Electrocatalytic oxidation of thiocholine at chemically modified cobalt hexacyanoferrate screen-printed electrodes
Identifieur interne : 000112 ( PascalFrancis/Checkpoint ); précédent : 000111; suivant : 000113Electrocatalytic oxidation of thiocholine at chemically modified cobalt hexacyanoferrate screen-printed electrodes
Auteurs : Fabiana Arduini [Italie] ; Alessio Cassisi [Italie] ; Aziz Amine [Maroc] ; Francesco Ricci [Italie] ; Danila Moscone [Italie] ; Giuseppe Palleschi [Italie]Source :
- Journal of electroanalytical chemistry : (1992) [ 1572-6657 ] ; 2009.
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Abstract
In this work, cobalt hexacyanoferrate (CoHCF) modified screen-printed electrodes were developed and characterised electrochemically. The effect of different cations was investigated showing a more reversible system with a well-defined peak around +0.35 V vs. Ag/AgCl when Na+ was used as cation in the supporting electrolyte. The transfer coefficient (α) and the apparent charge transfer rate constant (ks) for electron transfer between the electrode and the CoHCF layer was calculated. The electrocatalytic behaviour of CoHCF towards oxidation of enzymatically generated thiocholine was thoroughly investigated. Cyclic voltammetry experiments performed in thiocholine solution showed the classical shape of mediated redox system. The diffusion constant of thiocholine was estimated using chronoamperometry. Also, the catalytic rate constant k of thiocholine at CoHCF-SPE was determined. The current due to thiocholine mediated oxidation was then evaluated in batch amperometric mode at +0.5 V vs. Ag/AgCl obtaining a linear range (5 × 10-7-1 × 10-5 mol L-1) with a low detection limit and a high sensitivity equal to 5 x 10-7 mol L-1 and 435 mA mol-1 L cm-2, respectively.
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wicri:stream="PascalFrancis" wicri:step="Checkpoint">000112</idno></publicationStmt><sourceDesc><biblStruct><analytic><title xml:lang="en" level="a">Electrocatalytic oxidation of thiocholine at chemically modified cobalt hexacyanoferrate screen-printed electrodes</title><author><name sortKey="Arduini, Fabiana" sort="Arduini, Fabiana" uniqKey="Arduini F" first="Fabiana" last="Arduini">Fabiana Arduini</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Dipartimento di Scienze e Tecnologie Chimiche, Università di Rama Tor Vergata, Via della Ricerca Scientifica</s1><s2>00133 Rome</s2><s3>ITA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></inist:fA14><country>Italie</country><placeName><settlement type="city">Rome</settlement><region nuts="2">Latium</region></placeName></affiliation><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>Consorzio Inteniniversitario Biostrutture e Biosistemi "INBB", Viale Medaglie d'Oro</s1><s2>Rome</s2><s3>ITA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></inist:fA14><country>Italie</country><placeName><settlement type="city">Rome</settlement><region nuts="2">Latium</region></placeName></affiliation></author><author><name sortKey="Cassisi, Alessio" sort="Cassisi, Alessio" uniqKey="Cassisi A" first="Alessio" last="Cassisi">Alessio Cassisi</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Dipartimento di Scienze e Tecnologie Chimiche, Università di Rama Tor Vergata, Via della Ricerca Scientifica</s1><s2>00133 Rome</s2><s3>ITA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></inist:fA14><country>Italie</country><placeName><settlement type="city">Rome</settlement><region nuts="2">Latium</region></placeName></affiliation><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>Consorzio Inteniniversitario Biostrutture e Biosistemi "INBB", Viale Medaglie d'Oro</s1><s2>Rome</s2><s3>ITA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></inist:fA14><country>Italie</country><placeName><settlement type="city">Rome</settlement><region nuts="2">Latium</region></placeName></affiliation></author><author><name sortKey="Amine, Aziz" sort="Amine, Aziz" uniqKey="Amine A" first="Aziz" last="Amine">Aziz Amine</name><affiliation wicri:level="1"><inist:fA14 i1="03"><s1>Faculté de Sciences et Techniques de Mohammadia, B.P. 146</s1><s2>Mohammadia</s2><s3>MAR</s3><sZ>3 aut.</sZ></inist:fA14><country>Maroc</country><wicri:noRegion>Mohammadia</wicri:noRegion></affiliation></author><author><name sortKey="Ricci, Francesco" sort="Ricci, Francesco" uniqKey="Ricci F" first="Francesco" last="Ricci">Francesco Ricci</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Dipartimento di Scienze e Tecnologie Chimiche, Università di Rama Tor Vergata, Via della Ricerca Scientifica</s1><s2>00133 Rome</s2><s3>ITA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></inist:fA14><country>Italie</country><placeName><settlement type="city">Rome</settlement><region nuts="2">Latium</region></placeName></affiliation><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>Consorzio Inteniniversitario Biostrutture e Biosistemi "INBB", Viale Medaglie d'Oro</s1><s2>Rome</s2><s3>ITA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></inist:fA14><country>Italie</country><placeName><settlement type="city">Rome</settlement><region nuts="2">Latium</region></placeName></affiliation></author><author><name sortKey="Moscone, Danila" sort="Moscone, Danila" uniqKey="Moscone D" first="Danila" last="Moscone">Danila Moscone</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Dipartimento di Scienze e Tecnologie Chimiche, Università di Rama Tor Vergata, Via della Ricerca Scientifica</s1><s2>00133 Rome</s2><s3>ITA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></inist:fA14><country>Italie</country><placeName><settlement type="city">Rome</settlement><region nuts="2">Latium</region></placeName></affiliation><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>Consorzio Inteniniversitario Biostrutture e Biosistemi "INBB", Viale Medaglie d'Oro</s1><s2>Rome</s2><s3>ITA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></inist:fA14><country>Italie</country><placeName><settlement type="city">Rome</settlement><region nuts="2">Latium</region></placeName></affiliation></author><author><name sortKey="Palleschi, Giuseppe" sort="Palleschi, Giuseppe" uniqKey="Palleschi G" first="Giuseppe" last="Palleschi">Giuseppe Palleschi</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Dipartimento di Scienze e Tecnologie Chimiche, Università di Rama Tor Vergata, Via della Ricerca Scientifica</s1><s2>00133 Rome</s2><s3>ITA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></inist:fA14><country>Italie</country><placeName><settlement type="city">Rome</settlement><region nuts="2">Latium</region></placeName></affiliation><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>Consorzio Inteniniversitario Biostrutture e Biosistemi "INBB", Viale Medaglie d'Oro</s1><s2>Rome</s2><s3>ITA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></inist:fA14><country>Italie</country><placeName><settlement type="city">Rome</settlement><region nuts="2">Latium</region></placeName></affiliation></author></analytic><series><title level="j" type="main">Journal of electroanalytical chemistry : (1992)</title><title level="j" type="abbreviated">J. electroanal. chem. : (1992)</title><idno type="ISSN">1572-6657</idno><imprint><date when="2009">2009</date></imprint></series></biblStruct></sourceDesc><seriesStmt><title level="j" type="main">Journal of electroanalytical chemistry : (1992)</title><title level="j" type="abbreviated">J. electroanal. chem. : (1992)</title><idno type="ISSN">1572-6657</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Buffer solution</term><term>Cobalt Hexacyanoferrates</term><term>Electrocatalysis</term><term>Electrocatalysts</term><term>Electrochemical detector</term><term>Electrochemical reaction</term><term>Electrodes</term><term>Lithium Chlorides</term><term>Modified material</term><term>Oxidation</term><term>Phosphates</term><term>Potassium Chlorides</term><term>Serigraphy</term><term>Sodium Chlorides</term></keywords><keywords scheme="Pascal" xml:lang="fr"><term>Electrocatalyse</term><term>Oxydation</term><term>Cobalt Hexacyanoferrate</term><term>Electrocatalyseur</term><term>Sérigraphie</term><term>Electrode</term><term>Détecteur électrochimique</term><term>Matériau modifié</term><term>Sodium Chlorure</term><term>Lithium Chlorure</term><term>Potassium Chlorure</term><term>Solution tampon</term><term>Phosphate</term><term>Réaction électrochimique</term><term>Thiocholine</term></keywords><keywords scheme="Wicri" type="topic" xml:lang="fr"><term>Phosphate</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">In this work, cobalt hexacyanoferrate (CoHCF) modified screen-printed electrodes were developed and characterised electrochemically. The effect of different cations was investigated showing a more reversible system with a well-defined peak around +0.35 V vs. Ag/AgCl when Na<sup>+</sup> was used as cation in the supporting electrolyte. The transfer coefficient (α) and the apparent charge transfer rate constant (k<sub>s</sub>) for electron transfer between the electrode and the CoHCF layer was calculated. The electrocatalytic behaviour of CoHCF towards oxidation of enzymatically generated thiocholine was thoroughly investigated. Cyclic voltammetry experiments performed in thiocholine solution showed the classical shape of mediated redox system. The diffusion constant of thiocholine was estimated using chronoamperometry. Also, the catalytic rate constant k of thiocholine at CoHCF-SPE was determined. The current due to thiocholine mediated oxidation was then evaluated in batch amperometric mode at +0.5 V vs. Ag/AgCl obtaining a linear range (5 × 10<sup>-7</sup>-1 × 10<sup>-5</sup> mol L<sup>-1</sup>) with a low detection limit and a high sensitivity equal to 5 x 10<sup>-7</sup> mol L<sup>-1</sup> and 435 mA mol<sup>-1</sup> L cm<sup>-2</sup>, respectively.</div></front></TEI><inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>1572-6657</s0></fA01><fA03 i2="1"><s0>J. electroanal. chem. : (1992)</s0></fA03><fA05><s2>626</s2></fA05><fA06><s2>1-2</s2></fA06><fA08 i1="01" i2="1" l="ENG"><s1>Electrocatalytic oxidation of thiocholine at chemically modified cobalt hexacyanoferrate screen-printed electrodes</s1></fA08><fA11 i1="01" i2="1"><s1>ARDUINI (Fabiana)</s1></fA11><fA11 i1="02" i2="1"><s1>CASSISI (Alessio)</s1></fA11><fA11 i1="03" i2="1"><s1>AMINE (Aziz)</s1></fA11><fA11 i1="04" i2="1"><s1>RICCI (Francesco)</s1></fA11><fA11 i1="05" i2="1"><s1>MOSCONE (Danila)</s1></fA11><fA11 i1="06" i2="1"><s1>PALLESCHI (Giuseppe)</s1></fA11><fA14 i1="01"><s1>Dipartimento di Scienze e Tecnologie Chimiche, Università di Rama Tor Vergata, Via della Ricerca Scientifica</s1><s2>00133 Rome</s2><s3>ITA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></fA14><fA14 i1="02"><s1>Consorzio Inteniniversitario Biostrutture e Biosistemi "INBB", Viale Medaglie d'Oro</s1><s2>Rome</s2><s3>ITA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></fA14><fA14 i1="03"><s1>Faculté de Sciences et Techniques de Mohammadia, B.P. 146</s1><s2>Mohammadia</s2><s3>MAR</s3><sZ>3 aut.</sZ></fA14><fA20><s1>66-74</s1></fA20><fA21><s1>2009</s1></fA21><fA23 i1="01"><s0>ENG</s0></fA23><fA43 i1="01"><s1>INIST</s1><s2>1150</s2><s5>354000184223950100</s5></fA43><fA44><s0>0000</s0><s1>© 2009 INIST-CNRS. All rights reserved.</s1></fA44><fA45><s0>40 ref.</s0></fA45><fA47 i1="01" i2="1"><s0>09-0184855</s0></fA47><fA60><s1>P</s1></fA60><fA61><s0>A</s0></fA61><fA64 i1="01" i2="1"><s0>Journal of electroanalytical chemistry : (1992)</s0></fA64><fA66 i1="01"><s0>NLD</s0></fA66><fC01 i1="01" l="ENG"><s0>In this work, cobalt hexacyanoferrate (CoHCF) modified screen-printed electrodes were developed and characterised electrochemically. The effect of different cations was investigated showing a more reversible system with a well-defined peak around +0.35 V vs. Ag/AgCl when Na<sup>+</sup> was used as cation in the supporting electrolyte. The transfer coefficient (α) and the apparent charge transfer rate constant (k<sub>s</sub>) for electron transfer between the electrode and the CoHCF layer was calculated. The electrocatalytic behaviour of CoHCF towards oxidation of enzymatically generated thiocholine was thoroughly investigated. Cyclic voltammetry experiments performed in thiocholine solution showed the classical shape of mediated redox system. The diffusion constant of thiocholine was estimated using chronoamperometry. Also, the catalytic rate constant k of thiocholine at CoHCF-SPE was determined. The current due to thiocholine mediated oxidation was then evaluated in batch amperometric mode at +0.5 V vs. Ag/AgCl obtaining a linear range (5 × 10<sup>-7</sup>-1 × 10<sup>-5</sup> mol L<sup>-1</sup>) with a low detection limit and a high sensitivity equal to 5 x 10<sup>-7</sup> mol L<sup>-1</sup> and 435 mA mol<sup>-1</sup> L cm<sup>-2</sup>, respectively.</s0></fC01><fC02 i1="01" i2="X"><s0>001C04E</s0></fC02><fC03 i1="01" i2="X" l="FRE"><s0>Electrocatalyse</s0><s5>01</s5></fC03><fC03 i1="01" i2="X" l="ENG"><s0>Electrocatalysis</s0><s5>01</s5></fC03><fC03 i1="01" i2="X" l="SPA"><s0>Electrocatálisis</s0><s5>01</s5></fC03><fC03 i1="02" i2="X" l="FRE"><s0>Oxydation</s0><s5>02</s5></fC03><fC03 i1="02" i2="X" l="ENG"><s0>Oxidation</s0><s5>02</s5></fC03><fC03 i1="02" i2="X" l="SPA"><s0>Oxidación</s0><s5>02</s5></fC03><fC03 i1="03" i2="X" l="FRE"><s0>Cobalt Hexacyanoferrate</s0><s2>NC</s2><s2>NA</s2><s5>03</s5></fC03><fC03 i1="03" i2="X" l="ENG"><s0>Cobalt Hexacyanoferrates</s0><s2>NC</s2><s2>NA</s2><s5>03</s5></fC03><fC03 i1="03" i2="X" l="SPA"><s0>Cobalto Hexacianoferrato</s0><s2>NC</s2><s2>NA</s2><s5>03</s5></fC03><fC03 i1="04" i2="3" l="FRE"><s0>Electrocatalyseur</s0><s5>04</s5></fC03><fC03 i1="04" i2="3" l="ENG"><s0>Electrocatalysts</s0><s5>04</s5></fC03><fC03 i1="05" i2="X" l="FRE"><s0>Sérigraphie</s0><s5>05</s5></fC03><fC03 i1="05" i2="X" l="ENG"><s0>Serigraphy</s0><s5>05</s5></fC03><fC03 i1="05" i2="X" l="SPA"><s0>Serigrafía</s0><s5>05</s5></fC03><fC03 i1="06" i2="X" l="FRE"><s0>Electrode</s0><s5>06</s5></fC03><fC03 i1="06" i2="X" l="ENG"><s0>Electrodes</s0><s5>06</s5></fC03><fC03 i1="06" i2="X" l="SPA"><s0>Electrodo</s0><s5>06</s5></fC03><fC03 i1="07" i2="X" l="FRE"><s0>Détecteur électrochimique</s0><s5>07</s5></fC03><fC03 i1="07" i2="X" l="ENG"><s0>Electrochemical detector</s0><s5>07</s5></fC03><fC03 i1="07" i2="X" l="SPA"><s0>Detector electroquímico</s0><s5>07</s5></fC03><fC03 i1="08" i2="X" l="FRE"><s0>Matériau modifié</s0><s5>08</s5></fC03><fC03 i1="08" i2="X" l="ENG"><s0>Modified material</s0><s5>08</s5></fC03><fC03 i1="08" i2="X" l="SPA"><s0>Material modificado</s0><s5>08</s5></fC03><fC03 i1="09" i2="X" l="FRE"><s0>Sodium Chlorure</s0><s2>NC</s2><s2>NA</s2><s5>09</s5></fC03><fC03 i1="09" i2="X" l="ENG"><s0>Sodium Chlorides</s0><s2>NC</s2><s2>NA</s2><s5>09</s5></fC03><fC03 i1="09" i2="X" l="SPA"><s0>Sodio Cloruro</s0><s2>NC</s2><s2>NA</s2><s5>09</s5></fC03><fC03 i1="10" i2="X" l="FRE"><s0>Lithium Chlorure</s0><s2>NC</s2><s2>NA</s2><s5>10</s5></fC03><fC03 i1="10" i2="X" l="ENG"><s0>Lithium Chlorides</s0><s2>NC</s2><s2>NA</s2><s5>10</s5></fC03><fC03 i1="10" i2="X" l="SPA"><s0>Litio Cloruro</s0><s2>NC</s2><s2>NA</s2><s5>10</s5></fC03><fC03 i1="11" i2="X" l="FRE"><s0>Potassium Chlorure</s0><s2>NC</s2><s2>FR</s2><s2>NA</s2><s5>11</s5></fC03><fC03 i1="11" i2="X" l="ENG"><s0>Potassium Chlorides</s0><s2>NC</s2><s2>FR</s2><s2>NA</s2><s5>11</s5></fC03><fC03 i1="11" i2="X" l="SPA"><s0>Potasio Cloruro</s0><s2>NC</s2><s2>FR</s2><s2>NA</s2><s5>11</s5></fC03><fC03 i1="12" i2="X" l="FRE"><s0>Solution tampon</s0><s5>12</s5></fC03><fC03 i1="12" i2="X" l="ENG"><s0>Buffer solution</s0><s5>12</s5></fC03><fC03 i1="12" i2="X" l="SPA"><s0>Solución de amortiguación</s0><s5>12</s5></fC03><fC03 i1="13" i2="X" l="FRE"><s0>Phosphate</s0><s2>NA</s2><s5>13</s5></fC03><fC03 i1="13" i2="X" l="ENG"><s0>Phosphates</s0><s2>NA</s2><s5>13</s5></fC03><fC03 i1="13" i2="X" l="SPA"><s0>Fosfato</s0><s2>NA</s2><s5>13</s5></fC03><fC03 i1="14" i2="X" l="FRE"><s0>Réaction électrochimique</s0><s5>32</s5></fC03><fC03 i1="14" i2="X" l="ENG"><s0>Electrochemical reaction</s0><s5>32</s5></fC03><fC03 i1="14" i2="X" l="SPA"><s0>Reacción electroquímica</s0><s5>32</s5></fC03><fC03 i1="15" i2="X" l="FRE"><s0>Thiocholine</s0><s2>NK</s2><s4>INC</s4><s5>76</s5></fC03><fN21><s1>138</s1></fN21></pA></standard></inist><affiliations><list><country><li>Italie</li><li>Maroc</li></country><region><li>Latium</li></region><settlement><li>Rome</li></settlement></list><tree><country name="Italie"><region name="Latium"><name sortKey="Arduini, Fabiana" sort="Arduini, Fabiana" uniqKey="Arduini F" first="Fabiana" last="Arduini">Fabiana Arduini</name></region><name sortKey="Arduini, Fabiana" sort="Arduini, Fabiana" uniqKey="Arduini F" first="Fabiana" last="Arduini">Fabiana Arduini</name><name sortKey="Cassisi, Alessio" sort="Cassisi, Alessio" uniqKey="Cassisi A" first="Alessio" last="Cassisi">Alessio Cassisi</name><name sortKey="Cassisi, Alessio" sort="Cassisi, Alessio" uniqKey="Cassisi A" first="Alessio" last="Cassisi">Alessio Cassisi</name><name sortKey="Moscone, Danila" sort="Moscone, Danila" uniqKey="Moscone D" first="Danila" last="Moscone">Danila Moscone</name><name sortKey="Moscone, Danila" sort="Moscone, Danila" uniqKey="Moscone D" first="Danila" last="Moscone">Danila Moscone</name><name sortKey="Palleschi, Giuseppe" sort="Palleschi, Giuseppe" uniqKey="Palleschi G" first="Giuseppe" last="Palleschi">Giuseppe Palleschi</name><name sortKey="Palleschi, Giuseppe" sort="Palleschi, Giuseppe" uniqKey="Palleschi G" first="Giuseppe" last="Palleschi">Giuseppe Palleschi</name><name sortKey="Ricci, Francesco" sort="Ricci, Francesco" uniqKey="Ricci F" first="Francesco" last="Ricci">Francesco Ricci</name><name sortKey="Ricci, Francesco" sort="Ricci, Francesco" uniqKey="Ricci F" first="Francesco" last="Ricci">Francesco Ricci</name></country><country name="Maroc"><noRegion><name sortKey="Amine, Aziz" sort="Amine, Aziz" uniqKey="Amine A" first="Aziz" last="Amine">Aziz Amine</name></noRegion></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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|texte= Electrocatalytic oxidation of thiocholine at chemically modified cobalt hexacyanoferrate screen-printed electrodes
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