A new solution route to silicates. Part 3: Aqueous sol-gel synthesis of willemite and potassium antimony silicate
Identifieur interne : 000B92 ( Istex/Corpus ); précédent : 000B91; suivant : 000B93A new solution route to silicates. Part 3: Aqueous sol-gel synthesis of willemite and potassium antimony silicate
Auteurs : L. Reynaud ; C. Brouca-Cabarrecq ; A. Mosset ; H. AhamdaneSource :
- Materials Research Bulletin [ 0025-5408 ] ; 1996.
Abstract
Willemite, α-Zn2SiO4, and KSbOSiO4 (KSS) were prepared by an aqueous sol-gel process, starting from a H2Si2O5 solution as silicon source. Willemite was obtained free from impurities, in a teflon-lined bomb at 473 K under autogenous pressure. In the case of KSS, the same procedure results in a clear solution which gives, by evaporation at room temperature, an amorphous gel. Orthorhombic KSS crystallizes from this gel at 1273 K.
Url:
DOI: 10.1016/0025-5408(96)00097-9
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<front><div type="abstract" xml:lang="en">Willemite, α-Zn2SiO4, and KSbOSiO4 (KSS) were prepared by an aqueous sol-gel process, starting from a H2Si2O5 solution as silicon source. Willemite was obtained free from impurities, in a teflon-lined bomb at 473 K under autogenous pressure. In the case of KSS, the same procedure results in a clear solution which gives, by evaporation at room temperature, an amorphous gel. Orthorhombic KSS crystallizes from this gel at 1273 K.</div>
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