Complete assignments of the 1H and 13C NMR spectra of 9,10‐didehydro retinoic acids
Identifieur interne : 000222 ( Istex/Corpus ); précédent : 000221; suivant : 000223Complete assignments of the 1H and 13C NMR spectra of 9,10‐didehydro retinoic acids
Auteurs : J. Thibonnet ; A. Duchêne ; J. Parrain ; M. AbarbriSource :
- Magnetic Resonance in Chemistry [ 0749-1581 ] ; 2006-05.
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Abstract
A new class of retinoic acids was synthesized containing a 9,10‐rigid bond. 1H and 13C NMR spectra were assigned for eight new compounds (all‐E, 13Z) containing a carboxylic acid or tertiobutylester polar end group. Assignments were based on the combination of one‐ and two‐ dimensional experiments (APT, COSY, HMBC). Copyright © 2006 John Wiley & Sons, Ltd.
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DOI: 10.1002/mrc.1800
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<abstractGroup><abstract type="main" xml:lang="en"><title type="main">Abstract</title>
<p>A new class of retinoic acids was synthesized containing a 9,10‐rigid bond. <sup>1</sup>
H and <sup>13</sup>
C NMR spectra were assigned for eight new compounds (all‐<i>E</i>
, 13<i>Z</i>
) containing a carboxylic acid or tertiobutylester polar end group. Assignments were based on the combination of one‐ and two‐ dimensional experiments (APT, COSY, HMBC). Copyright © 2006 John Wiley & Sons, Ltd.</p>
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<name type="personal"><namePart type="given">J.</namePart>
<namePart type="family">Thibonnet</namePart>
<affiliation>Laboratoire de Synthèse et Physicochimie Organique et Thérapeutique, Faculté des Sciences de Tours, Parc de Grandmont, EA 3857, 37200 Tours, France</affiliation>
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<affiliation>Laboratoire de Synthèse et Physicochimie Organique et Thérapeutique, Faculté des Sciences de Tours, Parc de Grandmont, EA 3857, 37200 Tours, France</affiliation>
<affiliation>Laboratoire de Synthèse et Physicochimie Organique et Thérapeutique, Faculté des Sciences de Tours, Parc de Grandmont, EA 3857, 37200 Tours, France.===</affiliation>
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<abstract lang="en">A new class of retinoic acids was synthesized containing a 9,10‐rigid bond. 1H and 13C NMR spectra were assigned for eight new compounds (all‐E, 13Z) containing a carboxylic acid or tertiobutylester polar end group. Assignments were based on the combination of one‐ and two‐ dimensional experiments (APT, COSY, HMBC). Copyright © 2006 John Wiley & Sons, Ltd.</abstract>
<subject lang="en"><genre>keywords</genre>
<topic>9</topic>
<topic>10‐didehydro retinoids</topic>
<topic>NMR</topic>
<topic>1H NMR</topic>
<topic>13C NMR</topic>
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<topic>Spectral Assignments and Reference Data</topic>
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<identifier type="ISSN">0749-1581</identifier>
<identifier type="eISSN">1097-458X</identifier>
<identifier type="DOI">10.1002/(ISSN)1097-458Xa</identifier>
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