Structure cristalline de type alluaudite K0.4Na3.6Co(MoO4)3
Identifieur interne : 000370 ( Ncbi/Merge ); précédent : 000369; suivant : 000371Structure cristalline de type alluaudite K0.4Na3.6Co(MoO4)3
Auteurs : Rawia Nasri [Tunisie] ; Noura Fakhar Bourguiba [Tunisie] ; Mohamed Faouzi Zid [Tunisie]Source :
- Acta Crystallographica Section E: Crystallographic Communications [ 2056-9890 ] ; 2015.
Abstract
A new triple molybdate K0.4Na3.6Co(MoO4)3 was synthesized using solid-state reaction at 973 K and characterized by X-ray diffraction. The structure is characterized by
Url:
DOI: 10.1107/S2056989014025894
PubMed: 25705436
PubMed Central: 4331865
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PMC:4331865Le document en format XML
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Na<sub>3.6</sub>
Co(MoO<sub>4</sub>
)<sub>3</sub>
</title>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Structure cristalline de type alluaudite K<sub>0.4</sub>
Na<sub>3.6</sub>
Co(MoO<sub>4</sub>
)<sub>3</sub>
</title>
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</nlm:aff>
<country xml:lang="fr">Tunisie</country>
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<author><name sortKey="Fakhar Bourguiba, Noura" sort="Fakhar Bourguiba, Noura" uniqKey="Fakhar Bourguiba N" first="Noura" last="Fakhar Bourguiba">Noura Fakhar Bourguiba</name>
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<front><div type="abstract" xml:lang="en"><p>A new triple molybdate K<sub>0.4</sub>
Na<sub>3.6</sub>
Co(MoO<sub>4</sub>
)<sub>3</sub>
was synthesized using solid-state reaction at 973 K and characterized by X-ray diffraction. The structure is characterized by <italic>M</italic>
<sub>2</sub>
O<sub>10</sub>
(<italic>M</italic>
= Co/Na) dimers, which are linked by MoO<sub>4</sub>
tetrahedra, forming infinite layers. The latter are connected on one hand by insertion of Mo1O<sub>4</sub>
tetrahedra and secondly by sharing corners with Mo2O<sub>4</sub>
tetrahedra.</p>
</div>
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Na<sub>3.6</sub>
Co(MoO<sub>4</sub>
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<author><name sortKey="Zid, Mohamed Faouzi" sort="Zid, Mohamed Faouzi" uniqKey="Zid M" first="Mohamed Faouzi" last="Zid">Mohamed Faouzi Zid</name>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">Structure cristalline de type alluaudite K<sub>0.4</sub>
Na<sub>3.6</sub>
Co(MoO<sub>4</sub>
)<sub>3</sub>
</title>
<author><name sortKey="Nasri, Rawia" sort="Nasri, Rawia" uniqKey="Nasri R" first="Rawia" last="Nasri">Rawia Nasri</name>
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</nlm:aff>
<country xml:lang="fr">Tunisie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
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<author><name sortKey="Fakhar Bourguiba, Noura" sort="Fakhar Bourguiba, Noura" uniqKey="Fakhar Bourguiba N" first="Noura" last="Fakhar Bourguiba">Noura Fakhar Bourguiba</name>
<affiliation wicri:level="1"><nlm:aff id="a">Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis,<country>Tunisie</country>
</nlm:aff>
<country xml:lang="fr">Tunisie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
</affiliation>
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<author><name sortKey="Zid, Mohamed Faouzi" sort="Zid, Mohamed Faouzi" uniqKey="Zid M" first="Mohamed Faouzi" last="Zid">Mohamed Faouzi Zid</name>
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</nlm:aff>
<country xml:lang="fr">Tunisie</country>
<wicri:regionArea># see nlm:aff country strict</wicri:regionArea>
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<front><div type="abstract" xml:lang="en"><p>A new triple molybdate K<sub>0.4</sub>
Na<sub>3.6</sub>
Co(MoO<sub>4</sub>
)<sub>3</sub>
was synthesized using solid-state reaction at 973 K and characterized by X-ray diffraction. The structure is characterized by <italic>M</italic>
<sub>2</sub>
O<sub>10</sub>
(<italic>M</italic>
= Co/Na) dimers, which are linked by MoO<sub>4</sub>
tetrahedra, forming infinite layers. The latter are connected on one hand by insertion of Mo1O<sub>4</sub>
tetrahedra and secondly by sharing corners with Mo2O<sub>4</sub>
tetrahedra.</p>
</div>
</front>
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<pubmed><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Structure cristalline de type alluaudite K0.4Na3.6Co(MoO4)3.</title>
<author><name sortKey="Nasri, Rawia" sort="Nasri, Rawia" uniqKey="Nasri R" first="Rawia" last="Nasri">Rawia Nasri</name>
<affiliation wicri:level="4"><nlm:affiliation>Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis, Tunisie.</nlm:affiliation>
<country xml:lang="fr">Tunisie</country>
<wicri:regionArea>Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis</wicri:regionArea>
<orgName type="university">Université de Tunis - El Manar</orgName>
<placeName><settlement type="city">Tunis</settlement>
<region type="region" nuts="2">Gouvernorat de Tunis</region>
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</author>
<author><name sortKey="Fakhar Bourguiba, Noura" sort="Fakhar Bourguiba, Noura" uniqKey="Fakhar Bourguiba N" first="Noura" last="Fakhar Bourguiba">Noura Fakhar Bourguiba</name>
<affiliation wicri:level="4"><nlm:affiliation>Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis, Tunisie.</nlm:affiliation>
<country xml:lang="fr">Tunisie</country>
<wicri:regionArea>Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis</wicri:regionArea>
<orgName type="university">Université de Tunis - El Manar</orgName>
<placeName><settlement type="city">Tunis</settlement>
<region type="region" nuts="2">Gouvernorat de Tunis</region>
</placeName>
</affiliation>
</author>
<author><name sortKey="Zid, Mohamed Faouzi" sort="Zid, Mohamed Faouzi" uniqKey="Zid M" first="Mohamed Faouzi" last="Zid">Mohamed Faouzi Zid</name>
<affiliation wicri:level="4"><nlm:affiliation>Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis, Tunisie.</nlm:affiliation>
<country xml:lang="fr">Tunisie</country>
<wicri:regionArea>Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis</wicri:regionArea>
<orgName type="university">Université de Tunis - El Manar</orgName>
<placeName><settlement type="city">Tunis</settlement>
<region type="region" nuts="2">Gouvernorat de Tunis</region>
</placeName>
</affiliation>
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<sourceDesc><biblStruct><analytic><title xml:lang="en">Structure cristalline de type alluaudite K0.4Na3.6Co(MoO4)3.</title>
<author><name sortKey="Nasri, Rawia" sort="Nasri, Rawia" uniqKey="Nasri R" first="Rawia" last="Nasri">Rawia Nasri</name>
<affiliation wicri:level="4"><nlm:affiliation>Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis, Tunisie.</nlm:affiliation>
<country xml:lang="fr">Tunisie</country>
<wicri:regionArea>Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis</wicri:regionArea>
<orgName type="university">Université de Tunis - El Manar</orgName>
<placeName><settlement type="city">Tunis</settlement>
<region type="region" nuts="2">Gouvernorat de Tunis</region>
</placeName>
</affiliation>
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<author><name sortKey="Fakhar Bourguiba, Noura" sort="Fakhar Bourguiba, Noura" uniqKey="Fakhar Bourguiba N" first="Noura" last="Fakhar Bourguiba">Noura Fakhar Bourguiba</name>
<affiliation wicri:level="4"><nlm:affiliation>Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis, Tunisie.</nlm:affiliation>
<country xml:lang="fr">Tunisie</country>
<wicri:regionArea>Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis</wicri:regionArea>
<orgName type="university">Université de Tunis - El Manar</orgName>
<placeName><settlement type="city">Tunis</settlement>
<region type="region" nuts="2">Gouvernorat de Tunis</region>
</placeName>
</affiliation>
</author>
<author><name sortKey="Zid, Mohamed Faouzi" sort="Zid, Mohamed Faouzi" uniqKey="Zid M" first="Mohamed Faouzi" last="Zid">Mohamed Faouzi Zid</name>
<affiliation wicri:level="4"><nlm:affiliation>Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis El Manar, 2092 El Manar Tunis, Tunisie.</nlm:affiliation>
<country xml:lang="fr">Tunisie</country>
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<orgName type="university">Université de Tunis - El Manar</orgName>
<placeName><settlement type="city">Tunis</settlement>
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</placeName>
</affiliation>
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<imprint><date when="2015" type="published">2015</date>
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<front><div type="abstract" xml:lang="en">A new triple molybdate, potassium sodium cobalt tris-(molybdate), K0.4Na3.6Co(MoO4)3, was synthesized using solid-state reactions. The Co(2+) and one Na(+) cation are located at the same general site, each with occupancy 0.5. Another site (site symmetry 2) is occupied by Na(+) and K(+) cations, with occupancies of 0.597 (7) and 0.402 (6), respectively. The other two Na(+) cations and one of the two Mo atoms lie on special positions (site symmetries -1, 2 and 2, respectively). The structure is characterized by M 2O10 (M = Co/Na) dimers, which are linked by MoO4 tetra-hedra, forming infinite layers. The latter are connected firstly by insertion of one type of MoO4 tetra-hedra and secondly by sharing corners with the other type of MoO4 tetra-hedra. This results in an open three-dimensional framework with the cavities occupied by the Na(+) and K(+) cations. The structure is isotypic with Na3In2As3O12 and Na3In2P3O12. A comparison is made with structures such as K2Co2(MoO4)3 and β-NaFe2(MoO4)3 and their differences are discussed.</div>
</front>
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