Stereochemical Sequence Dictates Unimolecular Diblock Copolymer Assembly.
Identifieur interne : 001D18 ( Ncbi/Merge ); précédent : 001D17; suivant : 001D19Stereochemical Sequence Dictates Unimolecular Diblock Copolymer Assembly.
Auteurs : Matthew R. Golder [États-Unis] ; Yivan Jiang [États-Unis] ; Paul E. Teichen [États-Unis] ; Hung V-T Nguyen [États-Unis] ; Wencong Wang [États-Unis] ; Nicole Milos [États-Unis] ; Seth A. Freedman [États-Unis] ; Adam P. Willard [États-Unis] ; Jeremiah A. Johnson [États-Unis]Source :
- Journal of the American Chemical Society [ 1520-5126 ] ; 2018.
Descripteurs français
- KwdFr :
- MESH :
- synthèse chimique : Polymères.
- Conformation moléculaire, Polymères, Stéréoisomérie.
English descriptors
- KwdEn :
- MESH :
- chemical , chemical synthesis : Polymers.
- chemical , chemistry : Polymers.
- Molecular Conformation, Stereoisomerism.
Abstract
Deciphering the significance of length, sequence, and stereochemistry in block copolymer self-assembly remains an ongoing challenge. A dearth of methods to access uniform block co-oligomers/polymers with precise stereochemical sequences has precluded such studies. Here, we develop iterative exponential growth methods for the synthesis of a small library of unimolecular stereoisomeric diblock 32-mers. X-ray scattering reveals that stereochemistry modulates the phase behavior of these polymers, which we rationalize based on simulations carried out on a theoretical model system. This work demonstrates that stereochemical sequence can play a crucial role in unimolecular polymer self-assembly.
DOI: 10.1021/jacs.7b12696
PubMed: 29356516
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Golder</name><affiliation wicri:level="1"><nlm:affiliation>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143, United States.</nlm:affiliation><country xml:lang="fr">États-Unis</country><wicri:regionArea>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143</wicri:regionArea><wicri:noRegion>Massachusetts 02143</wicri:noRegion></affiliation></author><author><name sortKey="Jiang, Yivan" sort="Jiang, Yivan" uniqKey="Jiang Y" first="Yivan" last="Jiang">Yivan Jiang</name><affiliation wicri:level="1"><nlm:affiliation>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143, United States.</nlm:affiliation><country xml:lang="fr">États-Unis</country><wicri:regionArea>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143</wicri:regionArea><wicri:noRegion>Massachusetts 02143</wicri:noRegion></affiliation></author><author><name sortKey="Teichen, Paul E" sort="Teichen, Paul E" uniqKey="Teichen P" first="Paul E" last="Teichen">Paul E. 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Freedman</name><affiliation wicri:level="1"><nlm:affiliation>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143, United States.</nlm:affiliation><country xml:lang="fr">États-Unis</country><wicri:regionArea>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143</wicri:regionArea><wicri:noRegion>Massachusetts 02143</wicri:noRegion></affiliation></author><author><name sortKey="Willard, Adam P" sort="Willard, Adam P" uniqKey="Willard A" first="Adam P" last="Willard">Adam P. Willard</name><affiliation wicri:level="1"><nlm:affiliation>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143, United States.</nlm:affiliation><country xml:lang="fr">États-Unis</country><wicri:regionArea>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143</wicri:regionArea><wicri:noRegion>Massachusetts 02143</wicri:noRegion></affiliation></author><author><name sortKey="Johnson, Jeremiah A" sort="Johnson, Jeremiah A" uniqKey="Johnson J" first="Jeremiah A" last="Johnson">Jeremiah A. Johnson</name><affiliation wicri:level="1"><nlm:affiliation>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143, United States.</nlm:affiliation><country xml:lang="fr">États-Unis</country><wicri:regionArea>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143</wicri:regionArea><wicri:noRegion>Massachusetts 02143</wicri:noRegion></affiliation></author></analytic><series><title level="j">Journal of the American Chemical Society</title><idno type="eISSN">1520-5126</idno><imprint><date when="2018" type="published">2018</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Molecular Conformation</term><term>Polymers (chemical synthesis)</term><term>Polymers (chemistry)</term><term>Stereoisomerism</term></keywords><keywords scheme="KwdFr" xml:lang="fr"><term>Conformation moléculaire</term><term>Polymères ()</term><term>Polymères (synthèse chimique)</term><term>Stéréoisomérie</term></keywords><keywords scheme="MESH" type="chemical" qualifier="chemical synthesis" xml:lang="en"><term>Polymers</term></keywords><keywords scheme="MESH" type="chemical" qualifier="chemistry" xml:lang="en"><term>Polymers</term></keywords><keywords scheme="MESH" qualifier="synthèse chimique" xml:lang="fr"><term>Polymères</term></keywords><keywords scheme="MESH" xml:lang="en"><term>Molecular Conformation</term><term>Stereoisomerism</term></keywords><keywords scheme="MESH" xml:lang="fr"><term>Conformation moléculaire</term><term>Polymères</term><term>Stéréoisomérie</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Deciphering the significance of length, sequence, and stereochemistry in block copolymer self-assembly remains an ongoing challenge. A dearth of methods to access uniform block co-oligomers/polymers with precise stereochemical sequences has precluded such studies. Here, we develop iterative exponential growth methods for the synthesis of a small library of unimolecular stereoisomeric diblock 32-mers. X-ray scattering reveals that stereochemistry modulates the phase behavior of these polymers, which we rationalize based on simulations carried out on a theoretical model system. This work demonstrates that stereochemical sequence can play a crucial role in unimolecular polymer self-assembly.</div></front></TEI><pubmed><MedlineCitation Status="MEDLINE" Owner="NLM"><PMID Version="1">29356516</PMID><DateCompleted><Year>2018</Year><Month>07</Month><Day>09</Day></DateCompleted><DateRevised><Year>2018</Year><Month>11</Month><Day>13</Day></DateRevised><Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Electronic">1520-5126</ISSN><JournalIssue CitedMedium="Internet"><Volume>140</Volume><Issue>5</Issue><PubDate><Year>2018</Year><Month>02</Month><Day>07</Day></PubDate></JournalIssue><Title>Journal of the American Chemical Society</Title><ISOAbbreviation>J. Am. Chem. Soc.</ISOAbbreviation></Journal><ArticleTitle>Stereochemical Sequence Dictates Unimolecular Diblock Copolymer Assembly.</ArticleTitle><Pagination><MedlinePgn>1596-1599</MedlinePgn></Pagination><ELocationID EIdType="doi" ValidYN="Y">10.1021/jacs.7b12696</ELocationID><Abstract><AbstractText>Deciphering the significance of length, sequence, and stereochemistry in block copolymer self-assembly remains an ongoing challenge. A dearth of methods to access uniform block co-oligomers/polymers with precise stereochemical sequences has precluded such studies. Here, we develop iterative exponential growth methods for the synthesis of a small library of unimolecular stereoisomeric diblock 32-mers. X-ray scattering reveals that stereochemistry modulates the phase behavior of these polymers, which we rationalize based on simulations carried out on a theoretical model system. This work demonstrates that stereochemical sequence can play a crucial role in unimolecular polymer self-assembly.</AbstractText></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Golder</LastName><ForeName>Matthew R</ForeName><Initials>MR</Initials><Identifier Source="ORCID">0000-0001-5848-7366</Identifier><AffiliationInfo><Affiliation>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143, United States.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Jiang</LastName><ForeName>Yivan</ForeName><Initials>Y</Initials><AffiliationInfo><Affiliation>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143, United States.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Teichen</LastName><ForeName>Paul E</ForeName><Initials>PE</Initials><AffiliationInfo><Affiliation>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143, United States.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Nguyen</LastName><ForeName>Hung V-T</ForeName><Initials>HV</Initials><AffiliationInfo><Affiliation>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143, United States.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Wang</LastName><ForeName>Wencong</ForeName><Initials>W</Initials><AffiliationInfo><Affiliation>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143, United States.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Milos</LastName><ForeName>Nicole</ForeName><Initials>N</Initials><AffiliationInfo><Affiliation>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143, United States.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Freedman</LastName><ForeName>Seth A</ForeName><Initials>SA</Initials><AffiliationInfo><Affiliation>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143, United States.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Willard</LastName><ForeName>Adam P</ForeName><Initials>AP</Initials><Identifier Source="ORCID">0000-0002-0934-4737</Identifier><AffiliationInfo><Affiliation>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143, United States.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Johnson</LastName><ForeName>Jeremiah A</ForeName><Initials>JA</Initials><Identifier Source="ORCID">0000-0001-9157-6491</Identifier><AffiliationInfo><Affiliation>Department of Chemistry, Massachusetts Institute of Technology , Cambridge, Massachusetts 02143, United States.</Affiliation></AffiliationInfo></Author></AuthorList><Language>eng</Language><GrantList CompleteYN="Y"><Grant><GrantID>F32 EB023101</GrantID><Acronym>EB</Acronym><Agency>NIBIB NIH HHS</Agency><Country>United States</Country></Grant><Grant><GrantID>R01 CA220468</GrantID><Acronym>CA</Acronym><Agency>NCI NIH HHS</Agency><Country>United States</Country></Grant><Grant><GrantID>R01 EB000231</GrantID><Acronym>EB</Acronym><Agency>NIBIB NIH HHS</Agency><Country>United States</Country></Grant></GrantList><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType><PublicationType UI="D052061">Research Support, N.I.H., Extramural</PublicationType><PublicationType UI="D013486">Research Support, U.S. Gov't, Non-P.H.S.</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2018</Year><Month>01</Month><Day>22</Day></ArticleDate></Article><MedlineJournalInfo><Country>United States</Country><MedlineTA>J Am Chem Soc</MedlineTA><NlmUniqueID>7503056</NlmUniqueID><ISSNLinking>0002-7863</ISSNLinking></MedlineJournalInfo><ChemicalList><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance UI="D011108">Polymers</NameOfSubstance></Chemical></ChemicalList><CitationSubset>IM</CitationSubset><MeshHeadingList><MeshHeading><DescriptorName UI="D008968" MajorTopicYN="N">Molecular Conformation</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D011108" MajorTopicYN="N">Polymers</DescriptorName><QualifierName UI="Q000138" MajorTopicYN="Y">chemical synthesis</QualifierName><QualifierName UI="Q000737" MajorTopicYN="N">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D013237" MajorTopicYN="N">Stereoisomerism</DescriptorName></MeshHeading></MeshHeadingList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="pubmed"><Year>2018</Year><Month>1</Month><Day>23</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate 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name="États-Unis"><noRegion><name sortKey="Golder, Matthew R" sort="Golder, Matthew R" uniqKey="Golder M" first="Matthew R" last="Golder">Matthew R. Golder</name></noRegion><name sortKey="Freedman, Seth A" sort="Freedman, Seth A" uniqKey="Freedman S" first="Seth A" last="Freedman">Seth A. Freedman</name><name sortKey="Jiang, Yivan" sort="Jiang, Yivan" uniqKey="Jiang Y" first="Yivan" last="Jiang">Yivan Jiang</name><name sortKey="Johnson, Jeremiah A" sort="Johnson, Jeremiah A" uniqKey="Johnson J" first="Jeremiah A" last="Johnson">Jeremiah A. Johnson</name><name sortKey="Milos, Nicole" sort="Milos, Nicole" uniqKey="Milos N" first="Nicole" last="Milos">Nicole Milos</name><name sortKey="Nguyen, Hung V T" sort="Nguyen, Hung V T" uniqKey="Nguyen H" first="Hung V-T" last="Nguyen">Hung V-T Nguyen</name><name sortKey="Teichen, Paul E" sort="Teichen, Paul E" uniqKey="Teichen P" first="Paul E" last="Teichen">Paul E. Teichen</name><name sortKey="Wang, Wencong" sort="Wang, Wencong" uniqKey="Wang W" first="Wencong" last="Wang">Wencong Wang</name><name sortKey="Willard, Adam P" sort="Willard, Adam P" uniqKey="Willard A" first="Adam P" last="Willard">Adam P. Willard</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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