An Unprecedented Hexapotassium‐Hexamagnesium 24‐Membered Macrocyclic Amide: A Polymetallic Cationic Host to Six Monodeprotonated Arene Anions
Identifieur interne : 000E03 ( Istex/Corpus ); précédent : 000E02; suivant : 000E04An Unprecedented Hexapotassium‐Hexamagnesium 24‐Membered Macrocyclic Amide: A Polymetallic Cationic Host to Six Monodeprotonated Arene Anions
Auteurs : Philip C. Andrews ; Alan R. Kennedy ; Robert E. Mulvey ; Colin L. Raston ; Brett A. Roberts ; René B. RowlingsSource :
- Angewandte Chemie International Edition [ 1433-7851 ] ; 2000-06-02.
English descriptors
Abstract
Six arene anions in a cationic [K6Mg6N12]6+ ring (see picture, arene=benzene) are reported in the mixed‐metal macrocyclic amide of 24 (!) ring atoms. The macrocycle is produced through a very effective synthesis, in which the anions are selectively monodeprotonated.
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DOI: 10.1002/1521-3773(20000602)39:11<1960::AID-ANIE1960>3.0.CO;2-D
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ISTEX:C452AF1664939252F03FAB375D340FA5E9741510Le document en format XML
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Rep. of Germany</copyright><eventGroup><event type="manuscriptReceived" date="2000-02-07"></event><event type="firstOnline" date="2000-06-14"></event><event type="publishedOnlineFinalForm" date="2000-06-14"></event><event type="xmlConverted" agent="Converter:JWSART34_TO_WML3G version:2.4.7 mode:FullText source:Header result:Header" date="2011-02-24"></event><event type="xmlConverted" agent="Converter:WILEY_ML3G_TO_WILEY_ML3GV2 version:3.8.8" date="2014-01-03"></event><event type="xmlConverted" agent="Converter:WML3G_To_WML3G version:4.1.7 mode:FullText,remove_FC" date="2014-10-14"></event></eventGroup><numberingGroup><numbering type="pageFirst">1960</numbering><numbering type="pageLast">1962</numbering></numberingGroup><linkGroup><link type="toTypesetVersion" href="file:ANIE.ANIE1960.pdf"></link></linkGroup></publicationMeta><contentMeta><countGroup><count type="figureTotal" number="12"></count><count type="tableTotal" number="0"></count><count type="referenceTotal" number="14"></count></countGroup><titleGroup><title type="main" xml:lang="en">An Unprecedented Hexapotassium‐Hexamagnesium 24‐Membered Macrocyclic Amide: A Polymetallic Cationic Host to Six Monodeprotonated Arene Anions</title></titleGroup><creators><creator xml:id="au1" creatorRole="author" affiliationRef="#afb"><personName><givenNames>Philip C.</givenNames><familyName>Andrews</familyName><degrees>Dr.</degrees></personName></creator><creator xml:id="au2" creatorRole="author" affiliationRef="#afa"><personName><givenNames>Alan R.</givenNames><familyName>Kennedy</familyName><degrees>Dr.</degrees></personName></creator><creator xml:id="au3" creatorRole="author" affiliationRef="#afa"><personName><givenNames>Robert E.</givenNames><familyName>Mulvey</familyName><degrees>Prof.</degrees></personName><contactDetails><email>r.e.mulvey@strath.ac.uk</email></contactDetails></creator><creator xml:id="au4" creatorRole="author" affiliationRef="#afb"><personName><givenNames>Colin L.</givenNames><familyName>Raston</familyName><degrees>Prof.</degrees></personName></creator><creator xml:id="au5" creatorRole="author" affiliationRef="#afb"><personName><givenNames>Brett A.</givenNames><familyName>Roberts</familyName></personName></creator><creator xml:id="au6" creatorRole="author" affiliationRef="#afa"><personName><givenNames>René B.</givenNames><familyName>Rowlings</familyName><degrees>Dr.</degrees></personName></creator></creators><affiliationGroup><affiliation xml:id="afa" countryCode="GB" type="organization"><unparsedAffiliation>Department of Pure and Applied Chemistry University of Strathclyde Glasgow, G1 1XL, UK, Fax: (+44) 141‐552‐0876</unparsedAffiliation></affiliation><affiliation xml:id="afb" countryCode="AU" type="organization"><unparsedAffiliation>Department of Chemistry Monash University Clayton, Victoria, 3168, Australia</unparsedAffiliation></affiliation></affiliationGroup><keywordGroup xml:lang="en" type="author"><keyword xml:id="kwd1">alkali metals</keyword><keyword xml:id="kwd2">alkaline earth metals</keyword><keyword xml:id="kwd3">amides</keyword><keyword xml:id="kwd4">macrocycles</keyword><keyword xml:id="kwd5">template synthesis</keyword></keywordGroup><abstractGroup><abstract type="graphical" xml:lang="en"><p><b>Six arene anions</b> in a cationic [K<sub>6</sub>Mg<sub>6</sub>N<sub>12</sub>]<sup>6+</sup> ring (see picture, arene=benzene) are reported in the mixed‐metal macrocyclic amide of 24 (!) ring atoms. The macrocycle is produced through a very effective synthesis, in which the anions are selectively monodeprotonated.<blockFixed type="graphic"><mediaResourceGroup><mediaResource alt="image" eRights="yes" copyright="WILEY-VCH" href="urn:x-wiley:14337851:media:ANIE1960:content"></mediaResource><mediaResource alt="thumbnail image" rendition="webLoRes" mimeType="image/gif" resourceExtraInfo="missing" href=""></mediaResource><mediaResource alt="original image" rendition="webOriginal" mimeType="image/x-unknown" resourceExtraInfo="missingGifOrJpg" href=""></mediaResource><mediaResource alt="magnified image" rendition="webHiRes" mimeType="image/x-unknown" resourceExtraInfo="missingGifOrJpg" href=""></mediaResource></mediaResourceGroup></blockFixed></p></abstract></abstractGroup></contentMeta><noteGroup><note xml:id="fnxx" numbered="no"><p>This work was supported by the UK Engineering and Physical Science Research Council (Grant award No. GR/M78113). Thanks are also extended to Dr. P. J. Nichols for help with the crystallographic work.</p></note></noteGroup></header></component></istex:document></istex:metadataXml><mods version="3.6"><titleInfo lang="en"><title>An Unprecedented Hexapotassium‐Hexamagnesium 24‐Membered Macrocyclic Amide: A Polymetallic Cationic Host to Six Monodeprotonated Arene Anions</title></titleInfo><titleInfo type="alternative" contentType="CDATA" lang="en"><title>An Unprecedented Hexapotassium‐Hexamagnesium 24‐Membered Macrocyclic Amide: A Polymetallic Cationic Host to Six Monodeprotonated Arene Anions</title></titleInfo><name type="personal"><namePart type="given">Philip C.</namePart><namePart type="family">Andrews</namePart><namePart type="termsOfAddress">Dr.</namePart><affiliation>Department of Chemistry Monash University Clayton, Victoria, 3168, Australia</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Alan R.</namePart><namePart type="family">Kennedy</namePart><namePart type="termsOfAddress">Dr.</namePart><affiliation>Department of Pure and Applied Chemistry University of Strathclyde Glasgow, G1 1XL, UK, Fax: (+44) 141‐552‐0876</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Robert E.</namePart><namePart type="family">Mulvey</namePart><namePart type="termsOfAddress">Prof.</namePart><affiliation>Department of Pure and Applied Chemistry University of Strathclyde Glasgow, G1 1XL, UK, Fax: (+44) 141‐552‐0876</affiliation><affiliation>E-mail: r.e.mulvey@strath.ac.uk</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Colin L.</namePart><namePart type="family">Raston</namePart><namePart type="termsOfAddress">Prof.</namePart><affiliation>Department of Chemistry Monash University Clayton, Victoria, 3168, Australia</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">Brett A.</namePart><namePart type="family">Roberts</namePart><affiliation>Department of Chemistry Monash University Clayton, Victoria, 3168, Australia</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">René B.</namePart><namePart type="family">Rowlings</namePart><namePart type="termsOfAddress">Dr.</namePart><affiliation>Department of Pure and Applied Chemistry University of Strathclyde Glasgow, G1 1XL, UK, Fax: (+44) 141‐552‐0876</affiliation><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="brief-communication" displayLabel="shortCommunication"></genre><originInfo><publisher>WILEY‐VCH Verlag GmbH</publisher><place><placeTerm type="text">Weinheim</placeTerm></place><dateIssued encoding="w3cdtf">2000-06-02</dateIssued><dateCaptured encoding="w3cdtf">2000-02-07</dateCaptured><copyrightDate encoding="w3cdtf">2000</copyrightDate></originInfo><language><languageTerm type="code" authority="rfc3066">en</languageTerm><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType><extent unit="figures">12</extent><extent unit="references">14</extent></physicalDescription><abstract type="graphical" lang="en">Six arene anions in a cationic [K6Mg6N12]6+ ring (see picture, arene=benzene) are reported in the mixed‐metal macrocyclic amide of 24 (!) ring atoms. The macrocycle is produced through a very effective synthesis, in which the anions are selectively monodeprotonated.</abstract><subject lang="en"><genre>keywords</genre><topic>alkali metals</topic><topic>alkaline earth metals</topic><topic>amides</topic><topic>macrocycles</topic><topic>template synthesis</topic></subject><relatedItem type="host"><titleInfo><title>Angewandte Chemie International Edition</title></titleInfo><titleInfo type="abbreviated"><title>Angew. Chem. Int. Ed.</title></titleInfo><genre type="journal">journal</genre><subject><genre>article-category</genre><topic>Communication</topic></subject><identifier type="ISSN">1433-7851</identifier><identifier type="eISSN">1521-3773</identifier><identifier type="DOI">10.1002/(ISSN)1521-3773</identifier><identifier type="PublisherID">ANIE</identifier><part><date>2000</date><detail type="volume"><caption>vol.</caption><number>39</number></detail><detail type="issue"><caption>no.</caption><number>11</number></detail><extent unit="pages"><start>1960</start><end>1962</end><total>3</total></extent></part></relatedItem><identifier type="istex">C452AF1664939252F03FAB375D340FA5E9741510</identifier><identifier type="DOI">10.1002/1521-3773(20000602)39:11<1960::AID-ANIE1960>3.0.CO;2-D</identifier><identifier type="ArticleID">ANIE1960</identifier><accessCondition type="use and reproduction" contentType="copyright">Copyright © 2000 WILEY‐VCH Verlag GmbH, Weinheim, Fed. Rep. of Germany</accessCondition><recordInfo><recordContentSource>WILEY</recordContentSource><recordOrigin>WILEY‐VCH Verlag GmbH</recordOrigin></recordInfo></mods></metadata><serie></serie></istex></record>Pour manipuler ce document sous Unix (Dilib)
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