Synthesis and structure of chloro(ligand)bis(diphenylglyoximato)cobalt(III) complexes
Identifieur interne : 002149 ( Istex/Curation ); précédent : 002148; suivant : 002150Synthesis and structure of chloro(ligand)bis(diphenylglyoximato)cobalt(III) complexes
Auteurs : Concepci N L Pez [Espagne] ; Santiago Alvarez [Espagne] ; Magdalena Aguil [Espagne] ; Xavier Solans [Espagne] ; Manuel Font-Altaba [Espagne]Source :
- Inorganica Chimica Acta [ 0020-1693 ] ; 1986.
Abstract
The synthesis and characterization of trans-chloro- (ligand)bis(diphenylglyoximato)cobalt(III) complexes [ligand = pyridine (py), α-, β-, or γ-picoline (α-pic, β-pic, γ-pic), 3,5-lutidine (lut), p-toluidine (p-tol) and PPh3] is presented. X-ray crystal structure determination of the pyridine (1) and p-toluidine (6) derivatives has been carried out. Compound 1 crystallizes in the monoclinic system, space group P21/n, with Z = 4 and unit cell parameters a = 23.124(4), b = 13.009(3) and c = 11.204(3) Å, and β= 93.14(2)°. Compound 6 crystallizes in the monoclinic system, space group P21/n, with Z = 4 and unit cell parameters a = 18.792(3), b = 12.540(2) and c = 15.346(3) Å, and β = 97.54(2)°.
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DOI: 10.1016/S0020-1693(00)82115-5
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(p-tol) and PPh3] is presented. X-ray crystal structure determination of the pyridine (1) and p-toluidine (6) derivatives has been carried out. Compound 1 crystallizes in the monoclinic system, space group P21/n, with Z = 4 and unit cell parameters a = 23.124(4), b = 13.009(3) and c = 11.204(3) Å, and β= 93.14(2)°. Compound 6 crystallizes in the monoclinic system, space group P21/n, with Z = 4 and unit cell parameters a = 18.792(3), b = 12.540(2) and c = 15.346(3) Å, and β = 97.54(2)°.</div></front></TEI></record>Pour manipuler ce document sous Unix (Dilib)
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