Complete assignments of the 1H and 13C NMR spectra of 9,10‐didehydro retinoic acids
Identifieur interne : 000222 ( Istex/Corpus ); précédent : 000221; suivant : 000223Complete assignments of the 1H and 13C NMR spectra of 9,10‐didehydro retinoic acids
Auteurs : J. Thibonnet ; A. Duchêne ; J. Parrain ; M. AbarbriSource :
- Magnetic Resonance in Chemistry [ 0749-1581 ] ; 2006-05.
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Abstract
A new class of retinoic acids was synthesized containing a 9,10‐rigid bond. 1H and 13C NMR spectra were assigned for eight new compounds (all‐E, 13Z) containing a carboxylic acid or tertiobutylester polar end group. Assignments were based on the combination of one‐ and two‐ dimensional experiments (APT, COSY, HMBC). Copyright © 2006 John Wiley & Sons, Ltd.
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DOI: 10.1002/mrc.1800
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ISTEX:09BA30B791C311891033ACC3ADE92A0762F71479Le document en format XML
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Copyright © 2006 John Wiley & Sons, Ltd.</p></abstract></abstractGroup></contentMeta></header></component></istex:document></istex:metadataXml><mods version="3.6"><titleInfo lang="en"><title>Complete assignments of the 1H and 13C NMR spectra of 9,10‐didehydro retinoic acids</title></titleInfo><titleInfo type="abbreviated" lang="en"><title>Spectral Assignments and Reference Data</title></titleInfo><titleInfo type="alternative" contentType="CDATA" lang="en"><title>Complete assignments of the 1H and 13C NMR spectra of 9,10‐didehydro retinoic acids</title></titleInfo><name type="personal"><namePart type="given">J.</namePart><namePart type="family">Thibonnet</namePart><affiliation>Laboratoire de Synthèse et Physicochimie Organique et Thérapeutique, Faculté des Sciences de Tours, Parc de Grandmont, EA 3857, 37200 Tours, France</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">A.</namePart><namePart type="family">Duchêne</namePart><affiliation>Laboratoire de Synthèse et Physicochimie Organique et Thérapeutique, Faculté des Sciences de Tours, Parc de Grandmont, EA 3857, 37200 Tours, France</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">J.‐L.</namePart><namePart type="family">Parrain</namePart><affiliation>Laboratoire Symbio, Equipe Synthèse par voie Organométallique associé au CNRS (UMR 6178), Université Paul Cézanne, Aix Marseille III, Campus Scientifique de Saint Jérôme, Avenue Escadrille Normandie‐Niemen, 13397 Marseille Cedex 20, France</affiliation><role><roleTerm type="text">author</roleTerm></role></name><name type="personal"><namePart type="given">M.</namePart><namePart type="family">Abarbri</namePart><affiliation>Laboratoire de Synthèse et Physicochimie Organique et Thérapeutique, Faculté des Sciences de Tours, Parc de Grandmont, EA 3857, 37200 Tours, France</affiliation><affiliation>Laboratoire de Synthèse et Physicochimie Organique et Thérapeutique, Faculté des Sciences de Tours, Parc de Grandmont, EA 3857, 37200 Tours, France.===</affiliation><role><roleTerm type="text">author</roleTerm></role></name><typeOfResource>text</typeOfResource><genre type="article" displayLabel="article"></genre><originInfo><publisher>John Wiley & Sons, Ltd.</publisher><place><placeTerm type="text">Chichester, UK</placeTerm></place><dateIssued encoding="w3cdtf">2006-05</dateIssued><dateCaptured encoding="w3cdtf">2005-12-21</dateCaptured><dateValid encoding="w3cdtf">2006-02-02</dateValid><copyrightDate encoding="w3cdtf">2006</copyrightDate></originInfo><language><languageTerm type="code" authority="rfc3066">en</languageTerm><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType><extent unit="figures">2</extent><extent unit="tables">2</extent><extent unit="references">6</extent></physicalDescription><abstract lang="en">A new class of retinoic acids was synthesized containing a 9,10‐rigid bond. 1H and 13C NMR spectra were assigned for eight new compounds (all‐E, 13Z) containing a carboxylic acid or tertiobutylester polar end group. Assignments were based on the combination of one‐ and two‐ dimensional experiments (APT, COSY, HMBC). Copyright © 2006 John Wiley & Sons, Ltd.</abstract><subject lang="en"><genre>keywords</genre><topic>9</topic><topic>10‐didehydro retinoids</topic><topic>NMR</topic><topic>1H NMR</topic><topic>13C NMR</topic></subject><relatedItem type="host"><titleInfo><title>Magnetic Resonance in Chemistry</title></titleInfo><titleInfo type="abbreviated"><title>Magn. Reson. Chem.</title></titleInfo><genre type="journal">journal</genre><subject><genre>article-category</genre><topic>Spectral Assignments and Reference Data</topic></subject><identifier type="ISSN">0749-1581</identifier><identifier type="eISSN">1097-458X</identifier><identifier type="DOI">10.1002/(ISSN)1097-458Xa</identifier><identifier type="PublisherID">MRC</identifier><part><date>2006</date><detail type="volume"><caption>vol.</caption><number>44</number></detail><detail type="issue"><caption>no.</caption><number>6</number></detail><extent unit="pages"><start>651</start><end>653</end><total>3</total></extent></part></relatedItem><identifier type="istex">09BA30B791C311891033ACC3ADE92A0762F71479</identifier><identifier type="DOI">10.1002/mrc.1800</identifier><identifier type="ArticleID">MRC1800</identifier><accessCondition type="use and reproduction" contentType="copyright">Copyright © 2006 John Wiley & Sons, Ltd.</accessCondition><recordInfo><recordContentSource>WILEY</recordContentSource><recordOrigin>John Wiley & Sons, Ltd.</recordOrigin></recordInfo></mods></metadata><serie></serie></istex></record>Pour manipuler ce document sous Unix (Dilib)
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