Size Matters: Chemical Synthesis of a Homogenous Arabinogalactan 92-mer.
Identifieur interne : 000C55 ( PubMed/Curation ); précédent : 000C54; suivant : 000C56Size Matters: Chemical Synthesis of a Homogenous Arabinogalactan 92-mer.
Auteurs : Maciej A. Walczak [États-Unis] ; Feng Zhu [États-Unis]Source :
- Chembiochem : a European journal of chemical biology [ 1439-7633 ] ; 2017.
Descripteurs français
- KwdFr :
- MESH :
- métabolisme : Mycobacterium tuberculosis, Paroi cellulaire.
- synthèse chimique : Galactanes.
- Galactanes, Morpholines, Méthanesulfonates, Oligosaccharides.
English descriptors
- KwdEn :
- MESH :
- chemical , chemical synthesis : Galactans.
- chemical , chemistry : Galactans, Mesylates, Morpholines, Oligosaccharides.
- metabolism : Cell Wall, Mycobacterium tuberculosis.
Abstract
31+30+31: Ye and colleagues have synthesized a branched 92-mer of arabinogalactan-a major component of the cell wall of M. tuberculosis-by linking a linear oligogalactan 30-mer with two d-arabinofuranose 31-mers. Their approach capitalizes on sequential, one-pot glycosylation reactions that result in a rapid increase in molecular complexity and efficient synthesis of a branched oligosaccharide.
DOI: 10.1002/cbic.201700311
PubMed: 28628733
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Walczak</name><affiliation wicri:level="1"><nlm:affiliation>Department of Chemistry and Biochemistry, University of Colorado, 215 UCB, Boulder, CO, 80309, USA.</nlm:affiliation><country xml:lang="fr">États-Unis</country><wicri:regionArea>Department of Chemistry and Biochemistry, University of Colorado, 215 UCB, Boulder, CO, 80309</wicri:regionArea></affiliation></author><author><name sortKey="Zhu, Feng" sort="Zhu, Feng" uniqKey="Zhu F" first="Feng" last="Zhu">Feng Zhu</name><affiliation wicri:level="1"><nlm:affiliation>Department of Chemistry and Biochemistry, University of Colorado, 215 UCB, Boulder, CO, 80309, USA.</nlm:affiliation><country xml:lang="fr">États-Unis</country><wicri:regionArea>Department of Chemistry and Biochemistry, University of Colorado, 215 UCB, Boulder, CO, 80309</wicri:regionArea></affiliation></author></analytic><series><title level="j">Chembiochem : a European journal of chemical biology</title><idno type="eISSN">1439-7633</idno><imprint><date when="2017" type="published">2017</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Cell Wall (metabolism)</term><term>Galactans (chemical synthesis)</term><term>Galactans (chemistry)</term><term>Mesylates (chemistry)</term><term>Morpholines (chemistry)</term><term>Mycobacterium tuberculosis (metabolism)</term><term>Oligosaccharides (chemistry)</term></keywords><keywords scheme="KwdFr" xml:lang="fr"><term>Galactanes ()</term><term>Galactanes (synthèse chimique)</term><term>Morpholines ()</term><term>Mycobacterium tuberculosis (métabolisme)</term><term>Méthanesulfonates ()</term><term>Oligosaccharides ()</term><term>Paroi cellulaire (métabolisme)</term></keywords><keywords scheme="MESH" type="chemical" qualifier="chemical synthesis" xml:lang="en"><term>Galactans</term></keywords><keywords scheme="MESH" type="chemical" qualifier="chemistry" xml:lang="en"><term>Galactans</term><term>Mesylates</term><term>Morpholines</term><term>Oligosaccharides</term></keywords><keywords scheme="MESH" qualifier="metabolism" xml:lang="en"><term>Cell Wall</term><term>Mycobacterium tuberculosis</term></keywords><keywords scheme="MESH" qualifier="métabolisme" xml:lang="fr"><term>Mycobacterium tuberculosis</term><term>Paroi cellulaire</term></keywords><keywords scheme="MESH" qualifier="synthèse chimique" xml:lang="fr"><term>Galactanes</term></keywords><keywords scheme="MESH" xml:lang="fr"><term>Galactanes</term><term>Morpholines</term><term>Méthanesulfonates</term><term>Oligosaccharides</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">31+30+31: Ye and colleagues have synthesized a branched 92-mer of arabinogalactan-a major component of the cell wall of M. tuberculosis-by linking a linear oligogalactan 30-mer with two d-arabinofuranose 31-mers. Their approach capitalizes on sequential, one-pot glycosylation reactions that result in a rapid increase in molecular complexity and efficient synthesis of a branched oligosaccharide.</div></front></TEI><pubmed><MedlineCitation Status="MEDLINE" Owner="NLM"><PMID Version="1">28628733</PMID><DateCompleted><Year>2017</Year><Month>09</Month><Day>28</Day></DateCompleted><DateRevised><Year>2018</Year><Month>04</Month><Day>18</Day></DateRevised><Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Electronic">1439-7633</ISSN><JournalIssue CitedMedium="Internet"><Volume>18</Volume><Issue>18</Issue><PubDate><Year>2017</Year><Month>09</Month><Day>19</Day></PubDate></JournalIssue><Title>Chembiochem : a European journal of chemical biology</Title><ISOAbbreviation>Chembiochem</ISOAbbreviation></Journal><ArticleTitle>Size Matters: Chemical Synthesis of a Homogenous Arabinogalactan 92-mer.</ArticleTitle><Pagination><MedlinePgn>1789-1791</MedlinePgn></Pagination><ELocationID EIdType="doi" ValidYN="Y">10.1002/cbic.201700311</ELocationID><Abstract><AbstractText>31+30+31: Ye and colleagues have synthesized a branched 92-mer of arabinogalactan-a major component of the cell wall of M. tuberculosis-by linking a linear oligogalactan 30-mer with two d-arabinofuranose 31-mers. Their approach capitalizes on sequential, one-pot glycosylation reactions that result in a rapid increase in molecular complexity and efficient synthesis of a branched oligosaccharide.</AbstractText><CopyrightInformation>© 2017 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.</CopyrightInformation></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Walczak</LastName><ForeName>Maciej A</ForeName><Initials>MA</Initials><AffiliationInfo><Affiliation>Department of Chemistry and Biochemistry, University of Colorado, 215 UCB, Boulder, CO, 80309, USA.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Zhu</LastName><ForeName>Feng</ForeName><Initials>F</Initials><AffiliationInfo><Affiliation>Department of Chemistry and Biochemistry, University of Colorado, 215 UCB, Boulder, CO, 80309, USA.</Affiliation></AffiliationInfo></Author></AuthorList><Language>eng</Language><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType><PublicationType UI="D013485">Research Support, Non-U.S. Gov't</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2017</Year><Month>08</Month><Day>09</Day></ArticleDate></Article><MedlineJournalInfo><Country>Germany</Country><MedlineTA>Chembiochem</MedlineTA><NlmUniqueID>100937360</NlmUniqueID><ISSNLinking>1439-4227</ISSNLinking></MedlineJournalInfo><ChemicalList><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance UI="D005685">Galactans</NameOfSubstance></Chemical><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance UI="D008698">Mesylates</NameOfSubstance></Chemical><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance UI="D009025">Morpholines</NameOfSubstance></Chemical><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance UI="D009844">Oligosaccharides</NameOfSubstance></Chemical><Chemical><RegistryNumber>8B2ZCK305O</RegistryNumber><NameOfSubstance UI="C037574">morpholine</NameOfSubstance></Chemical><Chemical><RegistryNumber>JE2SY203E8</RegistryNumber><NameOfSubstance UI="C012077">trifluoromethanesulfonic acid</NameOfSubstance></Chemical><Chemical><RegistryNumber>SL4SX1O487</RegistryNumber><NameOfSubstance UI="C005653">arabinogalactan</NameOfSubstance></Chemical></ChemicalList><CitationSubset>IM</CitationSubset><MeshHeadingList><MeshHeading><DescriptorName UI="D002473" MajorTopicYN="N">Cell Wall</DescriptorName><QualifierName UI="Q000378" MajorTopicYN="N">metabolism</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D005685" MajorTopicYN="N">Galactans</DescriptorName><QualifierName UI="Q000138" MajorTopicYN="N">chemical synthesis</QualifierName><QualifierName UI="Q000737" MajorTopicYN="Y">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D008698" MajorTopicYN="N">Mesylates</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="N">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D009025" MajorTopicYN="N">Morpholines</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="N">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D009169" MajorTopicYN="N">Mycobacterium tuberculosis</DescriptorName><QualifierName UI="Q000378" MajorTopicYN="N">metabolism</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D009844" MajorTopicYN="N">Oligosaccharides</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="N">chemistry</QualifierName></MeshHeading></MeshHeadingList><KeywordList Owner="NOTNLM"><Keyword MajorTopicYN="Y">arabinogalactan</Keyword><Keyword MajorTopicYN="Y">carbohydrates</Keyword><Keyword MajorTopicYN="Y">mycobacteria</Keyword><Keyword MajorTopicYN="Y">oligosaccharides</Keyword><Keyword MajorTopicYN="Y">total synthesis</Keyword></KeywordList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="received"><Year>2017</Year><Month>06</Month><Day>09</Day></PubMedPubDate><PubMedPubDate PubStatus="pubmed"><Year>2017</Year><Month>6</Month><Day>20</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="medline"><Year>2017</Year><Month>9</Month><Day>29</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="entrez"><Year>2017</Year><Month>6</Month><Day>20</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate></History><PublicationStatus>ppublish</PublicationStatus><ArticleIdList><ArticleId IdType="pubmed">28628733</ArticleId><ArticleId IdType="doi">10.1002/cbic.201700311</ArticleId></ArticleIdList></PubmedData></pubmed></record>Pour manipuler ce document sous Unix (Dilib)
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