Preparation of Co-Sn alloys by electroreduction of Co(II) and Sn(II) in molten LiCl-KCl
Identifieur interne : 000631 ( Main/Curation ); précédent : 000630; suivant : 000632Preparation of Co-Sn alloys by electroreduction of Co(II) and Sn(II) in molten LiCl-KCl
Auteurs : H. Groult [France] ; H. El Ghallali [France, Maroc] ; A. Barhoun [Maroc] ; E. Briot [France] ; L. Perrigaud [France] ; S. Hernandorena [France] ; F. Lantelme [France]Source :
- Electrochimica acta [ 0013-4686 ] ; 2010.
Descripteurs français
- Pascal (Inist)
- Potassium Chlorure, Lithium Chlorure, Réduction chimique, Cobalt alliage, Etain alliage, Sel fondu, Electrolyte fondu, Alliage binaire, Dépôt électrolytique, Cobalt II Composé, Etain II Composé, Effet température, Electrode, Carbone, Etat vitreux, Molybdène, Microscopie électronique balayage, Diffraction RX, Réaction électrochimique, Condition opératoire, Structure surface, Morphologie.
- Wicri :
English descriptors
- KwdEn :
- Binary alloy, Carbon, Chemical reduction, Cobalt II Compounds, Cobalt alloy, Electrochemical reaction, Electrodeposition, Electrodes, Glassy state, Lithium Chlorides, Molten electrolyte, Molten salt, Molybdenum, Morphology, Operating conditions, Potassium Chlorides, Scanning electron microscopy, Surface structure, Temperature effect, Tin II Compounds, Tin alloy, X ray diffraction.
Abstract
Co-Sn alloys were prepared by an electrochemical route in molten LiCl-KCl between 400 and 550 °C. The Sn(IV)/Sn(II), Sn(II)/Sn(0) and Co(II)/Co(0) redox couples were studied by cyclic voltammetry and/or chronopotentiometry over the temperature range. The diffusion coefficient values of Co(II) ions were measured. For example, it was found that the DCo(II) values deduced from chronopotentiometry range from DCo(II) = 1.65 x 10-5 cm2 s-1 at 400°C to 4.95 × 10-5 cm2 s-1 at 550°C. The standard potential of the Co(II)/Co(0) redox couple in molten LiCl-KCl was measured at 400°C: E0Co(II)/Co(0) = -1.35 V vs Cl2/Cl-. Finally, Co-Sn alloys were prepared in potentiostatic mode. The influence of the temperature of molten LiCl-KCl, the applied potential and the deposition time on the morphology and the composition of the Co-Sn alloys were also investigated. For T > 450°C, the following tendency has been observed: the more negative the potential, the higher the Sn content in the deposited alloy. Thus, depending on the operating conditions, pure CoSn or CoSn2 can be prepared.
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Groult</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>UPMC Univ Paris 06, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>CNRS, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation></author><author><name sortKey="El Ghallali, H" sort="El Ghallali, H" uniqKey="El Ghallali H" first="H." last="El Ghallali">H. El Ghallali</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>UPMC Univ Paris 06, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation><affiliation wicri:level="1"><inist:fA14 i1="03"><s1>Université Abdelmalek Essaâdi, Faculté des Sciences, LPCIE</s1><s2>93000 Tétouan</s2><s3>MAR</s3><sZ>2 aut.</sZ><sZ>3 aut.</sZ></inist:fA14><country>Maroc</country><wicri:noRegion>93000 Tétouan</wicri:noRegion></affiliation></author><author><name sortKey="Barhoun, A" sort="Barhoun, A" uniqKey="Barhoun A" first="A." last="Barhoun">A. Barhoun</name><affiliation wicri:level="1"><inist:fA14 i1="03"><s1>Université Abdelmalek Essaâdi, Faculté des Sciences, LPCIE</s1><s2>93000 Tétouan</s2><s3>MAR</s3><sZ>2 aut.</sZ><sZ>3 aut.</sZ></inist:fA14><country>Maroc</country><wicri:noRegion>93000 Tétouan</wicri:noRegion></affiliation></author><author><name sortKey="Briot, E" sort="Briot, E" uniqKey="Briot E" first="E." last="Briot">E. 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Perrigaud</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>UPMC Univ Paris 06, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>CNRS, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation></author><author><name sortKey="Hernandorena, S" sort="Hernandorena, S" uniqKey="Hernandorena S" first="S." last="Hernandorena">S. Hernandorena</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>UPMC Univ Paris 06, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>CNRS, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation></author><author><name sortKey="Lantelme, F" sort="Lantelme, F" uniqKey="Lantelme F" first="F." last="Lantelme">F. 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Groult</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>UPMC Univ Paris 06, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>CNRS, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation></author><author><name sortKey="El Ghallali, H" sort="El Ghallali, H" uniqKey="El Ghallali H" first="H." last="El Ghallali">H. El Ghallali</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>UPMC Univ Paris 06, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation><affiliation wicri:level="1"><inist:fA14 i1="03"><s1>Université Abdelmalek Essaâdi, Faculté des Sciences, LPCIE</s1><s2>93000 Tétouan</s2><s3>MAR</s3><sZ>2 aut.</sZ><sZ>3 aut.</sZ></inist:fA14><country>Maroc</country><wicri:noRegion>93000 Tétouan</wicri:noRegion></affiliation></author><author><name sortKey="Barhoun, A" sort="Barhoun, A" uniqKey="Barhoun A" first="A." last="Barhoun">A. Barhoun</name><affiliation wicri:level="1"><inist:fA14 i1="03"><s1>Université Abdelmalek Essaâdi, Faculté des Sciences, LPCIE</s1><s2>93000 Tétouan</s2><s3>MAR</s3><sZ>2 aut.</sZ><sZ>3 aut.</sZ></inist:fA14><country>Maroc</country><wicri:noRegion>93000 Tétouan</wicri:noRegion></affiliation></author><author><name sortKey="Briot, E" sort="Briot, E" uniqKey="Briot E" first="E." last="Briot">E. Briot</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>UPMC Univ Paris 06, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>CNRS, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation></author><author><name sortKey="Perrigaud, L" sort="Perrigaud, L" uniqKey="Perrigaud L" first="L." last="Perrigaud">L. Perrigaud</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>UPMC Univ Paris 06, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>CNRS, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation></author><author><name sortKey="Hernandorena, S" sort="Hernandorena, S" uniqKey="Hernandorena S" first="S." last="Hernandorena">S. Hernandorena</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>UPMC Univ Paris 06, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>CNRS, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation></author><author><name sortKey="Lantelme, F" sort="Lantelme, F" uniqKey="Lantelme F" first="F." last="Lantelme">F. Lantelme</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>UPMC Univ Paris 06, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>CNRS, UMR 7195 PECSA, Physicochimie des Electrolytes, Colloïdes, Sciences Analytiques</s1><s2>75005 Paris</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Île-de-France</region><settlement type="city">Paris</settlement></placeName></affiliation></author></analytic><series><title level="j" type="main">Electrochimica acta</title><title level="j" type="abbreviated">Electrochim. acta</title><idno type="ISSN">0013-4686</idno><imprint><date when="2010">2010</date></imprint></series></biblStruct></sourceDesc><seriesStmt><title level="j" type="main">Electrochimica acta</title><title level="j" type="abbreviated">Electrochim. acta</title><idno type="ISSN">0013-4686</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Binary alloy</term><term>Carbon</term><term>Chemical reduction</term><term>Cobalt II Compounds</term><term>Cobalt alloy</term><term>Electrochemical reaction</term><term>Electrodeposition</term><term>Electrodes</term><term>Glassy state</term><term>Lithium Chlorides</term><term>Molten electrolyte</term><term>Molten salt</term><term>Molybdenum</term><term>Morphology</term><term>Operating conditions</term><term>Potassium Chlorides</term><term>Scanning electron microscopy</term><term>Surface structure</term><term>Temperature effect</term><term>Tin II Compounds</term><term>Tin alloy</term><term>X ray diffraction</term></keywords><keywords scheme="Pascal" xml:lang="fr"><term>Potassium Chlorure</term><term>Lithium Chlorure</term><term>Réduction chimique</term><term>Cobalt alliage</term><term>Etain alliage</term><term>Sel fondu</term><term>Electrolyte fondu</term><term>Alliage binaire</term><term>Dépôt électrolytique</term><term>Cobalt II Composé</term><term>Etain II Composé</term><term>Effet température</term><term>Electrode</term><term>Carbone</term><term>Etat vitreux</term><term>Molybdène</term><term>Microscopie électronique balayage</term><term>Diffraction RX</term><term>Réaction électrochimique</term><term>Condition opératoire</term><term>Structure surface</term><term>Morphologie</term></keywords><keywords scheme="Wicri" type="topic" xml:lang="fr"><term>Carbone</term><term>Molybdène</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Co-Sn alloys were prepared by an electrochemical route in molten LiCl-KCl between 400 and 550 °C. The Sn(IV)/Sn(II), Sn(II)/Sn(0) and Co(II)/Co(0) redox couples were studied by cyclic voltammetry and/or chronopotentiometry over the temperature range. The diffusion coefficient values of Co(II) ions were measured. For example, it was found that the D<sub>Co</sub>(II) values deduced from chronopotentiometry range from D<sub>Co</sub>(II) = 1.65 x 10<sup>-5</sup> cm<sup>2</sup> s<sup>-1</sup> at 400°C to 4.95 × 10<sup>-5 </sup>cm<sup>2</sup> s<sup>-1</sup> at 550°C. The standard potential of the Co(II)/Co(0) redox couple in molten LiCl-KCl was measured at 400°C: E<sup>0</sup><sub>Co(II)/Co(0)</sub> = -1.35 V vs Cl<sub>2</sub>/Cl<sup>-</sup>. Finally, Co-Sn alloys were prepared in potentiostatic mode. The influence of the temperature of molten LiCl-KCl, the applied potential and the deposition time on the morphology and the composition of the Co-Sn alloys were also investigated. For T > 450°C, the following tendency has been observed: the more negative the potential, the higher the Sn content in the deposited alloy. Thus, depending on the operating conditions, pure CoSn or CoSn<sub>2</sub> can be prepared.</div></front></TEI></record>Pour manipuler ce document sous Unix (Dilib)
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