Studies on coordination compounds—VIII. Syntheses, structural, magnetic, spectral and thermal properties of some cobalt(II), nickel(II) and copper(II) complexes of 2-aminopyrimidine
Identifieur interne : 000590 ( Istex/Corpus ); précédent : 000589; suivant : 000591Studies on coordination compounds—VIII. Syntheses, structural, magnetic, spectral and thermal properties of some cobalt(II), nickel(II) and copper(II) complexes of 2-aminopyrimidine
Auteurs : Paavo O. Lumme ; Hilkka KnuuttilaSource :
- Polyhedron [ 0277-5387 ] ; 1995.
Abstract
The complexes bis[triaqua(2-aminopyrimidine)-μ-sulphato-O,O′-cobalt(II)] dihydrate (1), catena-[diaqua(2(2-aminopyrimidine))-μ-sulphato-O,O′nickel(II)]2-amino-pyrimidine (2), [pentaaqua(2-aminopyrimidine)nickel(II)]sulphate 2-aminopyrimidine (3) and catena-[aqua(2(2-aminopyrimidine))-μ-sulphato-O,O′-copper(II)] dihydrate (4) were prepared, structure determined by X-ray methods and physical properties studied by magnetic, IR, NMR, EPR and reflectance methods. The thermal behaviour was studied by TG and mass spectrometric methods. The results are discussed on a structural basis.
Url:
DOI: 10.1016/0277-5387(94)00442-H
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Box 6, SF-00014, Helsinki, Finland</mods:affiliation></affiliation></author><author><name sortKey="Knuuttila, Hilkka" sort="Knuuttila, Hilkka" uniqKey="Knuuttila H" first="Hilkka" last="Knuuttila">Hilkka Knuuttila</name><affiliation><mods:affiliation>Department of Chemistry, University of Jyväskylä, Jyväskylä, Finland</mods:affiliation></affiliation></author></titleStmt><publicationStmt><idno type="wicri:source">ISTEX</idno><idno type="RBID">ISTEX:90F6EE7CF1BCFDDA3E1BE5DDBEF400919C0A94A1</idno><date when="1995" year="1995">1995</date><idno type="doi">10.1016/0277-5387(94)00442-H</idno><idno type="url">https://api.istex.fr/document/90F6EE7CF1BCFDDA3E1BE5DDBEF400919C0A94A1/fulltext/pdf</idno><idno type="wicri:Area/Istex/Corpus">000590</idno><idno type="wicri:explorRef" wicri:stream="Istex" wicri:step="Corpus" wicri:corpus="ISTEX">000590</idno></publicationStmt><sourceDesc><biblStruct><analytic><title level="a">Studies on coordination compounds—VIII. 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Box 6, SF-00014, Helsinki, Finland</affiliation></author><author xml:id="author-2"><persName><forename type="first">Hilkka</forename><surname>Knuuttila</surname></persName><note type="biography">Present address: Research Centre, Neste OY, 06850 Kulloo, Finland.</note><affiliation>Present address: Research Centre, Neste OY, 06850 Kulloo, Finland.</affiliation><affiliation>Department of Chemistry, University of Jyväskylä, Jyväskylä, Finland</affiliation></author></analytic><monogr><title level="j">Polyhedron</title><title level="j" type="abbrev">POLY</title><idno type="pISSN">0277-5387</idno><idno type="PII">S0277-5387(00)X0026-5</idno><imprint><publisher>ELSEVIER</publisher><date type="published" when="1995"></date><biblScope unit="volume">14</biblScope><biblScope unit="issue">12</biblScope><biblScope unit="page" from="1553">1553</biblScope><biblScope unit="page" to="1563">1563</biblScope></imprint></monogr><idno type="istex">90F6EE7CF1BCFDDA3E1BE5DDBEF400919C0A94A1</idno><idno type="DOI">10.1016/0277-5387(94)00442-H</idno><idno type="PII">0277-5387(94)00442-H</idno></biblStruct></sourceDesc></fileDesc><profileDesc><creation><date>1995</date></creation><langUsage><language ident="en">en</language></langUsage><abstract xml:lang="en"><p>The complexes bis[triaqua(2-aminopyrimidine)-μ-sulphato-O,O′-cobalt(II)] dihydrate (1), catena-[diaqua(2(2-aminopyrimidine))-μ-sulphato-O,O′nickel(II)]2-amino-pyrimidine (2), [pentaaqua(2-aminopyrimidine)nickel(II)]sulphate 2-aminopyrimidine (3) and catena-[aqua(2(2-aminopyrimidine))-μ-sulphato-O,O′-copper(II)] dihydrate (4) were prepared, structure determined by X-ray methods and physical properties studied by magnetic, IR, NMR, EPR and reflectance methods. The thermal behaviour was studied by TG and mass spectrometric methods. The results are discussed on a structural basis.</p></abstract></profileDesc><revisionDesc><change when="1995">Published</change></revisionDesc></teiHeader></istex:fulltextTEI><json:item><original>false</original><mimetype>text/plain</mimetype><extension>txt</extension><uri>https://api.istex.fr/document/90F6EE7CF1BCFDDA3E1BE5DDBEF400919C0A94A1/fulltext/txt</uri></json:item></fulltext><metadata><istex:metadataXml wicri:clean="Elsevier, elements deleted: tail"><istex:xmlDeclaration>version="1.0" encoding="utf-8"</istex:xmlDeclaration><istex:docType PUBLIC="-//ES//DTD journal article DTD version 4.5.2//EN//XML" URI="art452.dtd" name="istex:docType"></istex:docType><istex:document><converted-article version="4.5.2" docsubtype="fla"><item-info><jid>POLY</jid><aid>9400442H</aid><ce:pii>0277-5387(94)00442-H</ce:pii><ce:doi>10.1016/0277-5387(94)00442-H</ce:doi><ce:copyright type="unknown" year="1995"></ce:copyright></item-info><head><ce:article-footnote><ce:label>☆</ce:label><ce:note-para>Part VII: P. Lumme and P. Knuuttila, <ce:italic>J. Thermal Analysis</ce:italic> 1982, <ce:bold>25</ce:bold>, 139.</ce:note-para></ce:article-footnote><ce:title>Studies on coordination compounds—VIII. Syntheses, structural, magnetic, spectral and thermal properties of some cobalt(II), nickel(II) and copper(II) complexes of 2-aminopyrimidine</ce:title><ce:author-group><ce:author><ce:given-name>Paavo O.</ce:given-name><ce:surname>Lumme</ce:surname><ce:cross-ref refid="COR1"><ce:sup>†</ce:sup></ce:cross-ref></ce:author><ce:affiliation><ce:textfn>Division of Inorganic Chemistry, Department of Chemistry, University of Helsinki, Vuorikatu 20, P.O. Box 6, SF-00014, Helsinki, Finland</ce:textfn></ce:affiliation><ce:correspondence id="COR1"><ce:label>†</ce:label><ce:text>Author to whom correspondence should be addressed.</ce:text></ce:correspondence></ce:author-group><ce:author-group><ce:author><ce:given-name>Hilkka</ce:given-name><ce:surname>Knuuttila</ce:surname><ce:cross-ref refid="FN1"><ce:sup>‡</ce:sup></ce:cross-ref></ce:author><ce:affiliation><ce:textfn>Department of Chemistry, University of Jyväskylä, Jyväskylä, Finland</ce:textfn></ce:affiliation><ce:footnote id="FN1"><ce:label>‡</ce:label><ce:note-para>Present address: Research Centre, Neste OY, 06850 Kulloo, Finland.</ce:note-para></ce:footnote></ce:author-group><ce:date-received day="5" month="5" year="1994"></ce:date-received><ce:date-accepted day="24" month="10" year="1994"></ce:date-accepted><ce:abstract><ce:section-title>Abstract</ce:section-title><ce:abstract-sec><ce:simple-para>The complexes bis[triaqua(2-aminopyrimidine)-μ-sulphato-O,O′-cobalt(II)] dihydrate (<ce:bold>1</ce:bold>), <ce:italic>catena</ce:italic>-[diaqua(2(2-aminopyrimidine))-μ-sulphato-O,O′nickel(II)]2-amino-pyrimidine (<ce:bold>2</ce:bold>), [pentaaqua(2-aminopyrimidine)nickel(II)]sulphate 2-aminopyrimidine (<ce:bold>3</ce:bold>) and <ce:italic>catena</ce:italic>-[aqua(2(2-aminopyrimidine))-μ-sulphato-O,O′-copper(II)] dihydrate (<ce:bold>4</ce:bold>) were prepared, structure determined by X-ray methods and physical properties studied by magnetic, IR, NMR, EPR and reflectance methods. The thermal behaviour was studied by TG and mass spectrometric methods. The results are discussed on a structural basis.</ce:simple-para></ce:abstract-sec></ce:abstract></head></converted-article></istex:document></istex:metadataXml><mods version="3.6"><titleInfo><title>Studies on coordination compounds—VIII. Syntheses, structural, magnetic, spectral and thermal properties of some cobalt(II), nickel(II) and copper(II) complexes of 2-aminopyrimidine</title></titleInfo><titleInfo type="alternative" contentType="CDATA"><title>Studies on coordination compounds—VIII. Syntheses, structural, magnetic, spectral and thermal properties of some cobalt(II), nickel(II) and copper(II) complexes of 2-aminopyrimidine</title></titleInfo><name type="personal"><namePart type="given">Paavo O.</namePart><namePart type="family">Lumme</namePart><affiliation>Division of Inorganic Chemistry, Department of Chemistry, University of Helsinki, Vuorikatu 20, P.O. Box 6, SF-00014, Helsinki, Finland</affiliation><description>Author to whom correspondence should be addressed.</description><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Hilkka</namePart><namePart type="family">Knuuttila</namePart><affiliation>Department of Chemistry, University of Jyväskylä, Jyväskylä, Finland</affiliation><description>Present address: Research Centre, Neste OY, 06850 Kulloo, Finland.</description><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="research-article" displayLabel="Full-length article"></genre><originInfo><publisher>ELSEVIER</publisher><dateIssued encoding="w3cdtf">1995</dateIssued><copyrightDate encoding="w3cdtf">1995</copyrightDate></originInfo><language><languageTerm type="code" authority="iso639-2b">eng</languageTerm><languageTerm type="code" authority="rfc3066">en</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType></physicalDescription><abstract lang="en">The complexes bis[triaqua(2-aminopyrimidine)-μ-sulphato-O,O′-cobalt(II)] dihydrate (1), catena-[diaqua(2(2-aminopyrimidine))-μ-sulphato-O,O′nickel(II)]2-amino-pyrimidine (2), [pentaaqua(2-aminopyrimidine)nickel(II)]sulphate 2-aminopyrimidine (3) and catena-[aqua(2(2-aminopyrimidine))-μ-sulphato-O,O′-copper(II)] dihydrate (4) were prepared, structure determined by X-ray methods and physical properties studied by magnetic, IR, NMR, EPR and reflectance methods. The thermal behaviour was studied by TG and mass spectrometric methods. The results are discussed on a structural basis.</abstract><note>Part VII: P. Lumme and P. Knuuttila, J. Thermal Analysis 1982, 25, 139.</note><relatedItem type="host"><titleInfo><title>Polyhedron</title></titleInfo><titleInfo type="abbreviated"><title>POLY</title></titleInfo><genre type="journal">journal</genre><originInfo><dateIssued encoding="w3cdtf">199506</dateIssued></originInfo><identifier type="ISSN">0277-5387</identifier><identifier type="PII">S0277-5387(00)X0026-5</identifier><part><date>199506</date><detail type="volume"><number>14</number><caption>vol.</caption></detail><detail type="issue"><number>12</number><caption>no.</caption></detail><extent unit="issue pages"><start>1531</start><end>1697</end></extent><extent unit="pages"><start>1553</start><end>1563</end></extent></part></relatedItem><identifier type="istex">90F6EE7CF1BCFDDA3E1BE5DDBEF400919C0A94A1</identifier><identifier type="DOI">10.1016/0277-5387(94)00442-H</identifier><identifier type="PII">0277-5387(94)00442-H</identifier><recordInfo><recordContentSource>ELSEVIER</recordContentSource></recordInfo></mods></metadata><serie></serie></istex></record>Pour manipuler ce document sous Unix (Dilib)
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