Polymerization of methyl methacrylate with Nickel(II)α‐benzoinoxime complex
Identifieur interne : 000A42 ( Istex/Corpus ); précédent : 000A41; suivant : 000A43Polymerization of methyl methacrylate with Nickel(II)α‐benzoinoxime complex
Auteurs : Hafida Harrar-Ferfera ; Farouk AmraniSource :
- Journal of Applied Polymer Science [ 0021-8995 ] ; 2008-05-05.
English descriptors
Abstract
Polymerizations of methyl methacrylate (MMA) monomer initiated by a novel Ni(II)α‐benzoinoxime complex have been achieved under homogeneous conditions in the 25–60°C temperature range. The activity for polymerization increases with reaction temperature and by carrying out the polymerization in solution of low‐polarity solvents without any induction time. The obtained polymers have weight‐average molecular weights about 105 and slight broad polydispersity indexes (2.2 ≤ Mw/Mn ≤ 3.3). Dependence of rate constants polymerization and decomposition of initiator (kapp and kd, respectively) on temperature was investigated and activation parameters were computed from Arrhenius plot. 1H‐NMR analysis of PMMA revealed a syndio‐rich atactic microstructure in agreement with conventional radical process. Radical scavenger TEMPO effect together with microstructure and molecular weight distributions data supported that the polymerization proceed via free radical mechanism. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008
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DOI: 10.1002/app.24711
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The activity for polymerization increases with reaction temperature and by carrying out the polymerization in solution of low‐polarity solvents without any induction time. The obtained polymers have weight‐average molecular weights about 105 and slight broad polydispersity indexes (2.2 ≤ Mw/Mn ≤ 3.3). Dependence of rate constants polymerization and decomposition of initiator (kapp and kd, respectively) on temperature was investigated and activation parameters were computed from Arrhenius plot. 1H‐NMR analysis of PMMA revealed a syndio‐rich atactic microstructure in agreement with conventional radical process. Radical scavenger TEMPO effect together with microstructure and molecular weight distributions data supported that the polymerization proceed via free radical mechanism. © 2008 Wiley Periodicals, Inc. 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The activity for polymerization increases with reaction temperature and by carrying out the polymerization in solution of low‐polarity solvents without any induction time. The obtained polymers have weight‐average molecular weights about 10<sup>5</sup> and slight broad polydispersity indexes (2.2 ≤ <i>M<sub>w</sub></i>/<i>M<sub>n</sub></i> ≤ 3.3). Dependence of rate constants polymerization and decomposition of initiator (<i>k</i><sub>app</sub> and <i>k<sub>d</sub></i>, respectively) on temperature was investigated and activation parameters were computed from Arrhenius plot. <sup>1</sup>H‐NMR analysis of PMMA revealed a syndio‐rich atactic microstructure in agreement with conventional radical process. Radical scavenger TEMPO effect together with microstructure and molecular weight distributions data supported that the polymerization proceed via free radical mechanism. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008</p></abstract></abstractGroup></contentMeta></header></component></istex:document></istex:metadataXml><mods version="3.6"><titleInfo lang="en"><title>Polymerization of methyl methacrylate with Nickel(II)α‐benzoinoxime complex</title></titleInfo><titleInfo type="abbreviated" lang="en"><title>Polymerization of MMA with Ni(II)α‐Benzoinoxime</title></titleInfo><titleInfo type="alternative" contentType="CDATA" lang="en"><title>Polymerization of methyl methacrylate with Nickel(II)α‐benzoinoxime complex</title></titleInfo><name type="personal"><namePart type="given">Hafida</namePart><namePart type="family">Harrar‐Ferfera</namePart><affiliation>Faculty of Chemistry, University of Sciences and Technology, Houari Boumediene, Algiers 16111, Algeria</affiliation><affiliation>Faculty of Chemistry, University of Sciences and Technology, Houari Boumediene, Algiers 16111, Algeria===</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Farouk</namePart><namePart type="family">Amrani</namePart><affiliation>Faculty of Chemistry, University of Sciences and Technology, Houari Boumediene, Algiers 16111, Algeria</affiliation><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="article" displayLabel="article"></genre><originInfo><publisher>Wiley Subscription Services, Inc., A Wiley Company</publisher><place><placeTerm type="text">Hoboken</placeTerm></place><dateIssued encoding="w3cdtf">2008-05-05</dateIssued><dateCaptured encoding="w3cdtf">2005-12-20</dateCaptured><dateValid encoding="w3cdtf">2006-04-17</dateValid><copyrightDate encoding="w3cdtf">2008</copyrightDate></originInfo><language><languageTerm type="code" authority="rfc3066">en</languageTerm><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType><extent unit="figures">10</extent><extent unit="tables">4</extent><extent unit="references">39</extent><extent unit="words">5267</extent></physicalDescription><abstract lang="en">Polymerizations of methyl methacrylate (MMA) monomer initiated by a novel Ni(II)α‐benzoinoxime complex have been achieved under homogeneous conditions in the 25–60°C temperature range. The activity for polymerization increases with reaction temperature and by carrying out the polymerization in solution of low‐polarity solvents without any induction time. The obtained polymers have weight‐average molecular weights about 105 and slight broad polydispersity indexes (2.2 ≤ Mw/Mn ≤ 3.3). Dependence of rate constants polymerization and decomposition of initiator (kapp and kd, respectively) on temperature was investigated and activation parameters were computed from Arrhenius plot. 1H‐NMR analysis of PMMA revealed a syndio‐rich atactic microstructure in agreement with conventional radical process. Radical scavenger TEMPO effect together with microstructure and molecular weight distributions data supported that the polymerization proceed via free radical mechanism. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008</abstract><subject lang="en"><genre>keywords</genre><topic>radical polymerization</topic><topic>kinetics</topic><topic>microstructure, Ni(II)</topic><topic>complex</topic></subject><relatedItem type="host"><titleInfo><title>Journal of Applied Polymer Science</title></titleInfo><titleInfo type="abbreviated"><title>J. Appl. Polym. 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