MersV1, PubMed, Corpus, bibRecord, 001E20

N'-[(1E)-3-Bromo-5-chloro-2-hy-droxy-benzyl-idene]-4-tert-butyl-benzo-hydrazide ethanol monosolvate.

Identifieur interne : 001E20 ( PubMed/Corpus ); précédent : 001E19; suivant : 001E21

N'-[(1E)-3-Bromo-5-chloro-2-hy-droxy-benzyl-idene]-4-tert-butyl-benzo-hydrazide ethanol monosolvate.

Auteurs : A. Thirugnanasundar ; K. Parthipan ; V S Xavier Anthonisamy ; G. Chakkaravarthi ; G. Rajagopal

Source :

Acta crystallographica. Section E, Structure reports online [ 1600-5368 ] ; 2011.

RBID : pubmed:22219898

Abstract

In the title compound, C(18)H(18)BrClN(2)O(2)·C(2)H(6)O, the hy-droxy group forms an intra-molecular O-H⋯N hydrogen bond, which influences the conformation of the Shiff base mol-ecule, where the two aromatic rings form a dihedral angle of 21.67 (8)°. Inter-molecular N-H⋯O and O-H⋯O hydrogen bonds link two Shiff base mol-ecules and two solvent mol-ecules into a centrosymmetric heterotetra-mer. Weak inter-molecular C-H⋯O inter-actions link further tetra-mers related by translation along the a axis into chains.

DOI: 10.1107/S160053681104027X
PubMed: 22219898

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pubmed:22219898

Le document en format XML

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<author><name sortKey="Parthipan, K" sort="Parthipan, K" uniqKey="Parthipan K" first="K" last="Parthipan">K. Parthipan</name>
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<author><name sortKey="Anthonisamy, V S Xavier" sort="Anthonisamy, V S Xavier" uniqKey="Anthonisamy V" first="V S Xavier" last="Anthonisamy">V S Xavier Anthonisamy</name>
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<front><div type="abstract" xml:lang="en">In the title compound, C(18)H(18)BrClN(2)O(2)·C(2)H(6)O, the hy-droxy group forms an intra-molecular O-H⋯N hydrogen bond, which influences the conformation of the Shiff base mol-ecule, where the two aromatic rings form a dihedral angle of 21.67 (8)°. Inter-molecular N-H⋯O and O-H⋯O hydrogen bonds link two Shiff base mol-ecules and two solvent mol-ecules into a centrosymmetric heterotetra-mer. Weak inter-molecular C-H⋯O inter-actions link further tetra-mers related by translation along the a axis into chains.</div>
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<Reference><Citation>Bioorg Med Chem. 2006 Nov 15;14(22):7482-9</Citation>
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<Reference><Citation>Acta Crystallogr D Biol Crystallogr. 2009 Feb;65(Pt 2):148-55</Citation>
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N'-[(1E)-3-Bromo-5-chloro-2-hy-droxy-benzyl-idene]-4-tert-butyl-benzo-hydrazide ethanol monosolvate.

N'-[(1E)-3-Bromo-5-chloro-2-hy-droxy-benzyl-idene]-4-tert-butyl-benzo-hydrazide ethanol monosolvate.

Source :

Abstract

Links to Exploration step

Le document en format XML

Pour manipuler ce document sous Unix (Dilib)

Pour mettre un lien sur cette page dans le réseau Wicri

Pour générer des pages wiki