Cobalt spinel CoAl2O4 via sol-gel process : elaboration and surface properties
Identifieur interne : 000D69 ( Main/Merge ); précédent : 000D68; suivant : 000D70Cobalt spinel CoAl2O4 via sol-gel process : elaboration and surface properties
Auteurs : S. Chemlal [Maroc] ; A. Larbot [France] ; M. Persin [France] ; J. Sarrazin [France] ; M. Sghyar [Maroc] ; M. Rafiq [Maroc]Source :
- Materials research bulletin [ 0025-5408 ] ; 2000.
Descripteurs français
- Pascal (Inist)
- Etude expérimentale, Poudre, Procédé sol gel, Suspension colloïdale, Déstatisation, Traitement thermique, Cristallisation, Spinelles, Aluminium oxyde, Cobalt oxyde, Caractérisation, Propriété thermique, Morphologie, Aire superficielle, Charge superficielle, pH, Mobilité électrophorétique, Coulée en barbotine, 8270, 8110D, Membrane, Ultrafiltration, CoAl2O4, Al Co O.
English descriptors
- KwdEn :
- Aluminium oxide, Characterization, Cobalt oxide, Colloidal suspension, Crystallization, Destatization, Electrophoretic mobility, Experimental study, Heat treatment, Membrane, Morphology, Powder, Slip casting, Sol gel process, Spinels, Surface area, Surface charge, Thermal properties, Ultrafiltration, pH.
Abstract
In this work the preparation of cobalt spinel CoAl2O4 is described. The technique of colloidal solution destabilization was used as the sol-gel process. The powder obtained from the dried gel was characterized by thermal analysis (thermogravimetric and differential), X-ray diffraction, infrared spectroscopy, and specific surface area measurement. Crystallization of CoAl2O4 spinels occurs at about 400°C. The study of surface properties (surface charge and electrophoretic mobility) of the spinel powder fired at 600°C, in suspension in different electrolyte solutions (10-3 molar ionic strength), shows that the spinel material charge depends on the pH of the solution. The spinel sol was used for the preparation of membrane by the slip-casting method.
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Pascal:01-0421046Le document en format XML
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O<sub>4</sub>
via sol-gel process : elaboration and surface properties</title>
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a">Cobalt spinel CoAl<sub>2</sub>
O<sub>4</sub>
via sol-gel process : elaboration and surface properties</title>
<author><name sortKey="Chemlal, S" sort="Chemlal, S" uniqKey="Chemlal S" first="S." last="Chemlal">S. Chemlal</name>
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<author><name sortKey="Rafiq, M" sort="Rafiq, M" uniqKey="Rafiq M" first="M." last="Rafiq">M. Rafiq</name>
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<series><title level="j" type="main">Materials research bulletin</title>
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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Aluminium oxide</term>
<term>Characterization</term>
<term>Cobalt oxide</term>
<term>Colloidal suspension</term>
<term>Crystallization</term>
<term>Destatization</term>
<term>Electrophoretic mobility</term>
<term>Experimental study</term>
<term>Heat treatment</term>
<term>Membrane</term>
<term>Morphology</term>
<term>Powder</term>
<term>Slip casting</term>
<term>Sol gel process</term>
<term>Spinels</term>
<term>Surface area</term>
<term>Surface charge</term>
<term>Thermal properties</term>
<term>Ultrafiltration</term>
<term>pH</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Etude expérimentale</term>
<term>Poudre</term>
<term>Procédé sol gel</term>
<term>Suspension colloïdale</term>
<term>Déstatisation</term>
<term>Traitement thermique</term>
<term>Cristallisation</term>
<term>Spinelles</term>
<term>Aluminium oxyde</term>
<term>Cobalt oxyde</term>
<term>Caractérisation</term>
<term>Propriété thermique</term>
<term>Morphologie</term>
<term>Aire superficielle</term>
<term>Charge superficielle</term>
<term>pH</term>
<term>Mobilité électrophorétique</term>
<term>Coulée en barbotine</term>
<term>8270</term>
<term>8110D</term>
<term>Membrane</term>
<term>Ultrafiltration</term>
<term>CoAl2O4</term>
<term>Al Co O</term>
</keywords>
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<front><div type="abstract" xml:lang="en">In this work the preparation of cobalt spinel CoAl<sub>2</sub>
O<sub>4</sub>
is described. The technique of colloidal solution destabilization was used as the sol-gel process. The powder obtained from the dried gel was characterized by thermal analysis (thermogravimetric and differential), X-ray diffraction, infrared spectroscopy, and specific surface area measurement. Crystallization of CoAl<sub>2</sub>
O<sub>4</sub>
spinels occurs at about 400°C. The study of surface properties (surface charge and electrophoretic mobility) of the spinel powder fired at 600°C, in suspension in different electrolyte solutions (10<sup>-3</sup>
molar ionic strength), shows that the spinel material charge depends on the pH of the solution. The spinel sol was used for the preparation of membrane by the slip-casting method.</div>
</front>
</TEI>
<affiliations><list><country><li>France</li>
<li>Maroc</li>
</country>
<region><li>Languedoc-Roussillon</li>
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<name sortKey="Rafiq, M" sort="Rafiq, M" uniqKey="Rafiq M" first="M." last="Rafiq">M. Rafiq</name>
<name sortKey="Sghyar, M" sort="Sghyar, M" uniqKey="Sghyar M" first="M." last="Sghyar">M. Sghyar</name>
</country>
<country name="France"><region name="Occitanie (région administrative)"><name sortKey="Larbot, A" sort="Larbot, A" uniqKey="Larbot A" first="A." last="Larbot">A. Larbot</name>
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<name sortKey="Sarrazin, J" sort="Sarrazin, J" uniqKey="Sarrazin J" first="J." last="Sarrazin">J. Sarrazin</name>
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