i2="1"><s1>DEMANGEAT (Claude)</s1>
<s9>ed.</s9>
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<fA14 i1="01"><s1>Department of Heterogeneous Catalysis and Surface Chemistry, Leiden Institute of Chemistry, Leiden University, P.O. Box 9502</s1>
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<s3>NLD</s3>
<sZ>1 aut.</sZ>
<sZ>3 aut.</sZ>
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<s3>MEX</s3>
<sZ>2 aut.</sZ>
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<fA15 i1="01"><s1>Laboratoire des Matériaux, Surfaces et Procédés pour la Catalyse (LMSPC), UMR 7515-CNRS-ULP-ECPM, 25 rue Becquerel</s1>
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<sZ>2 aut.</sZ>
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<fA15 i1="03"><s1>Institut de Physique et Chimie des Matériaux de Strasbourg (IPCMS), Université Louis Pasteur, UMR 7504-CNRS-ULP, 23 rue du Loess, BP 43</s1>
<s2>67034 Strasbourg</s2>
<s3>FRA</s3>
<sZ>3 aut.</sZ>
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<fA20><s1>178-181</s1>
</fA20>
<fA21><s1>2006</s1>
</fA21>
<fA23 i1="01"><s0>ENG</s0>
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<fA43 i1="01"><s1>INIST</s1>
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<s5>354000142867030060</s5>
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<fA45><s0>19 ref.</s0>
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<fA47 i1="01" i2="1"><s0>06-0371423</s0>
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<fA60><s1>P</s1>
<s2>C</s2>
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<fA66 i1="01"><s0>NLD</s0>
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<fC01 i1="01" l="ENG"><s0>Oxidation of propene and propane to CO<sub>2</sub>
 and H<sub>2</sub>
O has been studied over Au/Al<sub>2</sub>
O<sub>3</sub>
 and two different Au/CuO/Al<sub>2</sub>
O<sub>3</sub>
 (4 wt.% Au and 7.4 wt.% Au) catalysts and compared with the catalytic behaviour of Au/Co<sub>3</sub>
O<sub>4</sub>
/Al<sub>2</sub>
O<sub>3</sub>
 (4.1 wt.% Au) and Pt/Al<sub>2</sub>
O<sub>3</sub>
 (4.8 wt.% Pt) catalysts. The various characterization techniques employed (XRD, HRTEM, TPR and DR-UV-vis) revealed the presence of metallic gold, along with a highly dispersed CuO (6 wt.% CuO), or more crystalline CuO phase (12 wt.% CuO). A higher CuO loading does not significantly influence the catalytic performance of the catalyst in propene oxidation, the gold loading appears to be more important. Moreover, it was found that 7.4Au/CuO/Al<sub>2</sub>
O<sub>3</sub>
 is almost as active as Pt/Al<sub>2</sub>
O<sub>3</sub>
, whereas Au/Co<sub>3</sub>
O<sub>4</sub>
/Al<sub>2</sub>
O<sub>3</sub>
 performs less than any of the CuO-containing gold-based catalysts. The light-off temperature for C<sub>3</sub>
H<sub>8</sub>
 oxidation is significantly higher than for C<sub>3</sub>
H<sub>6</sub>
. For this reaction the particle size effect appears to prevail over the effect of gold loading. The most active catalysts are 4Au/CuO/Al<sub>2</sub>
O<sub>3</sub>
 (gold particles less than 3 nm) and 4Au/Co<sub>3</sub>
O<sub>4</sub>
/Al<sub>2</sub>
O<sub>3</sub>
 (gold particles less than 5 nm).</s0>
</fC01>
<fC02 i1="01" i2="X"><s0>001C01A03</s0>
</fC02>
<fC03 i1="01" i2="X" l="FRE"><s0>Oxydation</s0>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="X" l="ENG"><s0>Oxidation</s0>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="X" l="SPA"><s0>Oxidación</s0>
<s5>01</s5>
</fC03>
<fC03 i1="02" i2="X" l="FRE"><s0>Propène</s0>
<s2>NK</s2>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="ENG"><s0>Propene</s0>
<s2>NK</s2>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="X" l="SPA"><s0>Propeno</s0>
<s2>NK</s2>
<s5>02</s5>
</fC03>
<fC03 i1="03" i2="X" l="FRE"><s0>Propane</s0>
<s2>NK</s2>
<s2>FX</s2>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="X" l="ENG"><s0>Propane</s0>
<s2>NK</s2>
<s2>FX</s2>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="X" l="SPA"><s0>Propano</s0>
<s2>NK</s2>
<s2>FX</s2>
<s5>03</s5>
</fC03>
<fC03 i1="04" i2="X" l="FRE"><s0>Or</s0>
<s2>NC</s2>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="X" l="ENG"><s0>Gold</s0>
<s2>NC</s2>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="X" l="SPA"><s0>Oro</s0>
<s2>NC</s2>
<s5>04</s5>
</fC03>
<fC03 i1="05" i2="X" l="FRE"><s0>Cuivre oxyde</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="X" l="ENG"><s0>Copper oxide</s0>
<s5>05</s5>
</fC03>
<fC03 i1="05" i2="X" l="SPA"><s0>Cobre óxido</s0>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="X" l="FRE"><s0>Alumine</s0>
<s2>NK</s2>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="ENG"><s0>Alumina</s0>
<s2>NK</s2>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="SPA"><s0>Alúmina</s0>
<s2>NK</s2>
<s5>06</s5>
</fC03>
<fC03 i1="07" i2="X" l="FRE"><s0>Catalyseur sur support</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="ENG"><s0>Supported catalyst</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="X" l="SPA"><s0>Catalizador sobre soporte</s0>
<s5>07</s5>
</fC03>
<fC03 i1="08" i2="X" l="FRE"><s0>Platine</s0>
<s2>NC</s2>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="ENG"><s0>Platinum</s0>
<s2>NC</s2>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="X" l="SPA"><s0>Platino</s0>
<s2>NC</s2>
<s5>08</s5>
</fC03>
<fC03 i1="09" i2="X" l="FRE"><s0>Additif</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="ENG"><s0>Additive</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="X" l="SPA"><s0>Aditivo</s0>
<s5>09</s5>
</fC03>
<fC03 i1="10" i2="X" l="FRE"><s0>Cobalt oxyde</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="ENG"><s0>Cobalt oxide</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="SPA"><s0>Cobalto óxido</s0>
<s5>10</s5>
</fC03>
<fC03 i1="11" i2="X" l="FRE"><s0>Catalyse hétérogène</s0>
<s5>11</s5>
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<s5>11</s5>
</fC03>
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<s5>11</s5>
</fC03>
<fC07 i1="01" i2="X" l="FRE"><s0>Métal transition</s0>
<s2>NC</s2>
<s5>12</s5>
</fC07>
<fC07 i1="01" i2="X" l="ENG"><s0>Transition metal</s0>
<s2>NC</s2>
<s5>12</s5>
</fC07>
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<s2>NC</s2>
<s5>12</s5>
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<s5>13</s5>
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<fN21><s1>247</s1>
</fN21>
<fN44 i1="01"><s1>OTO</s1>
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<fN82><s1>OTO</s1>
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<pR><fA30 i1="01" i2="1" l="ENG"><s1>Colloquium on Environment, Materials, Physics and Energy</s1>
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<s4>2004-12-11</s4>
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<affiliations><list><country><li>Mexique</li>
<li>Pays-Bas</li>
</country>
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<tree><country name="Pays-Bas"><noRegion><name sortKey="Gluhoi, Andreea C" sort="Gluhoi, Andreea C" uniqKey="Gluhoi A" first="Andreea C." last="Gluhoi">Andreea C. Gluhoi</name>
</noRegion>
<name sortKey="Nieuwenhuys, Bernard E" sort="Nieuwenhuys, Bernard E" uniqKey="Nieuwenhuys B" first="Bernard E." last="Nieuwenhuys">Bernard E. Nieuwenhuys</name>
</country>
<country name="Mexique"><noRegion><name sortKey="Bogdanchikova, Nina" sort="Bogdanchikova, Nina" uniqKey="Bogdanchikova N" first="Nina" last="Bogdanchikova">Nina Bogdanchikova</name>
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   |texte=   Total oxidation of propene and propane over gold-copper oxide on alumina catalysts Comparison with Pt/Al2O3
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	Serveur d'exploration sur le cobalt au Maghreb
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Serveur d'exploration sur le cobalt au Maghreb

Total oxidation of propene and propane over gold-copper oxide on alumina catalysts Comparison with Pt/Al2O3

Total oxidation of propene and propane over gold-copper oxide on alumina catalysts Comparison with Pt/Al2O3

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